Pulse Tube Cryocoolers (PTC) is widely used in aerospace and missile guiding systems where extreme reliability and ruggedness are crucial. PTCs, in particular, are a class of rugged refrigeration systems that are capable of maintaining temperatures as low as 4 K, without a moving part in their cold end. The operation of PTCs is based on complicated and poorly-understood solid-fluid interactions involving periodic flows of a cryogenic fluid in micro porous structures. Currently, PTCs is often modeled as one-dimensional flow fields using methods whose relevance to cryocoolers is at best questionable. Furthermore, recent CFD-based investigations have underscored the need for adequate closure relations representing periodic flows in anisotropic micro porous media, and have shown that multi-dimensional effects can be significant in PTCs. The objectives of this investigation were to experimentally measure and correlate the anisotropic hydrodynamic parameters for typical micro porous structures that are used in the regenerators of PTCs fillers; perform modeling and CFD-based simulations to elucidate the component and system-level thermo-fluidic processes in modern pulse tube cryocooler designs; and perform a preliminary CFD-based assessment of the effect of miniaturization on the thermal performance of a current PTC design. In the experiments, the measurement and correlation of the directional (axial and radial) permeabilities and Forchheimer s inertial coefficients of meshed screen, sintered mesh, foam metal, and stacked micro-machined plate regenerator fillers were of interest. Hydrodynamic parameters under steady-state conditions were addressed first. Pressure drops were measured for purely axial flow in cylindrical test sections and predominantly radial flows in annular test sections that contained regenerator fillers of interest, under steady-state conditions. The permeabilities and Forchheimer s inertial coefficients were then obtained in an iterative process where agreement between the data and the predictions of detailed CFD simulations addressing the entire test sections and their surroundings were sought. Periodic flows were then addressed. Using high frequency pressure transducers and hot wire anemometry, instantaneous pressures and mass fluxes are measured under periodic purely axial flow conditions. CFD simulations of the experiments were then performed, whereby permeabilities and Forchheimer coefficients that bring about agreement between data and simulation results were calculated.

The objective of this work is to investigate the performance of SiGe HBTs and scaled CMOS devices in extreme environments. In this work, the inverse mode operation of SiGe HBTs is investigated as a potential solution to the vulnerability of SiGe HBTs to single event effects. The performance limitations of SiGe HBTs operating in inverse mode are investigated through an examination of the effects of scaling on inverse mode performance and optimization schemes for inverse mode performance enhancements are discussed and demonstrated. In addition the performance of scaled MOSFETs, that constitute the digital backbone of any BiCMOS technology, is investigated under radiation exposure and cryogenic temperatures. Extreme environments and their effects on semiconductor devices are introduced in Chapter 1. The immunity of 90nm MOSFETs to total ionizing dose damage under proton radiation is demonstrated. Inverse mode operation of SiGe HBTs is introduced in Chapter 2 as a potential radiation hard solution by design. The effect of scaling on inverse mode performance of SiGe HBTs is investigated and the performance limitations in inverse mode are identified. Optimization schemes for improving inverse mode performance of SiGe HBTs are discussed in Chapter 3. Inverse mode performance enhancement is demonstrated experimentally in optimized device structures manufactured in a commercial third generation SiGe HBT BiCMOS platform. Further, a cascode device structure, the combines the radiation immunity of an inverse mode structure with the performance of a forward mode common emitter device is XIV discussed. Finally, idealized doping profiles for inverse mode performance enhancement is discussed through TCAD simulations. The cryogenic performance of inverse mode SiGe HBTs are discussed in Chapter 4. A novel base current behavior at cryogenic temperature is identified and its effect on the inverse mode performance is discussed. Matching performance of a 90nm bulk CMOS technology at cryogenic temperatures is investigated experimentally and through TCAD simulations in Chapter 5. The effect of various process parameters on the temperature sensitivity of threshold voltage mismatch is discussed. The potential increase of mismatch in subthreshold MOSFETs operating in cryogenic temperatures due to hot carrier effects is also investigated.

