Inconel 718 is a nickel-based superalloy with a series of superior properties, such as high strength, creep-resistance, and corrosion-resistance. Additive manufacturing (AM) is appealing to Inconel 718 because of its near-net-shape production capability to circumvent poor machinability. However, AM parts are prone to detrimental porosity, reducing their fatigue resistance. Thus, further understanding of AM fatigue behavior is required before widespread industrial use. The microstructural and fatigue properties of heat treated AM Inconel 718, produced using Laser Engineered Net Shaping (LENSTM), are evaluated at room and elevated temperatures. Fully reversed, strain-controlled fatigue tests were performed on cylindrical specimens at strain amplitudes of 0.001 to 0.01 mm/mm. Fracture surfaces were inspected using a scanning electron microscope (SEM). Heat treatment caused initial dendritic microstructure to mostly reorm into an equiaxed grain structure. AM specimens experienced reduced fatigue life in testing as compared to wrought material due to inclusions or pores near the surface

This study experimentally quantified the structure-property relations with respect to fatigue of an extruded AZ61 magnesium alloy and captured the behavior with a microstructure-sensitive MultiStage Fatigue Model. Experiments were conducted in the extruded and transverse directions under low and high cycle strain control fatigue conditions. The cyclic behavior of this alloy displayed varying degrees of cyclic hardening depending on the strain amplitude and the specimen orientation. The fracture surfaces of the fatigued specimens were analyzed using a scanning electron microscope in order to quantify structure-property relations with respect to microstructural features. Correlations between particle size, nearest neighbor distance, and grain size as a function of failure cycles were quantified. Finally, a multistage fatigue model based on the structure-property relations quantified in this study was employed to capture the anisotropic fatigue damage of the AZ61 magnesium alloy.

A need exists for a more robust method of evaluating musculoskeletal injuries resulting from impact conditions, particularly blasts. Computational modeling is a promising method of achieving this goal. The accuracy of a model depends on high quality mechanical properties for each component. This study examined the mechanical properties of porcine muscle along with structure property relationships. Fresh muscle was tested in compression and tension at strain rates of 0.1 s-1, 0.01 s-1, and 0.001 s-1. Viscoelastic properties were observed including strain rate dependency, stress state dependency, anisotropy, relaxation, and hysteresis. Image analysis was conducted in compression on controls, 30% strain, and 50% strain, relating stress-strain data with structural changes. The effect of rigor was also seen in the tensile response of muscle. Thawed tissue was examined to investigate the effects of freezing. It was found that freezing did not significantly change the mechanical properties, but substantial microstructural changes did occur.

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AA7075 is a precipitation hardening structural aluminum alloy, which has garnered considerable interest in automotive industry, primarily due its lightweighting capacity compared to many other aluminum alloys from 2xxx and 6xxx series. However, the damage evolution in AA7075 is quite complex due to the presence of different second phase particles in the microstructure and their contribution on damage evolution is largely unknown at large plastic strains. The common second phase particles are η precipitates, θ precipitates and Fe-rich intermetallic particles. The current work presents an extensive multiscale numerical framework, which in conjunction with complementary experiments, is applied to study strain localization, void nucleation, growth, and coalescence in a particle rich matrix. Experimentally, void nucleation is observed to be driven by particle decohesion and particle fracture. Nanoscale molecular dynamics (MD) simulation is carried out to estimate interface properties of the three distinct particle types. The extracted properties are used as input for real particle field 2D and 3D microstructure based finite element (FE) models. The stochastic nature of particle fracture is described using a Weibull distribution, while the effect of grains is incorporated in terms of their Taylor factors. Ductile matrix is described using the well known Gurson Tvergaard Needleman (GTN) void damage model. Complementary experiments included uniaxial tensile tests carried out in-situ in Scanning Electron Microscope (SEM) and X-ray Computed Tomography (XCT), ex-situ high resolution XCT and Electron Back Scattered Diffraction (EBSD) tests. The FE models with three distinct particle stoichiometries and three competing damage mechanisms, show good agreement with experimental observations. Particle fracture marginally dominates particle decohesion. At low plastic strains, void nucleation is initiated by decohesion and fracture of larger Fe-rich particles, which facilitate formation of localized deformation bands. At large plastic strain, elevated stresses within the localized bands facilitate decohesion and fracture of more resistant η and θ precipitates. Due to their inherent larger size and more irregular morphology, θ precipitates contribute to voiding more than η precipitates. Under uniaxial tensile loads, void growth takes place in the middle of the specimen, driven by higher triaxiality stress state in the middle, relative to the surface. Void coalescence occurs along deformation bands driven by higher stresses due accumulated plastic strain within the bands, in a process known as void sheeting. / Thesis / Doctor of Philosophy (PhD)

In 1998, the United States National Committee on Biomechanics (USNCB) established an evolving discipline called Functional Tissue Engineering (FTE). In establishing this discipline, the goals of the USNCB were to advance FTE by increasing awareness among tissue engineers about the importance of restoring function when engineering tissue constructs. Another goal was to encourage tissue engineers to incorporate these functional criteria in the design, manufacturing and optimization of tissue engineered constructs. Based on this motivation, an investigation of the structure and mechanical properties of the rabbit patellar tendon will be executed, with the ultimate goal of creating a multiscale soft tissue model based on internal state variable (ISV) theory. Many continuum scale models, mostly phenomenological and microstrucutral, have been created to contribute to the understanding of the complex functional properties of the tendon, such as its anisotropy, inhomogeneity, nonlinearity, and viscoelasticity. However, none of these models have represented the mechanical behavior of the tendon in the presence of internal structural change on a multiscale level. The development of a multiscale ISV model will allow the capture of the irreversible, path history dependent aspects of the material behavior. The objective of this study is to contribute to the multiscale ISV model development by quantifying the structure- property relations. In particular, the fibril distribution at the microstructural level and the resultant multiaxial stress states (longitudinal and transverse compression and longitudinal tension) will be examined).

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