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The Determination of Mechanical Properties of Biomedical MaterialsChien, Hui-Lung 29 August 2012 (has links)
The mechanical properties of biomedical materials were determined and discussed in this study. The extension and tensile tests for aorta and coronary artery were carried out using tensile testing machine. Based on incompressibility of biological soft tissue, the stress-stretch curves of arteries were obtained. This study proposed a nonlinear Ogden material model for the numerical simulation of coronary artery extension during stent implantation. The corresponding Ogden model parameters were derived by the obtained stress-stretch curves from tensile tests. For validation, the proposed nonlinear Ogden material model for coronary artery was applied to a Palmaz type stent implantation process. The simulated stent deformation was found to be reasonable. It had a good correlation with the measured results.
The microindentation experiments were used to measure the mechanical properties of enamel and dentine of human teeth in this study. To reveal the relation between the experimental parameters and measured mechanical properties, Young¡¦s moduli were investigated by varying experimental parameters. The parameter of maximum indentation load significantly influences measured values. Young¡¦s modulus varies very slightly when 10 to 100 mN of maximum indentation load applied. Young¡¦s modulus is not sensitive to the parameters of portion of unloading data and teeth age.
The combination of finite element analysis and curve-fitting method is proposed to determine the mechanical properties of thin film deposited on substrate. The mechanical properties of thin film, i.e. Young¡¦s modulus, yield strength and strain-hardening exponent, were extracted by applying an iterative curve-fitting scheme to the experimental and simulated force-indentation depth curves during the microindentation loading and unloading processes. The variation of mechanical properties of TiN thin films with thicknesses ranging from 0.2 to 1.4 £gm was extracted. The results presented the film thickness effect makes the Young¡¦s modulus of TiN thin films reduces with reducing film thickness, particularly at thicknesses less than 0.8 £gm. Therefore, it can be inferred that a film thickness of 0.8 £gm possibly represents the upper bound when employing macroscopic mechanics with bulk material properties.
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Mechanical properties of PVDF/MWCNT fibers prepared by flat/cylindrical near-field electrospinningKe, Chien-An 04 September 2012 (has links)
This study presents near-field electrospinning (NFES) on flat and hollow cylindrical process to fabricate permanent piezoelectricity of polyvinylidene fluoride (PVDF)/ multi-walled carbon nanotube (MWCNT) piezoelectric nanofibers. Then the mechanical properties of fibers were measured. PVDF is a potential piezoelectric polymer material combining desirable mechanical, thermal, electrical properties with excellent chemical resistance. The existing researches mostly focused on piezoelectric thin film process. However, the research of characteristic about piezoelectric fiber is little. The methods of measurement of the mechanical properties (Young¡¦s modulus, hardness, and tensile strength¡Belongation) of the electrospun PVDF/MWCN composite nanofiber were carried out by using nano-indention test (MTS Nanoindenter Windows XP System) and tensile test (Microforce Testing System). By setting electric field (1¡Ñ107 V/m), rotating velocity (900 rpm) of the hollow cylindrical glass tube on a motion X-Y stage (2 mm/sec) and PVDF solution concentration (16 wt%), and MWCNT (0.03 wt%), in-situ electric poling, mechanical stretching and morphology of PVDF nanofiber were demonstrated. After the experiments of nano-indention test and tensile strength test, it is suggested that the good mechanical properties in NFES on cylindrical process. The results show that the mechanical properties of composite nanofiber are better than the conventional NFES process. The Young¡¦s modulus of 16% PVDF fiber prepared by cylindrical process is 0.89 GPa and hardness is 26.5 MPa. The mechanical properties were increased 56.2% and 49.4% after adding 0.03% of MWCNT, corresponding to 1.39 GPa and 39.6 MPa. The tensile strength was increased 32.7% and elongation at breaking point was increased 35% after adding 0.03% MWCNT.
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Porous ß-type Ti-Nb alloy for biomedical applicationsZhuravleva, Ksenia 17 July 2014 (has links) (PDF)
One of the most important factors for a successful performance of a load-bearing implant for hard tissue replacement is its mechanical compatibility with human bone. That implies that the stiffness should be close to that of a bone and the strength of the implant material must be high enough to bear the load applied under physiological conditions. The Young´s modulus of most of the commonly used biomedical alloys is larger than that of a human bone (around 100 GPa for cp Ti, 112 GPa for Ti-6Al-4V versus 10-30 GPa for cortical human bone). A stiffness reduction of Ti alloys can be achieved by two approaches: (i) selecting an alloy composition with low Young´s modulus i.e. a ß-type alloy and (ii) introducing a reasonable amount of porosity. The composition of Ti-40Nb was chosen for the present work, as it allows to stabilize a single ß-type phase with low Young´s modulus at room temperature.