Cette thèse expérimentale explore les propriétés supraconductrices du silicium très fortement dopé, en particulier au bore, ainsi que les propriétés physiques anormale observées à plus hautes températures. La supraconductivité de Si:B est obtenue sous 1K, pour des dopages en bore supérieurs à la limite de solubilité du bore dans le silicium. Le Si:B est métallique à ces taux de dopage. Dans une première partie, nous exposons les différentes techniques expérimentales exploitées au cours de cette thèse. Nous expliquons les différentes techniques de dopage hors équilibre identifiées pour doper du silicium au-delà de la limite de solubilité, puis les techniques de caractérisation pour contrôler la qualité des couches dopées obtenues, ainsi que les méthodes de mesures aux très basses températures. Dans une deuxième partie, nous exposons les résultats obtenus sur la supraconductivité de Si:B en faisant varier dans un premier temps le taux de dopage en bore, puis en renouvelant l'étude à différentes épaisseurs de couche dopée. Nous montrons notamment que l'évolution de la Tc avec le couplage électron-phonon $lambda$ ne suit pas une loi de McMillan classique, mais plutôt une loi de puissance comme celle observée dans le cas du diamant supraconducteur. Nous montrons que ce résultat peut être expliqué dans le cadre d'un modèle d'un supraconducteur à deux couches de $lambda$ différents. En étudiant la dépendance en température et angulaire de Hc2, nous montrons que Si:B est un supraconducteur intrinsèquement de type I, mais qui devient de type II sous effet d'impuretés, et que la supraconductivité est à caractère bidimensionnel. Dans une troisième partie, nous présentons des comportements anormaux de certaines caractéristiques physiques mesurées dans certaines séries de Si:B, à partir de 50K et qui persistent jusqu'à au moins 400K. Nous présentons des mesures de magnétotransport, d'effet Hall et de mesures thermoélectriques qui présentent toutes des caractéristiques hautement non linéaires, et donc anormales pour un métal. L'origine de ces anomalies est toujours ouverte. Enfin, nous présentons quelques perspectives de travail, en particulier les premières mesures sur un échantillon avec une géométrie de type SQUID. / This experimental PhD thesis explore the superconductivity of heavily boron doped epilayers as well as some unusual properties observed at high temperatures. The superconductivity of Si:B is observed below 1K and triggered by boron content exceeding the solubility limit of boron into silicon. For such high boron contents, the silicon layers are metallic. In a first part, we develop the various experimental techniques used. We explain the principles of the out-of-equilibrium doping techniques required to doped beyond the solubility limit. We develop also on the characterisation techniques used to control the quality of the samples, as well as the low temperatures measurement techniques. In a second part, we show the results obtained on the superconductivity of Si:B, obtained forst by varying the boron content at a given layer thickness, and then as a function of the layer thickness. We show that the evolution of Tc with the electron-phonon coupling constant lambda doesn't follow the classical McMillan law, but rather a power of law as it was reported for superconducting diamond. We show that this result can be explained by a double layer model with dislocations resulting in two different lambda values for each sublayer. The study of the temperature and angular dependency of the Hc2 also show that Si:B is an intrinsic type I superconductor turned into type II with defect effects, and that the superconductivity is bidimensionnal. In a third part, we present the anomalous high temperature behaviour of some Si:B epilayers, starting from 50K and observed at least up to 400K. We present magnetotransport, Hall effect and thermoelectric measurements that all show a highly non linear behaviour, unusual for a metal. The origin of these anomalies is still an open question. We finally present some future perspectives, including the first measurements on a Si:B SQUID-like geometry.

