The objective of a coating operation is to transfer a defect free liquid film onto a continuous substrate in order to meet the requirements of the final products. Mainly two concerns govern the process. The first concern is the economics of the process and the second concern is the quality of the coated film. The economics of the process are dictated by the speed of coating and the film thickness. Clearly, higher speeds mean better productivity hence less cost of operation and thinner films are desirable because less material is being used. Quality is governed by film uniformity and integrity, indicating that the film will perform as designed. Film defects such as streaks or tiny air bubbles are indication that the film properties are not uniform rendering it unacceptable to customers. One of the most versatile coating systems to achieve thin films at high speeds is reverse roll coating which has been used for a long time all over the world. At low speed, typically 1m/s, this coating operation is inherently stable and with small gaps of order 100 microns can ii lead to film thickness of order 30-50 microns. Much research, theoretical and experimental, has been devoted to this coating flow but only at low speeds and for large gaps (>100 microns). There are no comprehensive data how very thin films, 20 microns and less (particularly lower limits in the region of 5 microns) can be achieved at high speeds, of 2 or more metres per second. This study is concerned precisely with this aim, that of investigating the effect of large speeds and small roller gaps (rollers nearly touching or in elastohydrodynamic contact) to achieve the very thin films desired by modern applications (electronics, medical and others). In order to achieve this aim, a rig was designed and built to enable to understand the effect of various coating conditions and liquid properties on the metered film thickness and coating instability. To achieve thin films at high speeds, small roll gap and low viscosity are needed, however flow instabilities will develop under these conditions. To achieve stable coating window at high speeds high surface tension is needed. It was found that the roll gap and the viscosity have complicated effect on the coating window. In the case of low viscosity liquid (7mPa.s), small roll gaps are needed, whereas in the case of high viscosity liquid (more than 30mPa.s), large gaps are needed. It was found that Weber number is better describer for ribbing instability in rigid reverse roll coating unlike in rigid forward roll coating in which capillary number is the one. In addition the potential of reverse deformable roll coating (rolls in elastohydrodynamic contact) was investigated in order to achieve much thinner films at higher speeds. As a result of the investigation of reverse deformable roll coating, it was found that there is a possibility to get much thinner stable films at much higher speeds compared to reverse rigid roll coating. The liquid transfer from an applicator roller to a PET film was investigated in this study. It was found that air stagnation at downstream meniscus and air entrainment at upstream meniscus depend on the liquid properties such as viscosity and surface tension and coating conditions such as web tension and wrap angle of web. As a result, wet film instability also depends on liquid properties and coating conditions. It was found that air stagnation causes streaks on the wet film and air entrainment caused bubbles on the wet film. To get a stable wet film, it was found that suitable viscosity and high surface tension were needed. / TOYOBO

High operation speeds and thin coating films are desirable in many industrial applications. But the quality of the product, which is primarily determined by an optimum process window, is affected by non-uniformities and instabilities originating at higher operation speeds. Unlike other academic works, because of associated industrial relevance, particular attention was given towards the use of industrially relevant coating systems or generation of model fluids, which replicate the real coating solutions. One of the novelties of the research proposed lie in an integrated approach, utilising a range of comparative rheometrical techniques, with a focus on measurement of: (i) high strain rate shear viscosity [η], (ii) high strain rate uniaxial extensional viscosity [ηE] (iii) high strain rate elasticity (N1). Deformable roll coating, in terms of classification, is the ultimate metered coating flow. The flow is controlled by the combination of hydrodynamic force and elastic deformation effect, which could be complicated by the presence of non-Newtonian fluid. This study necessitated the design and construction of a sophisticated deformable coating rig with the ability to operate over a wide range of conditions. Although the irregularities and instabilities associated with the roller coating process has been studied previously, the concerned speeds of operation in this study is around three times higher. The main objectives of this study was to carry out a comprehensive experimental programme establishing relationship exist between film thickness, film quality and operating parameters. Main identified operating parameters are roll speeds, roll gaps or applied load between the rolls, the elasticity with thickness of elastomeric layer and different rheological properties of the coating fluids. Surface instabilities and air entrainment are identified as the major limitations to being able to coat at higher speeds. / Tata Steel Europe / The full text was made available at the end of the embargo, 1st July 2020

