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This dissertation proposes novel solutions for important drawbacks of antenna arrays. One of the main contributions of the presented work is size reduction and nulling performance improvement of traditionally large anti-jam global positioning system (GPS) arrays using miniature antennas and electrically small resonators emulating an engineered metamaterial. Specifically, a miniaturized coupled double loop (CDL) dual band antenna is first introduced as a small antenna element of the compact GPS array. The loops that are capacitively coupled using lumped element capacitor, and employ metallic pins around their perimeter to improve the radiation efficiency by achieving a volumetric current distribution. This design is employed for the implementation of a compact 2x2 GPS array by reducing the inter-element spacing between the adjacent elements. However, having the antenna elements in close proximity of each other yields to a high mutual coupling and potentially degrades the nulling performance. The mutual coupling is performed by observing the magnetic field distribution within the array. It is noticed that the mutual coupling can be reduced by using metamaterial resonators. The right hand circular polarization (RHCP) radiation nature of the array complicates the mutual coupling suppression as compared to linear arrays. It is determined that split ring resonator (SRRs) are effective to mitigate the mutual coupling problem if placed strategically around the antenna elements. The study is verified experimentally where the mutual coupling is reduced by more than 10 dB. Lowering the mutual coupling improved the array's nulling capability by increasing the nulls depth by 8 dB as well as enhancing the accuracy of the nulls' locations. The second major contribution of the presented work is to introduce a novel microfluidic based beam-scanning technique for the implementation of low cost mm-wave antenna arrays. Traditionally, beam scanning capability is obtained using mechanical steering of the entire antenna structure or electronic components such as switches or phase shifters. The former is bulky, whereas the latter technique requires integrating substantial and expensive hardware in the array's feed network. For instance, a beam-scanning 1x8 focal plane array (FPA) would employ 7 single pole double through (SPDT) switches in its feed network. If an 8x8 FPA is desired, then 8x7+8 switches are required that results in an efficient design in terms of power loss and cost. In this dissertation, the microfluidic principles are introduced for designing and implementing affordable beam scanning antenna array with high gain radiation. Specifically, a microfluidic-based focal plane array 1x8 (MFPA) is designed and implemented at 30 GHz. The proposed MFPA consists of microfluidic channels connecting reservoirs. Both of the channels and reservoirs are filled with a low loss dielectric solution, and the antenna is formed by using a small volume of liquid metal. The beam scanning capability is obtained by placing the array at the focal point of a microwave lens and moving the antenna among the reservoirs using a micropump. Therefore, the feed network is extremely simplified by avoiding using SPDT switches. In addition, a strategic design methodology for a completely passive resonant based corporate feed network is discussed. The array is characterized numerically and verified experimentally. The simulated and measured performances are in a very good agreement with ±300 FoV and > 21 dB realized gain. However, the array's radiation pattern exhibits high side lobe level (SLL) due to the resonant nature of the introduced corporate feed network. Consequently, new resonant and non-resonant straight based feed networks are introduced to alleviate the high SLL issue. Moreover, they are modeled with appropriate equivalent circuits in order to analyze the array's performance analytically in terms of -10 dB |S11| bandwidth and power loss. The analytical solution is based on the transmission line theory and two ports network analysis. It is verified with the full wave simulations and a very good agreement is observed. Using the straight feed network reduces the SLL to more than 20 dB relative the pattern's peak. This enhancement in the performance is verified experimentally as well by designing, fabricating and testing a 30 GHz MFPA fed using a resonant based straight network. A ±250 FoV is obtained with a SLL < -20 dB and 4% -10 dB |S11| bandwidth.

In modern wireless communication and radar systems, filters play an important role in getting a high-quality signal while rejecting spurious and neighboring unwanted signals. The filters with reconfigurable features, such as tunable bandwidths or switchable dual bands, also play a key part both in realizing the compact size of the system and in supporting multi-communication services. The Chapters II-IV of this dissertation show the studies of the filters for microwave communication. Bandpass filters realized in ring resonators with stepped impedance stubs are introduced. The effective locations of resonant frequencies and transmission zeros are analyzed, and harmonic suppression by interdigital-coupled feed lines is discussed. To vary mid-upper and mid-lower passband bandwidths separately, the characteristic impedances of the open-circuited stubs are changed. Simultaneous change of each width of the open-circuited stub results in variable passband bandwidths. Asymmetric stepped-impedance resonators are also used to develop independently controllable dual-band (2.4 and 5.2 GHz) bandpass filters. By extending feed lines, a transmission zero is created, which results in the suppression of the second resonance of 2.4-GHz resonators. To determine the precise transmission zeros, an external quality factor at feeders is fixed while extracting coupling coefficients between the resonators. Two kinds of feed lines, such as hook-type and spiral-type, are developed, and PIN diodes are controlled to achieve four states of switchable dual-band filters. Beam-scanning features of the antennas are very important in the radar systems. Phase shifters using piezoelectric transducers and dielectric leaky-wave antennas using metal strips are studied in the Chapters V-VII of this dissertation. Meandered microstrip lines are used to reduce the size of the phase shifters working up to 10 GHz, and reflection-type phase shifters using piezoelectric transducers are developed. A dielectric film with metal strips fed by an image line with a high dielectric constant is developed to obtain wide and symmetrical beam-steering angle. In short, many techniques are presented for realizing reconfigurable filters and large beam-scan features in this dissertation. The result of this work should have many applications in various wireless communication and radar systems.