Há alguns anos, diversos estudos da influência dos parâmetros do tratamento térmico vêm sendo desenvolvidos, para a obtenção de propriedades que permitam atingir os requisitos de trabalho e que gerem ferramentas de vida útil estendida. Nesse contexto, tem sido demonstrado que o tratamento criogênico não só provoca a transformação da austenita residual, trazendo melhorias no dimensional da ferramenta, mas também pode promover a precipitação de carbonetos finos, com ganho em tenacidade e propriedades de desgaste.Neste estudo são relatados os resultados obtidos de ensaios de dureza, desgaste, impacto Charpy e microscopia TEM, efetuado em amostras de aço H13.Os tratamentos térmicos foram realizados em forno a vácuo com resfriamento por nitrogênio sob 5 bar de pressão, sendo utilizados os seguintes parâmetros: austenitização1040ºC, têmpera, e revenimento a 540ºC. As amostras foram comparadas com a condição de base que passou por tratamento térmico convencional, as outras condições foram submetidas a um revenido alternado com o banho criogênico. Nas rotas criogênicas o tempo de encharque em nitrogênio líquido foi de 1, 24 e 48 horas. Uma análise desses resultados permitiu constatar que o tratamento criogênico melhora a resistência ao desgaste, e influencia levemente a dureza. / A few years ago, several studies of the influence of parameters heat treatment have been developed to obtain properties that could meet the job requirements and managing tools for extended life. In this context, it has been demonstrated that the cryogenic treatment not only causes the transformation of austenite residual, bringing improvements in dimensional tool, but also can promote the precipitation of fine carbides, and an increase in toughness and wear properties. In this study there are the results of the test of hardness, two body abrasion wear, Charpy impact followed by microscopy TEM analyses were performed in samples from H13 steel. The heat treatments were performed in a vacuum furnace with cooling by nitrogen under pressure of 5 bar, and used the following parameters: austenitizing 1040°C, quenching, and tempering at 540°C. The aim was compared the H13 performance under of conventional heat treatment and cryogenic bath after quenching and before tempering. Soaking times in the cryogenic temperature were: 1, 24, and 48 hours. Analyses this results has shown the heat treatment increased the wear resistance, and slightly affects the hardness.

No description available.

Evaporative cooling is an alternative and efficient method of cooling in dry climates. When a liquid evaporates into the surrounding gas, the energy required for the change of phase produces a cooling effect. The wet bulb depression is the measure of potential for evaporative cooling. Greater the wet bulb depression greater is the cooling effect, and vice versa. The residential desert cooler, apart from cooling the air increases the humidity of the air in the room by absorbing moisture from the water supplied to the cooler. This may result in an undesirable increase in humidity level. Allergies is an additional problem with direct evaporative coolers. Indirect evaporative cooling does not have these two drawbacks. In the present work a small indirect evaporative cooler is developed with a cross flow heat exchanger and the performance of the cooler is evaluated under controlled environmental conditions. The results are compared with the results of an analytical model developed by assuming constant water film temperature on the external wall of the heat exchanger tube. The experimental results of the cooler show a satisfactory agreement with the analytical values. Design calculations are presented to show the performance characteristics of indirect evaporative coolers under different temperature and humidity conditions of the ambient. It has been shown that reducing the heat exchanger tube diameter to around 2 mm results in better cooling effect. Climatic conditions of different Indian cities are discussed with respect to the expected effectiveness of indirect evaporative coolers.

L'observation de la désintégration double bêta sans émission de neutrino (0ν2β) fournirait des informations essentielles sur la nature du neutrino et son échelle de masse absolue. Ce processus consiste en la transformation simultanée de deux protons en deux neutrons avec l'émission de deux électrons et aucun neutrino. Cette transition n'est possible que si les neutrinos sont égaux aux antineutrinos (nature Majorana du neutrino). Les recherches pour une désintégration à ce point rare représentent un défi technique complexe, car les expériences de prochaine génération visent des sensibilités de l'ordre de 10^27-10^28 ans afin d'avoir un potentiel de découverte élevé. Cette thèse est focalisée sur les projets LUMINEU et CUPID-Mo, développant la technique des bolomètres scintillants pour la recherche de désintégration 0ν2β avec le radio-isotope 100Mo.Les bolomètres sont des détecteurs cryogéniques mesurant l'énergie des particules déposées via un changement de température