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<p>Robotic platforms have several characteristics such as speed and precision that make them enticing for use in medical procedures. Companies such as Intuitive Medical and Titan Medical have taken advantage of these features to introduce surgical robots for minimally invasive procedures. Such robots aim to reduce procedure and patient recovery times. Current technology requires platforms to be master-slave manipulators controlled by a surgeon, effectively converting the robot into an expensive surgical tool. Research into the interaction between robotic platforms and deformable objects such as human tissue is necessary in the development of autonomous and semi-autonomous surgical systems. This thesis investigates a class of robust linear controllers based on a worst case performance measure known as the $H_{\infty}$ norm, for the purpose of performing so called Indirect Deformable Object Manipulation (IDOM). This task allows positional regulation of regions of interest in a deformable object without directly interacting with them, enabling tasks such as stabilization of tumors during biopsies or automatic suturing. A complete approach to generating linear $H_{\infty}$ based controllers is presented, from derivation of a plant model to the actual synthesis of the controller. The introduction of model uncertainty requires $\mu$ synthesis techniques, which extend $H_{\infty}$ designs to produce highly robust controller solutions. In addition to $H_{\infty}$ and $\mu$ synthesis designs, the thesis presents an approach to design an optimal PID controller with gains that minimize the $H_{\infty}$ norm of a weighted plant. The three control approaches are simulated performing set point regulation in $\text{MATLAB}^{TM}$'s $simulink$. Simulations included disturbance inputs and noises to test stability and robustness of the approaches. $H_{\infty}$ controllers had the best robust performance of the controllers simulated, although all controllers simulated were stable. The $H_{\infty}$ and PID controllers were validated in an experimental setting, with experiments performed on two different deformable synthetic materials. It was found that $H_{\infty}$ techniques were highly robust and provided good tracking performance for a material that behaved in a relatively elastic manner, but failed to track well when applied to a highly nonlinear rubber compound. PID based control was outperformed by $H_{\infty}$ control in experiments performed on the elastic material, but proved to be superior when faced with the nonlinear material. These experimental findings are discussed and a linear $H_{\infty}$ control design approach is proposed.</p> / Master of Applied Science (MASc)

This research endeavor develops Isogeometric approach for analysis of composite structures and take advantage of higher order continuity, smoothness and variation diminishing property of Nurbs basis for stress analysis of composite and sandwich beams and plates. This research also computes stress concentration factor in a composite plate with a hole. Isogeometric nonlinear/linear finite element code is developed for static and dynamic analysis of laminated composite plates. Nurbs linear, quadratic, higher-order and k-refined elements are constructed using various refinement procedures and validated with numerical testing. Nurbs post-processor for in-plane and interlaminar stress calculation in laminated composite and sandwich plates is developed. Nurbs post-processor is found to be superior than regular finite element and in good agreement with the literature. Nurbs Isgoemetric analysis is used for stress analysis of laminated composite plate with open-hole. Stress concentration factor is computed along the hole edge and good agreement is obtained with the literature. Nurbs Isogeometric finite element code for free-vibration and linear dynamics analysis of laminated composite plates also obtain good agreement with the literature. Main highlights of the research are newly developed 9 control point linear Nurbs element, k-refined and higher-order Nurbs elements in isogeometric framework. Nurbs elements remove shear-locking and hourglass problems in thin plates in context of first-order shear deformation theory without the additional step and compute better stresses than Lagrange finite element and higher order shear deformation theory for comparatively thick plates i.e. a/h = 4. Also, Nurbs Isogeometric analysis perform well for vibration and dynamic problems and for straight and curved edge problems. / Ph. D.

The process of froth flotation relies on using air bubbles to collect desired mineral particles dispersed in aqueous media on the surface, while leaving undesirous mineral particles behind. For a particle to be collected on the surface of a bubble, the thin liquid films (or wetting films) of water formed in between must rupture. According to the Frumkin-Derjaguin isotherm, it is necessary that wetting films can rupture when the disjoining pressures are negative. However, the negative disjoining pressures are difficult to measure due to the instability and short lifetimes of the films. In the present work, two new methods of determining negative disjoining pressures have been developed. One is to use the modified thin film pressure balance (TFPB) technique, and the other is to directly determine the interaction forces using the force apparatus for deformable surfaces (FADS) developed in the present work. The former is designed to obtain spatiotemporal profiles of unstable wetting films by recording the optical interference patterns. The kinetic information derived from the spatiotemporal profiles were then used to determine the disjoining pressures using an analytical expression derived in the present work on the basis of the Reynolds lubrication theory. The technique has been used to study the effects of surface hydrophobicity, electrolyte (Al3+ ions) concentration, and bubble size on the stability of wetting films. Further, the geometric mean combining rule has been tested to see if the disjoining pressures of the wetting films can be predicted from the disjoining pressures of the colloid films formed between two hydrophobic surfaces and the disjoining pressures of the foam films formed between two air bubbles. The FADS is capable of directly measuring the interaction forces between air bubble and solid surface, and simultaneously monitoring the bubble deformation. The results were analyzed using the Reynolds lubrication theory and the extended DLVO theory to determine both the hydrodynamic and disjoining pressures. The FADS was used to study the effects of surface hydrophobicity and approach speeds. The results show that hydrophobic force is the major driving force for the bubble-particle interactions occurring in flotation. / Ph. D.

