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Surface Acoustic Wave (SAW) devices are manufactured using standard metallization and photolithographic techniques that have been established by the semiconductor industry. The facilities in the newly developed Microelectronics laboratory at the University of Central Florida will be utilized in the fabrication of a SAW device. This thesis will outline the complete procedure beginning with the initial design from given specifications, up to mask generation, fabricating and testing of the device. This will serve to calibrate the fabrication process for future work in SAW device and semiconductor fabrication. The models that are used in the SAWCAD design software will be verified by comparing the theoretical and experimental results.

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Mémoire numérisé par la Direction des bibliothèques de l'Université de Montréal.

At the molecular level the entropic “hydrophobic effect” is responsible for high interfacial energies between hydrophobic solids and aqueous liquids, the low solubility of apolar solutes in aqueous solvents, and self-assembly in biological processes, such as vesicle formation and protein folding. Although it is known that a strong attraction between apolar molecules exists at the molecular level, it is not clear how this force scales up to objects with dimensions in the range 100 nm–1 m. This work sets out to measure the forces between particles with a radius of about 10 µm. Because we can only measure the total force, which includes the van der Waals force and the electrostatic forces, it is important to isolate the effect of “hydrophobicity”. We do this by measuring for systems where the particles are very hydrophobic (water contact angle, θ ~110°) and the van der Waals and electrostatic forces are very small. Under these conditions we find that the total force is very small: it is similar to the van der Waals force at separations exceeding 5 nm. Many early works on the hydrophobic force reported surface force at over 100 nm of separation. However, many of these strong, long-ranged attractive forces are likely caused by submicron interfacial bubbles, known as nanobubbles. Nanobubbles were imaged with an atomic force microscope to better understand their stability and dependence on solution properties, such as initial concentration of dissolved gas and changes in gas concentration. We found that nanobubbles still formed in degassed solutions and that lowering the dissolved gas concentration did not reduce the bubble size, implying that nanobubbles do not form from dissolved gas in the liquid phase or do not contain gas and are instead water vapor. Furthermore, addition of an oxygen scavenger agent, sodium sulfite, to a liquid phase that had been pressured with oxygen did not reduce bubble size which could be evidence that nanobubbles are impermeable to gas diffusion across the gas liquid interface, do not form from the dissolved gas in the surrounding liquid, or do not contain gas and are instead water vapor. / Ph. D.

A modular simulation model of a marine powertrain consisting of a prime mover, propeller shaft, propulsor, and control system was developed, tested, and used to demonstrate the ability to analyze the marine powertrain numerically. The modularity of the model allows for the user to easily substitute different or more advanced modules, or add additional modules to obtain a greater level of detail or simulate more complex interactions of systems with the marine powertrain. Current and historical trends indicate an interest in all electric ship design, and the use of surface piercing propellers for small craft. Due to the availability of towing tank data from a surface piercing propeller, an all electric prime mover module, surface piercing propeller module, propeller shaft module, and PID control module were coded, integrated, and operated, simulating a complete powertrain. Simulations were conducted using full-scale real-world conditions to demonstrate the model functionality and level of detail. Simulation results provided insight into the vibrational excitation, stability, and control of such a powertrain. / Master of Science

Yes / The prevalence of micromoulded components has steadily increased over recent years. The production of such components is extremely sensitive to a number of variables that may potentially lead to significant changes in the surface geometry, often regarded as a crucial determinant of the product¿s functionality and quality. So far, traditional large-scale quality assessment techniques have been used in micromoulding. However, these techniques are not entirely suitable for small scales . Techniques such as Atomic Force Mi- croscopy (AFM) or White Light Interferometry (WLI) have been used for obtaining full three-dimensional profiles of micromoulded components, pro- ducing large data sets that are very difficult to manage. This work presents a method of characterizing surface features of micro and nano scale based on the use of the Biharmonic equation as means of describing surface profiles whilst guaranteeing tangential (C1) continuity. Thus, the problem of rep- resenting surface features of micromoulded components from massive point clouds is transformed into a boundary-value problem, reducing the amount of data required to describe any given surface feature.The boundary conditions needed for finding a particular solution to the Biharmonic equation are extracted from the data set and the coefficients associated with a suitable analytic solution are used to describe key design parameters or geometric properties of a surface feature. Moreover, the expressions found for describ- ing key design parameters in terms of the analytic solution to the Biharmonic equation may lead to a more suitable quality assessment technique for mi- cromoulding than the criteria currently used. In summary this technique provides a means for compressing point clouds representing surface features whilst providing an analytic description of such features. The work is applicable to many other instances where surface topography is in need of efficient representation.

Recent progress in layered transition metal dichalcogenides (TMDs) has led to various promising electronic and optoelectronic applications. However, the structure of materials plays a critical role in electronic and optoelectronic devices, and determines performance. Electronic and optoelectronic devices typically consist of multiple layers that form electrical homojunctions or heterojunctions. Therefore, in a device it can be expected that a WS2 layer may serve as the substrate for a subsequent layer in a multilayer device stack and determine how the layer grows. In transistor structures, roughness at the channel/gate dielectric interface introduces field variations and charge scattering. Therefore, understanding the relations between processing, surface morphology and properties is important. In this project, the effects of pulsed laser deposition (PLD) processing conditions on the surface morphology of few layered WS2 films were studied. WS2 films were synthesized under processing conditions that represent the extremes of surface supersaturation and kinetic energy transfer from the flux to the growing films, and evolution of the surface morphology was studied. The specific conditions were 1Hz/50mJ, 10Hz/50mJ, 1Hz/300mJ, and 10Hz/300mJ respectively. Combining AFM, XRD and Raman analyses, it was determined that deposition at 10Hz/300mJ, provided the best structural properties and surface morphology. Growth appeared to be 3D-cluster, and was governed by supersaturation rather than by surface diffusion processes. No clear correlation between mobility and surface roughness was found. Hall measurements and XPS data show the highest mobility was obtained with the highest S/W ratio, indicating that point defect scattering rather than scattering from surface roughness was dominant.

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