Yes / This paper presents empirical results of an innovative beam scanning leaky-wave antenna (LWA) which enables scanning over a wide angle from -35o to +34.5o between 57 GHz and 62 GHz, with broadside radiation centered at 60 GHz. The proposed LWA design is based on composite right/left-handed transmission-line (CRLH-TL) concept. The single layer antenna structure includes a matrix of 3×9 square slots that is printed on top of the dielectric substrate; and printed on the bottom ground-plane are Π and Tshaped slots that enhance the impedance bandwidth and radiation properties of the antenna. The proposed antenna structure exhibits metamaterial property. The slot matrix provides beam scanning as a function of frequency. Physical and electrical size of the antenna is 18.7×6×1.6 mm3 and 3.43􀣅􀫙×1.1􀣅􀫙×0.29􀣅􀫙, respectively; where 􀣅􀫙 is free space wavelength at 55 GHz. The antenna has a measured impedance bandwidth of 10 GHz (55 GHz to 65 GHz) or fractional bandwidth of 16.7%. Its optimum gain and efficiency are 7.8 dBi and 84.2% at 62 GHz. / Partially supported by innovation programme under grant agreement H2020-MSCA-ITN-2016 SECRET- 722424 and the financial support from the UK Engineering and Physical Sciences Research Council (EPSRC) under grant EP/E022936/1.

Lithium-ion batteries(LIBs) have dominated the energy storage market in the past two decades. The high specific energy, low self-discharge, relatively high power and low maintenance of LIBs enabled the revolution of electronic devices and electric vehicle industry, changed the communication and transportation styles of the modern world. Although the specific energy of LIBs has increased significantly since first commercialized in 1991, it has reached a bottleneck with current electrode materials. To meet the increasing market demand, it is necessary to develop high capacity electrode materials.<div><br></div><div>Current commercial anode material for LIB is graphite which has a specific capacity of 372 mAh g-1. Other group IV elements (silicon (Si), germanium (Ge), tin (Sn)) have much higher capacities. However, group IV elements have large volume change during lithiation/delithiation, leading to pulverization of active materials and disconnection between electrode particles and current collector, resulting in fast capacity fading. To address this issue, it is essential to understand the microstructural evolution of Si, Ge and Sn during cycling.<br></div><div><br></div><div>This dissertation is mainly focused on the morphological and structural evolution of Sn and Ge based materials. In this dissertation, anin situ focused ion beam-scanning electron microscopy (FIB-SEM) method is developed to investigate the microstructuralevolution of a single electrode particle and correlate with its electrochemical performance. This method is applied toall projects. The first project is to investigate the microstructural evolution of a Sn particle during cycling. Surface structures of Sn particles are monitored and correlated with different states of charge. The second project is to investigate the morphological evolution of Ge particles at different conditions. Different structures (nanopores, cracks, intact surface) appear at different cycling rates. The third project is to study selenium doped Ge (GeSe) anodes. GeSe and Ge particles are tested at the same condition. Se doping forms Li-Ge-Se network, provides fast Li transport and buffers volume change. The fourth project is to study the reaction front of Ge particle during lithiation. Micron-sized Ge particles have two reaction fronts and a wedge shape reaction interface, which is different from the well-known core-shell mode. The fifth project is to investigate antimony (Sb)-coated porous Ge particles. The Sb coating suppresses electrolyte decomposition and porous structure alleviates volume change. The results in this dissertation reveal fundamental information about the reaction mechanism of Sn and Ge anode. The results also show the effects of doping, porous structuring and surface coating of anode materials.</div>

