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Doctor of Philosophy / Department of Statistics / James W. Neill / Checking the adequacy of a proposed parametric nonlinear regression model is important in order to obtain useful predictions and reliable parameter inferences. Lack of fit is said to exist when the regression function does not adequately describe the mean of the response vector. This dissertation considers asymptotics, implementation and a comparative performance for the likelihood ratio tests suggested by Neill and Miller (2003). These tests use constructed alternative models determined by decomposing the lack of fit space according to clusterings of the observations. Clusterings are selected by a maximum power strategy and a sequence of statistical experiments is developed in the sense of Le Cam. L2 differentiability of the parametric array of probability measures associated with the sequence of experiments is established in this dissertation, leading to local asymptotic normality. Utilizing contiguity, the limit noncentral chi-square distribution under local parameter alternatives is then derived. For implementation purposes, standard linear model projection algorithms are used to approximate the likelihood ratio tests, after using the convexity of a class of fuzzy clusterings to form a smooth alternative model which is necessarily used to approximate the corresponding maximum optimal statistical experiment. It is demonstrated empirically that good power can result by allowing cluster selection to vary according to different points along the expectation surface of the proposed nonlinear regression model. However, in some cases, a single maximum clustering suffices, leading to the development of a Bonferroni adjusted multiple testing procedure. In addition, the maximin clustering based likelihood ratio tests were observed to possess markedly better simulated power than the generalized likelihood ratio test with semiparametric alternative model presented by Ciprian and Ruppert (2004).

The content of this dissertation is divided into two main topics: 1) nonlinear profile monitoring and 2) an improved approximate distribution for the T² statistic based on the successive differences covariance matrix estimator. Part 1: Nonlinear Profile Monitoring In an increasing number of cases the quality of a product or process cannot adequately be represented by the distribution of a univariate quality variable or the multivariate distribution of a vector of quality variables. Rather, a series of measurements are taken across some continuum, such as time or space, to create a profile. The profile determines the product quality at that sampling period. We propose Phase I methods to analyze profiles in a baseline dataset where the profiles can be modeled through either a parametric nonlinear regression function or a nonparametric regression function. We illustrate our methods using data from Walker and Wright (2002) and from dose-response data from DuPont Crop Protection. Part 2: Approximate Distribution of T² Although the T² statistic based on the successive differences estimator has been shown to be effective in detecting a shift in the mean vector (Sullivan and Woodall (1996) and Vargas (2003)), the exact distribution of this statistic is unknown. An accurate upper control limit (UCL) for the T² chart based on this statistic depends on knowing its distribution. Two approximate distributions have been proposed in the literature. We demonstrate the inadequacy of these two approximations and derive useful properties of this statistic. We give an improved approximate distribution and recommendations for its use. / Ph. D.

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This thesis is aimed to Design of Experiments methodology. Main purpose of this thesis is to create detailed materials for lessons of Design of Experiments in Quality Control courses. Thesis contains case studies which are applicable for education purposes. Design of Experiments has been applied for solder joints quality evaluation. Solder joints have been modeled in software ANSYS and finite element method has been applied for thermomechanical stress evaluation.