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The research has been analyzed by using scanning electron and transmission electron microscopy (SEM and TEM).To research microstructure in single crystal alumina induced by Vickers indentation and the effect of alumina microstructure induced by deformation twinning. Sapphire is a kind of alumina single crystal called Corundum. It has fine machinery, optical, chemistry and anti-radiationary nature and been used widespread in industry world in recent years. Mechanical twinning is the main mode of plastic deformation. It has two types (1) basal twinning (2) rhombohedral twinning. When author pressed 20 N on (0001) plane, it produces B (0001), R1 ( 102) and R1 ¡¨ ( 104) in cross- section. But when pressing 20 N in (1 10) plane, it produces B (0001), B 1 ( 101) and R2 ( 012) in cross-section. In order to understand the role of pressure direction in twinning at room temperature, this research will discuss what effects will be produced twinning microstructure of alumina sample and derivation of dislocation microstructure by using scanning electron and transmission electron microscopy.

Thesis (Ph. D.) in Physics--University of Maine, 2001. / Includes vita. Includes bibliographical references (leaves 122-128).

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Autoclave processing of large scale, one-piece structural parts made of carbon fiber-reinforced polymer composite materials is the key to decreasing manufacturing costs while at the same time increasing quality. Nonetheless, even in manufacturing simple flat parts, residual strains and stresses are unavoidable. For structural design purposes and to aid in the assembly procedures, it is desirable to have proven numerical tools that can be used to predict these residual geometrical and material properties in advance, thus avoid the costly experimental trial and error methods. A 2-D finite element-based code, COMPRO, has previously been developed in-house for predicting autoclave process-induced deformations and residual stresses in composite parts undergoing an entire cure cycle. To simulate the tool-part interaction, an important source of residual deformations/stresses, COMPRO used a non-zero thickness elastic shear layer as its only interface option. Moreover, the code did not account for the large deformations and strains and the resulting nonlinear effects that can arise during the early stages of the cure cycle when the material is rather compliant. In the present work, a contact surface employing a penalty method formulation is introduced at the tool-part interface. Its material-dependent parameters are a function of temperature, degree of cure, pressure and so forth. This makes the stick-slip condition plus separation between the part and the tool possible. The large displacements/rotations and large shear strains that develop at the early stages of the cure cycle when the resin has a very low elastic modulus provided the impetus to include a large strain/deformation option in COMPRO. A new “co-rotational stress formulation” was developed and found to provide a robust method for numerical treatment of very large deformation/strain problems involving anisotropic materials of interest here. Several verification and validation examples are used to calibrate the contact interface parameters and to demonstrate the correctness of implementation and the accuracy of the proposed method. A number of comparisons are made with exact solutions, other methods, other experiments and the same models in other commercial codes. Finally, several interesting cases are examined to explore the results of COMPRO predictions with the added options.

No description available.

No description available.

No description available.

Autoclave processing of large scale, one-piece structural parts made of carbon fiber-reinforced polymer composite materials is the key to decreasing manufacturing costs while at the same time increasing quality. Nonetheless, even in manufacturing simple flat parts, residual strains and stresses are unavoidable. For structural design purposes and to aid in the assembly procedures, it is desirable to have proven numerical tools that can be used to predict these residual geometrical and material properties in advance, thus avoid the costly experimental trial and error methods. A 2-D finite element-based code, COMPRO, has previously been developed in-house for predicting autoclave process-induced deformations and residual stresses in composite parts undergoing an entire cure cycle. To simulate the tool-part interaction, an important source of residual deformations/stresses, COMPRO used a non-zero thickness elastic shear layer as its only interface option. Moreover, the code did not account for the large deformations and strains and the resulting nonlinear effects that can arise during the early stages of the cure cycle when the material is rather compliant. In the present work, a contact surface employing a penalty method formulation is introduced at the tool-part interface. Its material-dependent parameters are a function of temperature, degree of cure, pressure and so forth. This makes the stick-slip condition plus separation between the part and the tool possible. The large displacements/rotations and large shear strains that develop at the early stages of the cure cycle when the resin has a very low elastic modulus provided the impetus to include a large strain/deformation option in COMPRO. A new “co-rotational stress formulation” was developed and found to provide a robust method for numerical treatment of very large deformation/strain problems involving anisotropic materials of interest here. Several verification and validation examples are used to calibrate the contact interface parameters and to demonstrate the correctness of implementation and the accuracy of the proposed method. A number of comparisons are made with exact solutions, other methods, other experiments and the same models in other commercial codes. Finally, several interesting cases are examined to explore the results of COMPRO predictions with the added options.

GPS has been used to monitor engineering structures for a number of reasons. One important reason for monitoring high rise buildings (and other engineering structures) is their safety assessment in events of extreme loading, such as earthquakes and storms. Decisions must be made as soon as possible, whether to allow re-occupation of such buildings, or to assess them for further damage. The time required to reach such decisions is cost-critical, both for the building owner or manager and for the agency doing the assessment. Peak inter-storey drift ratio and detection of permanent damage are some of the damage assessment parameters recommended by assessment agencies. Traditionally, accelerometers have been used to monitor these parameters. Accelerometers measure accelerations which are double-integrated to get displacements. These double integrated displacements are then used for computing the inter-storey drift ratios and locating permanent damage. Displacements obtained by double-integration and inter-storey drift ratios by subtraction of these displacements, are often erroneous and unreliable and direct measurement of displacement is preferred. Direct measurement of displacement is required at a number of points along the height of the building. For example, for computing inter-storey drift ratios, measurements of displacement at both the floor level and roof level are required. Such points on buildings and other engineering structures of vertical profile are termed as mid-height points in this thesis. While GPS has been used for deformation monitoring of engineering structures and to assist in damage assessment during and after extreme loading events, its use has been limited to roof top installations. / This research is an attempt to measure displacements at mid-height locations of engineering structures of vertical profile using GPS. (For complete abstract open document).