Recent advances in metamaterials research has enabled the development of highly sensitive near-field microwave sensors with unprecedented sensitivity. In this work, we take advantage of the increase in the sensitivity to produce a compact, lightweight, affordable, and accurate measurement system for the applications of microwave imaging and material characterization. This sensitivity enhancement due to the inclusion of metamaterials opens the door for the use of inexpensive microwave components and circuits such as direct detectors while leveraging the high sensitivity of the metamaterial probe to deliver an overall accurate measurement system comparable to that of a traditional probe used in conjunction with a vector network analyzer. The sensor developed is composed of a metamaterial sensor with an RF direct detection circuit. In this work, two prototype measurement systems have been designed and tested. Measurement of small cracks in conductors and material characterization using the proposed system were performed. The results from the newly developed sensors were compared with the results from vector network analyzer measurements. Good agreement was obtained. The feasibility of a compact, lightweight, affordable, and accurate system has been demonstrated by using the developed prototypes.

The ultrasonic nondestructive technique is mainly used to evaluate interior defect, material properties and outside dimensions by measuring the transmitting and reflecting sound waves. Generally, the evaluation of the ultrasonic testing depends on the amplitudes and delay time of the received signals; however, this research is focused on the analysis of the phase differences of the received signals. The leakage phenomenon of surface waves propagating at the liquid-solid interface has been studied for more than fifty years. The main characteristic of this phenomenon is the 180-degree phase difference between the reflected and leaky ultrasound when a bounded ultrasonic beam is incidented. And the null zone caused by the interference of these two waves is appearing in the reflected field. The phase difference is changed as the surface condition altered, including surface roughness and layered structures. The normal-mode theory is used at this research to analyze the analytical model of the leaky surface wave in thin layered structures. In experiments, the measurements of the reflected field are proceeded by the scanning system, so as to analyze the phase difference between the reflected and leaky ultrasound and calculate the layer thickness by the phase difference. As a result of the surface roughness of the thin layers, the leakage is more serious when the ultrasound propagates with lower frequency. For the consideration of locating the null-zone in the reflected field, this research prefers using lower frequency as an initial frequency at the beginning of the testing, then increasing the frequency to achieve a better sensitive of the thickness.

Nickel-base superalloys obtain high temperature mechanical properties through formation of precipitate phases formed via heat treatment. The precipitate microstructure evolves with heat treatment or thermal exposure, which can lead to degrading mechanical properties. This project focuses on the use of electrical resistivity as a non-destructive testing method to monitor the precipitate phase in Waspaloy (a polycrystalline nickel-base superalloy). The evolution of the precipitate microstructure is characterized throughout the volume of the specimens using both small angle neutron scattering (SANS) and ultra small angle X-ray scattering (USAXS) measurements. These measurements are also aided by microscopy and X-ray diffraction measurements.

Structural health monitoring (SHM) is an active research area devoted to the assessment of the structural integrity of critical components of aerospace, civil and mechanical systems. Guided wave methods have been proposed for SHM of plate-like structures using permanently attached piezoelectric transducers, which generate and sense waves to evaluate the presence of damage. Effective interrogation of structural health is often facilitated by sensors and actuators with the ability to perform directional scanning. In this research, the novel class of Frequency Steerable Acoustic Transducers (FSATs) is proposed for directional generation/sensing of guided waves. The FSATs are characterized by a spatial arrangement of the piezoelectric material which leads to frequency-dependent directionality. The resulting FSATs can be employed both for directional sensing and generation of guided waves, without relying on phasing and control of a large number of channels. Because there is no need for individual control of transducer elements, hardware and power requirements are drastically reduced so that cost and hardware limitations of traditional phased arrays can be partially overcome. The FSATs can be also good candidates for remote sensing and actuation applications, due to their hardware simplicity and robustness. Validation of the proposed concepts first employs numerical methods. Next, the prototyping of the FSATs allows an experimental investigation confirming the analytical and numerical predictions. Imaging algorithm based on frequency warping is also proposed to enhance results representation.

This research seeks to expand the role of variational and adjoint processing methods into segments of the sonar, radar, and nondestructive testing communities where they have not yet been widely introduced. First, synthetic aperture reconstruction is expressed in terms of the adjoint operator. Many, if not all, practical imaging modalities can be traced back to this general result, as the adjoint is the foundation for backprojection-type algorithms. Next, active surfaces are developed in the context of the Helmholtz equation for the cases of opaque scatterers (i.e., with no interior field) embedded in free space, and penetrable scatterers embedded in a volume which may be bounded. The latter are demonstrated numerically using closed-form solutions based on spherical harmonics. The former case was chosen as the basis for a laboratory experiment using Lamb waves in an aluminum plate. Lamb wave propagation in plates is accurately described by the Helmholtz equation, where the field quantity is the displacement potential. However, the boundary conditions associated with the displacement potential formulation of Lamb waves are incompatible with the shape gradient derived for the Helmholtz equation, except for very long or very short wavelengths. Lastly, optical flow is used to solve a new and unique problem in the field of synthetic aperture sonar. Areas of acoustic focusing and dilution attributable to refraction can sometimes resemble the natural bathymetry of the ocean floor. The difference is often visually indistinguishable, so it is desirable to have a means of detecting these transient refractive effects without having to repeat the survey. Optical flow proved to be effective for this purpose, and it is shown that the parameters used to control the algorithm can be linked to known properties of the data collection and scattering physics.