The samples were produced by a powder metallurgical approach. The Ti-40Nb alloy powder was obtained by ball-milling of elemental Ti and Nb powders. The influence of the milling parameters on the oxygen content in the milled powder was studied. Powders with a lowest oxygen content of 0.4 wt.-% had an almost single ß-type phase after heat treatment and quenching.
Porous samples were produced by loose powder sintering, hot-pressing and sintering with NaCl as a space-holder. The influence of the different processing routes and different porosities on the mechanical properties of the alloy was studied. The samples produced by loose powder sintering had mechanical properties close to those of cortical human bone (Young´s modulus 20 GPa, compression strength 150 MPa) and the samples produced by loose sintering with space-holder materials had mechanical properties close to those of human spongy bone (Young´s modulus 0.2-2 GPa, compression strength 50 MPa). Porous Ti-40Nb samples were coated with bone-like hydroxyapatite by an electrochemical deposition method in order to improve the osseointegration of the samples with bone tissue. The experiments were carried out with samples produced by different routes and a correlation between the deposition parameters and the morphology of the hydroxyapatite needles was found.
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Porous ß-type Ti-Nb alloy for biomedical applicationsZhuravleva, Ksenia 20 June 2014 (has links)
One of the most important factors for a successful performance of a load-bearing implant for hard tissue replacement is its mechanical compatibility with human bone. That implies that the stiffness should be close to that of a bone and the strength of the implant material must be high enough to bear the load applied under physiological conditions. The Young´s modulus of most of the commonly used biomedical alloys is larger than that of a human bone (around 100 GPa for cp Ti, 112 GPa for Ti-6Al-4V versus 10-30 GPa for cortical human bone). A stiffness reduction of Ti alloys can be achieved by two approaches: (i) selecting an alloy composition with low Young´s modulus i.e. a ß-type alloy and (ii) introducing a reasonable amount of porosity. The composition of Ti-40Nb was chosen for the present work, as it allows to stabilize a single ß-type phase with low Young´s modulus at room temperature.
The samples were produced by a powder metallurgical approach. The Ti-40Nb alloy powder was obtained by ball-milling of elemental Ti and Nb powders. The influence of the milling parameters on the oxygen content in the milled powder was studied. Powders with a lowest oxygen content of 0.4 wt.-% had an almost single ß-type phase after heat treatment and quenching.
Porous samples were produced by loose powder sintering, hot-pressing and sintering with NaCl as a space-holder. The influence of the different processing routes and different porosities on the mechanical properties of the alloy was studied. The samples produced by loose powder sintering had mechanical properties close to those of cortical human bone (Young´s modulus 20 GPa, compression strength 150 MPa) and the samples produced by loose sintering with space-holder materials had mechanical properties close to those of human spongy bone (Young´s modulus 0.2-2 GPa, compression strength 50 MPa). Porous Ti-40Nb samples were coated with bone-like hydroxyapatite by an electrochemical deposition method in order to improve the osseointegration of the samples with bone tissue. The experiments were carried out with samples produced by different routes and a correlation between the deposition parameters and the morphology of the hydroxyapatite needles was found.