Fluorescence lifetime imaging microscopy (FLIM) is an imaging modality that is able to provide key insights into subcellular processes. When used to measure Förster resonance energy transfer (FRET), for instance, it can discern protein-protein interactions and conformational changes. This kind of information is highly useful in the drug screening process in order to determine the effectiveness of drug leads and their mechanisms of action. FLIM has yet to be successfully translated to high-content screening (HCS) platforms due to the high throughput and fine temporal and spatial resolution requirements of HCS. Our prototype HCS FLIM system uses a time-resolving instrument called a streak camera to multiplex the FLIM scanning process, allowing for 100 confocal spots to be simultaneously scanned across a sample. There have been a few major advancements to the prototype. First the fiber array used to connect the fluorescence channels to the streak camera was characterized. Its alternating fiber delay scheme was successful in greatly reducing optical crosstalk between adjacent channels. Next, an optical beam scanner for parallel excitation beams was designed and implemented, greatly improving the possible scan speeds of the system. The streak camera was upgraded to a higher repetition rate sweep, and modifications to system components and reconstruction procedures were made to accommodate the new sweep unit. A single-photon avalanche diode array was also tested as a possible replacement for the streak camera, and was found to offer photon detection efficiency advantages. Finally, improvements were made to the excitation power and optical throughput of the system in order to reduce the required exposure time. These advances to the prototype system bring it closer to realizing the requirements of HCS FLIM, and provide a clear picture for future improvements and research directions. / Thesis / Doctor of Philosophy (PhD) / Fluorescent proteins are commonly used to tag subcellular targets so that they can easily be distinguished with a fluorescence microscope. While this can help visualize where different organelles and proteins are located in the cell, a great deal more information can be gained by measuring the fluorescence lifetime at each point in the sample, which is highly sensitive to the microenvironment. Fluorescence lifetime imaging microscopy (FLIM) has the potential to be a powerful technique for testing drug leads in the drug discovery process, although current FLIM systems are not able to provide the high throughput speeds and high temporal resolution required for drug screening. This thesis project has succeeded in improving a highly parallel FLIM microscope by reducing inter-channel crosstalk, implementing an optical scanner, improving power and optical throughput, and investigating future time-resolving instruments. This progress has brought the prototype setup closer to being used in a drug screening environment.

Yes / The paper presents a technique to enhance the isolation between adjacent radiating elements which is common in densely packed antenna arrays. Such antennas provide frequency beam-scanning capability needed in Multiple-Input Multiple-Output (MIMO) systems and Synthetic Aperture Radars (SARs). The method proposed here uses a metamaterial decoupling slab (MTMDS), which is located between radiating elements, to suppress mutual-coupling between the elements that would otherwise degrade the antenna efficiency and performance in both the transmit and receive mode. The proposed MTM-DS consists of mirror imaged Eshaped slits engraved on a microstrip patch with inductive stub. Measured results confirm over 9–11 GHz with no MTM-DS the average isolation (S12) is -27 dB; however, with MTM-DS the average isolation improves to -38 dB. With this technique the separation between the radiating element can be reduced to 0.66λo, where λ0 is free space wavelength at 10 GHz. In addition, with this technique there is 15% improvement in operating bandwidth. At frequencies of high impedance match of 9.95 GHz and 10.63 GHz the gain is 4.52 dBi and 5.40 dBi, respectively. Furthermore, the technique eliminates poor front-to-back ratio encountered in other decoupling methods. MTM-DS is also relatively simple to implement. Assuming adequate space is available between adjacent radiators the MTM-DS can be fixed retrospectively on existing antenna arrays, which makes the proposed method versatile. / Partially supported by innovation programme under grant agreement H2020-MSCA-ITN-2016 SECRET- 722424 and the financial support from the UK Engineering and Physical Sciences Research Council (EPSRC) under grant EP/E022936/1.

Cette thèse s'inscrit dans le cadre du projet collaboratif FUI RFID AERO dont le leader est Eurocopter. Le but de ce projet est le développement d'un système assurant la traçabilité des différentes pièces d'un aéronef. Cette thèse se focalise sur la conception d'antennes lecteur et de tags RFID UHF faible coût.Deux objectifs sont visés dans le cadre de cette thèse. Le premier est la conception d'antennes pour lecteurs RFID fonctionnant en contact ou à proximité des surfaces métalliques. Nos conceptions sont basées d'une part sur les phénomènes d'ondes constructives en plaçant une surface métallique à un quart de la longueur d'onde. D'une autre part, la conception repose sur l'utilisation de structures AMC. De plus, nous proposons une méthode de réduction de dimensions de cellules AMC. Le second objectif de la thèse est la miniaturisation de tags pour l'identification de pièces essentiellement métalliques. Nous proposons des méthodes de conception de tags miniatures durcis, non détachables ou flexibles ainsi qu'un prototype pour chacune d'entre elles.Enfin, les antennes lecteur et tags développés dans cette thèse, les lecteurs RFID et des systèmes connexes développées par d'autres partenaires ont été mis en œuvre dans un aéronef. Les tests du système complet sont satisfaisants et répond aux objectifs du projet. / This Ph.D thesis is part of the FUI RFID AERO project led by Eurocopter. The aim of this project is to provide a traceability system of the aircraft items. This work focuses on low-cost UHF RFID reader antennas and tags design.Two research axes are developed. The first one is the RFID reader antennas design for metallic surfaces. The designs are based on constructive wave phenomenon by placing a metallic plate at a quarter wavelength of the radiating element. On the other hand, the insertion of AMC structures was also studied. Furthermore, we propose a size reduction technique for AMC structures. The second goal is tag size miniaturization for metallic or non-metallic objects identification. We propose design methods of size miniaturization for hard or flexible tags. Besides, we apply these methods by designing one tag for each family.Finally, the reader antennas and tags proposed in this thesis, the RFID readers and the related systems developed by the others partners were implemented into an aircraft. Tests of the complete system are in good agreement with the expected goals.