Alkali-silica reaction (ASR) and delayed ettringite formation (DEF) are expansive reactions that can lead to the premature deterioration of concrete structures. Both have been implicated in the deterioration of numerous structures around the world, including many transportation structures in Texas. As a result of considerable research advances, ASR and DEF are now avoidable in new construction, but evaluating and managing the existing stock of structures damaged by these mechanisms remains a challenge. While the published guidance for evaluating structures is very effective at diagnosing the presence of ASR and DEF, there remain significant weaknesses with respect to the evaluation of structural safety and serviceability and nondestructive testing (NDT) is a minor component of the evaluation process. The research described in this dissertation involved a wide range of tests on plain and reinforced concrete at multiple scales. This included small cylinders and prisms, larger plain and reinforced concrete specimens in outdoor exposure, full-scale reinforced concrete beams, and core samples from the outdoor exposure specimens and full-scale reinforced concrete beams. Nondestructive test methods were applied at all scales, and the full-scale beams were also tested in four-point flexure to determine the effects of ASR and DEF on flexural strength and serviceability. Severe expansions from ASR and DEF did not reduce the strength of the full-scale beams or result in excessive deflections under live loads, despite significant decreases in the compressive strength and elastic modulus measured from core samples. Most NDT methods were found to be effective at low expansions but had difficulty correlating to larger expansions. Two promising NDT methods have been identified for future research and development, and guidance regarding existing test methods is offered. / text

Quick mass production of homogeneous thin film material is required in paper, plastic, fabric, and thin film industries. Due to the high feed rates and small thicknesses, machine vision and other nondestructive evaluation techniques are used to ensure consistent, defect-free material by continuously assessing post-production quality. One of the fastest growing inspection areas is for 0.5-500 micrometer thick thin films, which are used for semiconductor wafers, amorphous photovoltaics, optical films, plastics, and organic and inorganic membranes. As a demonstration application, a prototype roll-feed imaging system has been designed to inspect high-temperature polymer electrolyte membrane (PEM), used for fuel cells, after being die cast onto a moving transparent substrate. The inspection system continuously detects thin film defects and classifies them with a neural network into categories of holes, bubbles, thinning, and gels, with a 1.2% false alarm rate, 7.1% escape rate, and classification accuracy of 96.1%. In slot die casting processes, defect types are indicative of a misbalance in the mass flow rate and web speed; so, based on the classified defects, the inspection system informs the operator of corrective adjustments to these manufacturing parameters. Thickness uniformity is also critical to membrane functionality, so a real-time, full-field transmission densitometer has been created to measure the bi-directional thickness profile of the semi-transparent PEM between 25-400 micrometers. The local thickness of the 75 mm x 100 mm imaged area is determined by converting the optical density of the sample to thickness with the Beer-Lambert law. The PEM extinction coefficient is determined to be 1.4 D/mm and the average thickness error is found to be 4.7%. Finally, the defect inspection and thickness profilometry systems are compiled into a specially-designed graphical user interface for intuitive real-time operation and visualization.

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Recent advances in metamaterials research has enabled the development of highly sensitive near-field microwave sensors with unprecedented sensitivity. In this work, we take advantage of the increase in the sensitivity to produce a compact, lightweight, affordable, and accurate measurement system for the applications of microwave imaging and material characterization. This sensitivity enhancement due to the inclusion of metamaterials opens the door for the use of inexpensive microwave components and circuits such as direct detectors while leveraging the high sensitivity of the metamaterial probe to deliver an overall accurate measurement system comparable to that of a traditional probe used in conjunction with a vector network analyzer. The sensor developed is composed of a metamaterial sensor with an RF direct detection circuit. In this work, two prototype measurement systems have been designed and tested. Measurement of small cracks in conductors and material characterization using the proposed system were performed. The results from the newly developed sensors were compared with the results from vector network analyzer measurements. Good agreement was obtained. The feasibility of a compact, lightweight, affordable, and accurate system has been demonstrated by using the developed prototypes.

Following Carslaw [1] and as discussed by Becker et al [2], the diffusion of ultrasonic energy in cement-based aggregates follow the heat diffusion equation. However, due to the finite size of the discs used in experiments by Becker, ultrasound energy is contained within the body for a longer period of time, as compared to [2]. Though the energy content of the disc in reality would eventually decay to zero, due to leaks and other mechanisms, a theoretical study of perfectly adiabatic case is useful to compare the residual energy values to material properties. As a particular example, the input energy sees multiple phenomena inside the material during propagation. The residual energy is this a combined effect of the multiple scattering, dissipative and diffusive processes. This objective of this thesis is to study the relationship between the residual spectral density and specimen geometry. The effort further aims to attribute the difference in the residual spectral energy density values in materials of similar geometry to the varying material properties of the heterogeneous materials. Finally, a study of the error propagation in the estimation is presented, along-with an analytical relationship showing the value of spectral energy density for discs of finite radius and height. Ref: 1. H. S. Carslaw, J.C.J., Conduction of Heat in Solids. 2nd ed ed. 1986: Oxford University Press, USA. 520 2. Becker, J., L.J. Jacobs, and J. Qu, Characterization of cement-based materials using diffuse ultrasound. Journal of Engineering Mechanics, 2003. 129(12): p. 1478-1484.