We have seen an increased interest and extensive research in the monitoring of a process over time whose characteristics are represented mathematically in functional forms such as profiles. Most of the current techniques require all of the data for each profile to determine the state of the process. Thus, quality engineers from industrial processes such as agricultural, aquacultural, and chemical cannot make process corrections to the current profile that are essential for correcting their processes at an early stage. In addition, the focus of most of the current techniques is on the statistical significance of the parameters or features of the model instead of the practical significance, which often relates to the actual quality characteristic. The goal of this research is to provide alternatives to address these two main concerns. First, we study the use of a Shewhart type control chart to monitor within profiles, where the central line is the predictive mean profile and the control limits are formed based on the prediction band. Second, we study a statistic based on a non-linear mixed model recognizing that the model leads to correlations among the estimated parameters. / Doctor of Philosophy / Checking the stability over time of the quality of a process which is best expressed by a relationship between a quality characteristic and other variables involved in the process has received increasing attention. The goal of this research is to provide alternative methods to determine the state of such a process. Both methods presented here are compared to the current methodologies. The first method will allow us to monitor a process while the data is still being collected. The second one is based on the quality characteristic of the process and takes full advantage of the model structure. Both methods seem to be more robust than the current most well-known method.

[pt] O monitoramento de perfis é utilizado para verificar a estabilidade de uma relação funcional envolvendo uma variável resposta e uma ou mais variáveis explicativas ao longo do tempo. Kang e Albin (2000) fizeram uso do gráfico de controle qui-quadrado com parâmetros de projeto fixos para monitorar perfis lineares representados por um modelo de regressão linear simples. Nessa dissertação, com base nos estudos de Kang e Albin (2000), desenvolvemos o gráfico de controle qui-quadrado com tamanho de amostra variável para o monitoramento de um perfil linear. O gráfico proposto monitora o intercepto e o coeficiente de inclinação de um modelo de regressão linear simples, com o uso de amostras com dois tamanhos. O desempenho do gráfico proposto é comparado com o desenvolvido por Kang e Albin (2000). A medida de desempenho utilizada na comparação é o número médio de amostras até um sinal, obtida através de uma análise baseada em cadeias de Markov. Concluímos que é vantajoso utilizar o gráfico de controle qui-quadrado com tamanho de amostra variável. / [en] The monitoring of profiles is used to verify the stability of a functional relationship involving a response variable and one or more explanatory variables over time. Kang and Albin (2000) employed the chi-square control chart with fixed design parameters for monitoring linear profiles represented by a simple linear regression model. Based on the studies of Kang and Albin (2000), we developed the chi-square control chart with variable sample size for monitoring a linear profile. The proposed chart monitors the intercept and slope coefficient of a simple linear regression model, using two different sample sizes. The performance of the graph developed by Kang and Albin (2000) and the one presented here is compared. The average run length, obtained through a Markov chain, was used as performance measure to compare the two charts. We conclude that it is advantageous to use the chi-square control chart with variable sample size.