dans l'absorbeur. Si des cristaux scintillants sont utilisés comme absorbeurs, les signaux lumineux peuvent être enregistrés avec un bolomètre auxiliaire, sensible à l'énergie totale déposée par les photons de scintillation. Une telle configuration permet de séparer les particules α des γ/β, en rejetant le fond le plus difficile. La technologie des bolomètres scintillants est décrite en détail comme une option pour une future expérience cryogénique à l'échelle d'une tonne, appelée CUPID, qui peut couvrir complètement la région de masses de neutrinos dans la hiérarchie inversée. / Neutrinoless double beta (0ν2β) decay is a process of great interest for neutrino physics: its observation would provide essential information on neutrino nature and its absolute mass scale. This process consists of the simultaneous transformation of two protons into two neutrons with the emission of two electrons and no neutrino, implying the violation of the total lepton number. Such transition is possible only if neutrinos are equal to antineutrinos (Majorana particles). The searches for such a rare decay are becoming a complicated technical challenge, as next generation of 0ν2β experiments aim at sensitivities of the order of half-life at 10^27-10^28 yr. This thesis is focused on LUMINEU and CUPID-Mo projects, developing the scintillating bolometers technique for 0ν2β decay search with 100Mo with Li2MoO4 crystals. Bolometers are cryogenic detectors measuring the deposited particle energy as a change of temperature in the absorber. The use of scintillating crystals allows to perform discrimination of α particles from γ/β ones due to different light output of these two particle types, rejecting the most challenging background. The scintillating bolometers technology is described in details as an option for a future ton-scale cryogenic experiment, named CUPID, which can completely cover the inverted hierarchy region of neutrino masses.

Les particules cosmiques sont émises par différentes sources galactiques et sont composées de protons et de noyaux d'hélium. Ces éléments interagissent avec les matériaux et y déposent leur énergie par interaction nucléaire. L'instrument Planck/HFI a observé le ciel depuis l'espace dans le but de cartographier le fond diffus cosmologique. Pour cela, HFI embarque un plan focal refroidit à 100 mK composé de 54 bolomètres. Le flux de particules cosmiques, interagissant avec les composants des détecteurs (thermomètre, grille, wafer), chauffe ponctuellement les capteurs (glitches) ce qui entraine une dégradation du signal scientifique. Leur étude a révélé un autre effet thermique caractérisé par un chauffage global du plan focal de l'ordre du microkelvin, les High Coincidence Events (HCE). Deux familles de HCE ont été isolées dans les données : les rapides, générés par des gerbes de particules secondaires formées dans les couches externes du satellite et interagissant avec l'ensemble de l'instrument HFI ; les lents, généré par la vaporisation d'hélium formant un lien thermique ponctuel entre le plan focal et l'étage à 1,6 K lui faisant face. L'exposition d'une matrice de bolomètres TES à une source de particules α a démontré une réponse similaire mais également des glitches simultanés entre les pixels.Ces recherches démontrent que les particules cosmiques et les gerbes de particules doivent être étudiées afin d'éviter des effets thermiques prédominant. Le développement des prochaines générations de détecteurs, devront ainsi prendre en compte ces interactions indissociables d'une mission spatiale et s'en prémunir. / Cosmic rays are emitted from different galactic sources and consist of protons and helium nuclei. These elements interact with matter and deposit part of their energy by nuclear interaction.The Planck/HFI instrument observed the sky from space to map the Cosmic Microwave Background. For this purpose, HFI has a focal plane cool down to 100 mK and composed of 54 bolometers. The interactions of the cosmic ray flux with the detectors' components (thermometer, grid and wafer) heat up regularly the sensor (glitches) which leads to a degradation of the scientific signal. Studying them revealed another thermal effect characterized by a thermal increase of the entire focal plane up to the microkelvin range, the High Coincidence Events (HCE).Two HCE famillies were separated: the fast ones, generated by cosmic ray showers developed in the external layers of the satellite and interacting with the entire HFI instrument and the slow ones, generated by the vaporisation of helium forming a ponctual thermal link between the focal plane and the 1.6 K stage facing it.Exposure of a TES bolometer matrix to an α particules source showed a similar response but also simultaneous glitches on several pixels. This work demonstrates that cosmic rays and particle showers on next low temperature experiments has to be studied to prevent predominating thermal effects from it. The developpement of futur space experiments will have to take these interactions into account to elimiate them from data.

