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111	Reverberation Chamber Modeling Using Finite-Difference Time-Domain Method Petit, Frédéric 12 1900 (has links) Since the last few years, the unprecedented growth of communication systems involving the propagation of electromagnetic waves is particularly due to developments in mobile phone technology. The reverberation chamber is a reliable bench-test, enabling the study of the effects of electromagnetic waves on a specific electronic appliance. However, the operating of a reverberation chamber being rather complicated, development of numerical models are of utmost importance to determine the crucial parameters to be considered.This thesis consists in the modelling and the simulation of the operating principles of a reverberation chamber by means of the Finite-Difference Time-Domain method. After a brief study based on field and power measurements performed in a reverberation chamber, the second chapter deals with the different problems encountered during the modelling. The consideration of losses being a very important factor in the operating of the chamber, two methods of implementation of these losses are set out in this chapter. Chapter~3 consists in the analysis of the influence of the stirrer on the first eigenmodes of the chamber; the latter modes can undergo a frequency shift of several MHz. Chapter~4 shows a comparison of results issued from high frequency simulations and theoretical statistical results. The problem of an object placed in the chamber, resulting in a field disturbance is also tackled. Finally, in the fifth chapter, a comparison of statistical results for stirrers having different shapes is set out. reverberation chamber mode-stirred chamber Modeling numerical method FDTD finite difference time domain stirrer numerical error non-uniform mesh FFT modes overlapping frequency shift eigen mode eigen frequency mode density quality factor losses modal study statistical study statistical test statistical criterion correlation angle Chi2 law Rayleigh low Gauss law PDF CDF QC T1
112	Development of High-throughput Membrane Filtration Techniques for Biological and Environmental Applications / Development of High-throughput Membrane Filtration Techniques Kazemi, Amir Sadegh 11 1900 (has links) Membrane filtration processes are widely utilized across different industrial sectors for biological and environmental separations. Examples of the former are sterile filtration and protein fractionation via microfiltration (MF) and ultrafiltration (UF) while drinking water treatment, tertiary treatment of wastewater, water reuse and desalination via MF, UF, nanofiltration (NF) and reverse-osmosis (RO) are examples of the latter. A common misconception is that the performance of membrane separation is solely dependent on the membrane pore size, whereas a multitude of parameters including solution conditions, solute concentration, presence of specific ions, hydrodynamic conditions, membrane structure and surface properties can significantly influence the separation performance and the membrane’s fouling propensity. The conventional approach for studying filtration performance is to use a single lab- or pilot-scale module and perform numerous experiments in a sequential manner which is both time-consuming and requires large amounts of material. Alternatively, high-throughput (HT) techniques, defined as the miniaturized version of conventional unit operations which allow for multiple experiments to be run in parallel and require a small amount of sample, can be employed. There is a growing interest in the use of HT techniques to speed up the testing and optimization of membrane-based separations. In this work, different HT screening approaches are developed and utilized for the evaluation and optimization of filtration performance using flat-sheet and hollow-fiber (HF) membranes used in biological and environmental separations. The effects of various process factors were evaluated on the separation of different biomolecules by combining a HT filtration method using flat-sheet UF membranes and design-of-experiments methods. Additionally, a novel HT platform was introduced for multi-modal (constant transmembrane pressure vs. constant flux) testing of flat-sheet membranes used in bio-separations. Furthermore, the first-ever HT modules for parallel testing of HF membranes were developed for rapid fouling tests as well as extended filtration evaluation experiments. The usefulness of the modules was demonstrated by evaluating the filtration performance of different foulants under various operating conditions as well as running surface modification experiments. The techniques described herein can be employed for rapid determination of the optimal combination of conditions that result in the best filtration performance for different membrane separation applications and thus eliminate the need to perform numerous conventional lab-scale tests. Overall, more than 250 filtration tests and 350 hydraulic permeability measurements were performed and analyzed using the HT platforms developed in this thesis. / Thesis / Doctor of Philosophy (PhD) / Membrane filtration is widely used as a key separation process in different industries. For example, microfiltration (MF) and ultrafiltration (UF) are used for sterilization and purification of bio-products. Furthermore, MF, UF and reverse-osmosis (RO) are used for drinking water and wastewater treatment. A common misconception is that membrane filtration is a process solely based on the pore size of the membrane whereas numerous factors can significantly affect the performance. Conventionally, a large number of lab- or full-scale experiments are performed to find the optimum operating conditions for each filtration process. High-throughput (HT) techniques are powerful methods to accelerate the pace of process optimization—they allow for multiple experiments to be run in parallel and require smaller amounts of sample. This thesis focuses on the development of different HT techniques that require a minimal amount of sample for parallel testing and optimization of membrane filtration processes with applications in environmental and biological separations. The introduced techniques can reduce the amount of sample used in each test between 10-50 times and accelerate process development and optimization by running parallel tests. Membrane filtration Ultrafiltration Downstream bio-processing High-throughput (HT) testing Wastewater treatment Hollow-fiber membranes Humic acids High-throughput filtration Design-of-experiments (DOE) Process optimization Microscale filtration Microfluidic flow control system Stirred well filtration SWF High-throughput hollow-fiber module HT-HF Constant TMP Constant flux Multi-modal filtration Bioseparation MMFC MS-PS-CFF PEG Dextran FITC-Dextran BSA DNA IgG α-lactalbumin Biomolecule separation Module hydrodynamics Concentration polarization Membrane fouling Micromixing Omega™ membrane Microscale processing Fouling test PVDF membrane Surface modification Polydopamine Membrane cleaning Membrane backwashing Sodium alginate Polyethersulfone PES Hydraulic permeability Membrane permeability ZeeWeed® membrane Filtration ionic strength Filtration pH Solution conditions Water treatment Environmental separations Biological separations

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Reverberation Chamber Modeling Using Finite-Difference Time-Domain Method

Development of High-throughput Membrane Filtration Techniques for Biological and Environmental Applications / Development of High-throughput Membrane Filtration Techniques