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Undersökning av mekaniska egenskaper hos sandwichelement av core-materialet Greenwood och ytskikt av papp : Styvhet, bärförmåga samt elementens beteenden vid belastning för olika tjocklekar på ytskikten / Examination of mechanical properties of sandwich panels made of the core-material Greenwood and surface layers of paperboard : Stiffness, ultimate capacity and structural behavior for different surface layer thicknessesNilsson, Maxim January 2023 (has links)
Byggbranschens utsläpp av växthusgaser utgör en stor andel av Sveriges totala utsläpp. För att minska de byggrelaterade utsläppen är det på många fronter som byggbranschen behöver förändras och effektiviseras. De senaste åren har en succesiv ökning av byggandet i trä skett vilket är gynnsamt då trä alternativet är mer klimatvänligt än stål och betong. De tuffa klimatmålen vi nu står framför innebär dock att mer behöver göras än att endast öka andelen träbyggnader. Pappersmassaindustrin är lätt att bortse ifrån, då den hittills inte varit relevant för byggbranschen och för att återanvändning är relativt framträdande inom den branschen. Ifrån sågverken som sönderdelar trästockar till virke fraktas flis som blir över till pappersbruk. Av flisen görs sedan bland annat diverse pappförpackningar som går att återvinna. Problemet är att dessa förpackningar endast går att återvinna ett visst antal gånger innan fibrerna blir obrukbara och istället används som biobränsle. Om byggmaterial skulle gå att producera baserat på dessa fibrer, skulle detta innebära en mer långlivad användning av dem. Ett byggmaterial som uppfunnits, gjort på fibrer från pappersmassabruk är core-materialet ”Greenwood”. Eftersom materialet är nytt och egenskaperna till stor del är okända krävs det att diverse studier görs som undersöker materialets olika egenskaper som är relevanta för en eventuell tillämpning inom byggbranschen. Denna studie avser att undersöka skjuvstyvhet, böjstyvhet och bärförmåga hos sandwichelement uppbyggda av core-materialet Greenwood och ytskikt av papp. Detta genom att först dynamiskt och statiskt testa de ingående materialens egenskaper, följt av böjprovning av nio sandwichbalkar med varierande tjocklek på ytskikten. Samtliga balkar testades även dynamiskt. Core-materialet Greenwood som ingick i sandwichelementen var endast den begränsande faktorn en gång av tio böjprov. När core-materialets skjuvstyvhet togs fram både dynamiskt och statiskt och när den omvandlades till en skjuvmodul visade det sig att Greenwood har en mer än dubbelt så stor styvhet som EPS-cellplast vid liknande densitet. Detta är intressant då denna cellplast ofta agerar som ett core-material i sandwichelement ute i byggbranschen. Testerna visar även på att balkarna har en relativt liten spridning vilket innebär att resultaten har god tillförlitlighet. Slutligen, kan det konstateras att dessa sandwichelement uppvisar sega egenskaper med en viss kvarvarande lastkapacitet även efter brott. Samtliga nämnda egenskaper ovan talar för en viss potential för tillämpning av dessa sandwichelement inom byggbranschen. Fortsatta studier av fukt- och krypegenskaper vid långtidsbelastning rekommenderas, vilket är viktigt för användning inom byggandet. De omfattande resultaten från föreliggande studie utgör dock ett bra underlag för fortsatta undersökningar och värdering av möjliga tillämpningar. / The construction industry`s greenhouse emissions, makes up for a large portion of Sweden’s total emissions. In order to reduce construction related emissions, a fair amount of fronts within the construction industry needs to be changed and streamlined. In the last couple of years, there has been a successive increase in the number of structures that are built from wood amongst other things, which is beneficial because the wood alternative is more climate friendly than steel and concrete. The current tough climate goals entails that more has to be done than just increasing the amount of wood constructions. The pulp industry is easy to write off because so far, it has not been relevant to the construction industry and because recycling is relatively prominent within that industry. From the sawmills that dismember wooden logs to lumber, leftover wood chips are transported to paper mills. Among other things, different cardboard packages that can be recycled are then made from those wood chips. The problem with these packages is that they can only be recycled a certain number of times before the fibers become unusable and instead, are used as biofuel. If building materials were to be able to be produced with these fibers, that would be a more long-lived use of them. A building material, recently invented, made of fiber from paper mills is the core-material “Greenwood”. Because the material is new and its properties for the most part are unknown, this requires that various studies are conducted that examines the different properties the material possesses that are relevant for a contingent enforcement within the construction industry. This study intends to examine the shear rigidity, flexural rigidity and maximum capacity for sandwich panels made from the core-material Greenwood and faces of paperboard. This was achieved by first dynamically and statically test the properties of the two different materials, followed by flexure testing nine sandwich beams with varying face thicknesses. Every beam was also tested dynamically. The core-material Greenwood which was a part of the sandwich panels, was only the limiting factor 1 time out of 10 flexure tests. When the shear rigidity of the core-material was calculated both statically and dynamically and when it was converted to a shear modulus it was shown that Greenwood has a rigidity of more than double that of EPS cellular plastic at similar density. This is interesting because this type of cellular plastic often acts as a core-material in sandwich structures found in the construction industry. The tests also show that the beams have a relatively small spread which means that the results have good reliability. Finally, it can be concluded that these sandwich panels exhibit ductile properties with a certain lasting load capacity even after ultimate load has been reached. Every property mentioned above indicates that there is a certain potential for applicability of these sandwich panels within the construction industry. Continued studies of moisture properties and creep properties during long-term loading is recommended, which is important for a possible use within construction. The extensive results from this study constitutes a good basis for continued research and assessment of possible applications.
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