Les boucles de circulation naturelle d'hélium diphasiques sont utilisées comme systèmes de refroidissement d'aimants supraconducteurs de grande envergure, vus leurs avantages inhérents de sûreté et d'entretien. Des exemples sont le détecteur CMS au CERN (déjà en opération) ou les aimants du spectromètre R3B-GLAD au GSI (en installation). Une des préoccupations majeures lors du refroidissement par ébullition est la crise d'ébullition : la dégradation soudaine du transfert de chaleur pariétal au-delà d'une certaine valeur de flux de chaleur, dénommée critique. L'augmentation de température de paroi qui en résulte peut entraîner la perte de l'état supraconducteur de l'aimant.Les boucles de circulation naturelle à l'hélium ont déjà été étudiées expérimentalement et numériquement en régime permanent, spécialement en régimes pré-critiques (ébullition nucléée). Les travaux sur les transferts de masse et de chaleur en hélium en ébullition en régime transitoire présents dans la littérature ciblent principalement des systèmes de petites dimensions, des canaux très étroits ou trop courts, ou l'ébullition en bain. Bien que des comportements qualitativement similaires sont attendus, l'extrapolation de ces résultats à une boucle de circulation naturelle n'est pas évident, si possible. C'est pourquoi une étude particulière du comportement thermohydraulique transitoire de boucles d'hélium en circulation naturelle, lors d'une augmentation soudaine de la charge thermique, est nécessaire. Une partie de cette étude consiste en des expériences sur une boucle d'hélium diphasique en circulation naturelle de 2 m de haut, à 4,2 K. Deux sections chauffées verticales de diamètre différent (10 et 6 mm) et d'environ 1 m de longueur ont été testées. Les transitoires sont induits par une marche soudaine de puissance. Deux types de condition initiale ont été considérés : statique (sans puissance initiale), et en équilibre dynamique (puissance initiale non-nulle). L'évolution de la température de paroi le long de la section, le débit massique et la perte de charge a été mesurée. Parmi d'autres phénomènes, un fort intérêt a été porté au début de la crise d'ébullition. Les valeurs limites de flux de chaleur final auxquelles la crise arrive ont été déterminées. D'un côté, on a observé que la crise peut avoir lieu de façon temporaire ou permanente à une puissance appréciablement plus faible qu'en régime permanente. De l'autre côté, l'augmentation de la circulation initiale, à travers le flux de chaleur initial, peut inhiber partiellement ou totalement cette crise d'ébullition prématurée. On a déterminé que cette dégradation du transfert de chaleur est l'issu de deux phénomènes en compétition, véritablement inhérents à la circulation naturelle : une étape initiale d'accumulation uniforme de vapeur, avec inversion ou diminution de la vitesse d'entrée, et l'établissement ultérieur de la circulation, avec le transit d'un front froid depuis l'entrée. Une analyse semi-empirique nous a permis de déterminer un critère, basé sur l'évolution dynamique du profile spatial du titre massique, pour prédire le déclenchement de la crise. Néanmoins, il est nécessaire de connaître à priori l'évolution du débit massique pour pouvoir appliquer ce critère. La dernière partie de ce travail est dévouée à la production et validation de modèles et outils de calcul pour la simulation du comportement thermohydraulique d'un tel système. Deux options de modélisation sont présentées. L'une est une simplification des équations du modèle homogène 1D des écoulements diphasiques (mise en place en COMSOL) ; l'autre reprend le modèle homogène tel quel (programmé en C). Les simulations d'évolution du débit massique sont en assez bon accord avec les mesures, à l'exception d'un léger déphasage temporel. Ceci pourrait être dû à la combinaison d'un retard de l'instrumentation pour la mesure du débit et de l'inexactitude des hypothèses de base du modèle homogène lors de transitoires très violents. / Boiling helium natural circulation loops are used as the cooling system of large superconducting magnets because of their inherent safety and maintenance advantages. Examples are the cooling systems of the CMS detector solenoid magnet at CERN (already in operation) or the R3B-GLAD spectrometer magnet at GSI (in installation phase). A major concern in boiling cooling systems is that of boiling crisis: a sudden deterioration of the wall heat transfer takes place when the surface heat flux exceeds a certain value, called the critical heat flux (CHF). The resulting high temperatures on the wall could ultimately entail the loss of superconducting state of the magnet.Helium natural circulation loops have already been studied experimentally and numerically in steady state, especially in the pre-critical heat and mass transfer regimes (nucleate boiling). Works on transient