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: Extraction of β-carotene from orange peel and carrot waste for cotton dyeingHECKER, SUSAN January 2014 (has links)
The further usage of vegetable and plant waste from juice pressing industry as textile dyes is presented in this thesis. The thesis is focused on β-carotene (C40H56) dyestuff extracted from orange peel and carrot residue. The three organic solvents; ethyl acetate, petroleum ether and hexane/acetone (1:1 v/v) were used for the extraction. The analysis of the extract was done by RP-HPLC with a C18 column. The yield and the purity of the extracted β-carotene were determined. The highest yield was achieved with petroleum ether whereas the other two solvents were nearly as good. The highest and purest amount on β-carotene was found in the extracts of carrots. The dyeing process was continued with β-carotene dyestuff of orange peel and carrot residue extracted from 27 g of residue on 0,8 g cotton in the dyeing ratio 1:50. Unmordant and post mordanted bleached and mercerized cotton fabric was dyed. 10% alum of the weight fraction of cotton was used as mordant. Colour measurements (K/S, C*, L*, a*, b*, h and ΔE) and fastness properties as light- (ISO-Norm B02) and wash fastness (ISO 105 – C) were tested. Fair light fastness grades were achieved by β-carotene dyestuff of orange peel residue dyed on cotton fabric. Poorer were the grades for β-carotene dyestuff of carrot residue for both unmordanted and mordanted samples. The wash fastness couldn’t achieve reasonable results neither for β-carotene dyestuff from carrots nor orange peel residue, dyed on cotton fabric. / Program: Master programme in Textile Engineering
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