Cette thèse porte sur les dispositifs de contrôle de faisceaux de protons balayés. La société IBA (Ion Beam Applications), ayant besoin d'une d'unité moniteur pour équiper ses centres de protonthérapie dotés de la technologie Pencil Beam Scanning, a fait appel au groupe applications médicales du Laboratoire de Physique Corpusculaire de Caen. En 2008, ce groupe a alors réalisé, en collaboration avec IBA, une chambre d'ionisation, nommée IC2/3, destinée à équiper la tête d'irradiation universelle IBA dédiée au PBS. Ce détecteur vérifie que la fluence particulaire reste conforme à celle planifiée. Une partie du travail de thèse a consisté à caractériser cette unité moniteur sur une gamme d'énergie faisceau, de position faisceau et de débit de dose applicables en protonthérapie. Après une introduction sur la protonthérapie, la phase de validation d'IC/3 est exposée dans ce mémoire. Les informations fournies par cette unité moniteur permettent le contrôle du faisceau en termes de fluence particulaire mais n'assurent pas le contrôle qualité du traitement en termes de distribution spatiale de dose. La seconde partie du travail de thèse a donc été de concevoir un dispositif, toujours pour les faisceaux de protons balayés, capable de reconstruire la distribution spatiale de dose délivrée dans le patient au cours du traitement. L'élaboration de son cahier des charges est présentée dans ce mémoire ainsi que les diverses études de conception. Ce travail a permis de parvenir à un certain nombre de recommandations pour sa réalisation mais également à diverses perspectives de recherche.

Das Laserstrahlhartlöten ermöglicht die Herstellung von Fügeverbindungen mit exzellenten Nahtqualitäten. Daher hat es sich bei anspruchsvollen Anwendungen, wie zweiteiligen Heckklappen und der Verbindung von Dach und Seitenwandrahmen (Dachnullfuge) etabliert. Um die hohen Qualitätsanforderungen durch das Laserstrahlhartlöten realisieren zu können, sind allerdings anspruchsvolle konstruktive Randbedingungen zu erfüllen, die über die Fertigungskette nicht immer vollständig sicherzustellen sind. Das Ergebnis solcher Fertigungs- und Materialschwankungen äußert sich dann oft als Nahtimperfektionen, die während des Laserlötprozesses entstehen. Diese verursachen vor allem mit steigenden Prozessgeschwindigkeiten einen erhöhten und kostenintensiven Nacharbeitsaufwand und sollten daher vermindert bzw. gänzlich vermieden werden. Das Ziel ist somit den Laserlötprozess so robust wie möglich auszulegen, um auf diese Fertigungsschwankungen ohne Einschränkungen in der Nahtqualität reagieren zu können. Im ersten Teil dieser Arbeit werden wesentliche Einflussfaktoren auf die Ausbildung der Nahtqualität am schrägen Bördelstoß untersucht und die systemtechnischen Grenzen mit einem statischen und runden Laserspot aufgezeigt. Weiterhin werden die resultierenden Nahtqualitäten durch das Laserstrahllöten mit gescanntem Laserstrahl in Vorschubrichtung untersucht. Die Ergebnisse zeigen, dass sich die Nahtqualität mit diesem innovativen Ansatz bezüglich des Anbindungsquerschnittes und der Oberflächenqualität weiter steigern lassen. Dies lässt sich ebenfalls für höhere Prozessgeschwindigkeiten realisieren. Abschließend werden neuartige Möglichkeiten der Prozessüberwachung, sowie erste Ansätze zur Prozessregelung des Laserstrahlhartlötens am schrägen Bördelstoß vorgestellt. Die erzielten Resultate zeigen, dass sich der Laserstrahlhartlötprozess durch die Regelung der Laserleistung in Verbindung mit evaluierten Temperaturfeldern im Bereich der Prozesszone online kontrollieren und sich dadurch die Prozessstabilität merklich steigern lässt.