boiling heat and mass transfer in helium present in the literature are mostly focused on small systems, very narrow channels, too short pipes or pool boiling. Although it is expected to find qualitative similarities with already observed behavior, the extrapolation to a natural circulation loop is not easy, if even possible. Hence the need for a particular study on the transient thermohydraulic behavior of helium natural circulation loops, after sudden increases in the heat load of the circuit.A part of this study consists of experiments conducted in a 2-meter high two-phase helium natural circulation loop at 4.2 K temperature. Two vertical heated sections with different diameters (10 and 6 mm) and around 1 m length were tested. Heat load transients were driven by a step-pulsed heat load. Transients with two types of initial conditions have been studied: static loop (no initial power applied) and in-dynamic-equilibrium loop (non-zero initial power applied). The evolutions of wall temperature along the heated section, total mass flow rate and pressure drop were measured. Among other phenomena, the nature of the onset of boiling crisis has received a special attention. The values of final heat flux limits for its occurrence have been determined. On the one hand, we observed that boiling crisis can take place in temporary or stable fashion at power significantly lower than in steady state. On the other hand, the increase of initial circulation, by raising initial heat flux, can inhibit partially or completely this power-premature boiling crisis. We could determine that this heat transfer deterioration is the result of two competing phenomena, veritably inherent to the natural circulation feature of the system: an initial stage of uniform vapor accumulation with inlet back-flow or velocity reduction, and the ulterior onset of circulation with the transit of a cold front from the entrance. A semi-empirical analysis of data allowed determining a criterion, based on the dynamic evolution of the quality profile in the section, to predict the incipience of boiling crisis. It became evident that it is necessary to know how the mass flow rate of the system is going to evolve, in order to apply the mentioned criterion.Hence, the other part of this work is aimed to the production and validation of models and calculation tools in order to simulate the thermohydraulic behavior of a two-phase helium natural circulation loop. Two modeling options are proposed. One of them consists of a simplification of the 1D two-phase homogeneous model equations (implemented in COMSOL) and the other of their full version (coded in C language). The simulated mass flow rate represents reasonably well the measured evolution except for a relatively small time phase-shift. This could be due to a combination of the delay of flow-metering instrumentation with the inaccuracy of the basic homogeneous model assumptions during violent transients.

Cryocooling is a continuously developing field of engineering, applied in the fieldsof aerospace, military, and medical sciences among others. There is a demand forsmaller and more efficient cryocoolers for spaceborne low-light observation missions,with many custom cooling systems having completed successful missions. The Stir-ling cycle is the most prevalent refrigeration technique used for space applications,with the pulse-tube, Joule-Thomson or reverse Brayton cycles being used in somespecial cases.A matrix heat exchanger is designed with 3D-printed 17-4 PH stainless steel end capsstreamlined for computer numerical control (CNC) production. The heat exchanger (HX) core consists of 1mm thick stainless steel spacers and 250μm thick copperchips that are tolerance-matched for photo etching, as well as pyrolytic graphitesheets (PGS) of 25μm, the thickest commercially available PGS without addedadhesive film material.The experiments of joining PGS and copper chips with Epo-Tek 301-2 epoxy tocreate a solid core structure for the heat exchanger did not result in a pressure-resistant laminate material. The graphite surface proved difficult to adhere to usingthis epoxy, creating voids, and easily delaminated into separate layers of PGS. Bond-ing the stack together using indium, testing epoxy with a higher ability to permeatethe PGS or diffusion-bonding through other means are presented as options forfurthering the HX development.Pressure testing of a copper-only laminated heat exchanger core showed that theend cap recess adhesion capability is a potential point of failure, as the designedstructure makes it impossible to inspect the results of the bond without curingthe epoxy and pressurising the system. The difficulty in establishing a tight seambetween the main counter-flow channels of the HX is also demonstrated here, asleakage between the channels occurred at pressures in the vicinity of 2