No / Axially loaded rubber blocks of long, thin rectangular and circular cross section whose ends are bonded to rigid plates are studied. Closed-form expressions, which satisfy exactly the governing equations and conditions based upon the classical theory of elasticity, are derived for the total axial deflection and stress distribution using a superposition approach. The corresponding relations are presented for readily calculating the apparent Young's modulus, Ea, the modified modulus, E'a, and the deformed lateral profiles of the blocks. From these, improved approximate elementary expressions for evaluating Ea and E'a are deduced. These estimates, and the precisely found values, agree for large values of the shape factor S, with those previously suggested, but also fit the experimental data more closely for small values of S. Confirmation is provided that the assumption of a parabolic lateral profile is invalid for small values of S.

Comment obtenir des données anatomiques pendant une neurochirurgie ? a été ce qui a guidé le travail développé dans le cadre de cette thèse. Les IRM sont actuellement utilisées en amont de l'opération pour fournir cette information, que ce soit pour le diagnostique ou pour définir le plan de traitement. De même, ces images pre-opératoires peuvent aussi être utilisées pendant l'opération, pour pallier la difficulté et le coût des images per-opératoires. Pour les rendre utilisables en salle d'opération, un recalage doit être effectué avec la position du patient. Cependant, le cerveau subit des déformations pendant la chirurgie, phénomène appelé Brain Shift, ce qui altère la qualité du recalage. Pour corriger cela, d'autres données pré-opératoires peuvent être acquises, comme la localisation de la surface corticale, ou encore des images US localisées en 3D. Ce nouveau recalage permet de compenser ce problème, mais en partie seulement. Ainsi, des modèles mécaniques ont été développés, entre autres pour apporter des solutions à l'amélioration de ce recalage. Ils permettent ainsi d'estimer les déformations du cerveau. De nombreuses méthodes existent pour implémenter ces modèles, selon différentes lois de comportement et différents paramètres physiologiques. Dans tous les cas, cela requiert un modèle anatomique patient-spécifique. Actuellement, ce modèle est obtenu par contourage manuel, ou quelquefois semi-manuel. Le but de ce travail de thèse est donc de proposer une méthode automatique pour obtenir un modèle du cerveau adapté sur l'anatomie du patient, et utilisable pour une simulation mécanique. La méthode implémentée se base sur les modèles déformables pour segmenter les structures anatomiques les plus pertinentes dans une modélisation bio-mécanique. En effet, les membranes internes du cerveau sont intégrées: falx cerebri and tentorium cerebelli. Et bien qu'il ait été démontré que ces structures jouent un rôle primordial, peu d'études les prennent en compte. Par ailleurs, la segmentation résultante de notre travail est validée par comparaison avec des données disponibles en ligne. De plus, nous construisons un modèle 3D, dont les déformations seront simulées en utilisant une méthode de résolution par Éléments Finis. Ainsi, nous vérifions par des expériences l'importance des membranes, ainsi que celle des paramètres physiologiques. / The general problem that motivates the work developed in this thesis is: how to obtain anatomical information during a neurosurgery?. Magnetic Resonance (MR) images are usually acquired before the surgery to provide anatomical information for diagnosis and planning. Also, the same images are commonly used during the surgery, because to acquire MRI images in the operating room is complex and expensive. To make these images useful inside the operating room, a registration between them and the patient's position has to be processed. The problem is that the brain suffers deformations during the surgery, in a process called brain shift, degrading the quality of registration. To correct this, intra-operative information may be used, for example, the position of the brain surface or US images localized in 3D. The new registration will compensate this problem, but only to a certain extent. Mechanical models of the brain have been developed as a solution to improve this registration. They allow to estimate brain deformation under certain boundary conditions. In the literature, there are a variety of methods for implementing these models, different equation laws used for continuum mechanic, and different reported mechanical properties of the tissues. However, a patient specific anatomical model is always required. Currently, most mechanical models obtain the associated anatomical model by manual or semi-manual segmentation. The aim of this thesis is to propose and implement an automatic method to obtain a model of the brain fitted to the patient's anatomy and suitable for mechanical modeling. The implemented method uses deformable model techniques to segment the most relevant anatomical structures for mechanical modeling. Indeed, the internal membranes of the brain are included: falx cerebri and tentorium cerebelli. Even though the importance of these structures is stated in the literature, only a few of publications include them in the model. The segmentation obtained by our method is assessed using the most used online databases. In addition, a 3D model is constructed to validate the usability of the anatomical model in a Finite Element Method (FEM). And the importance of the internal membranes and the variation of the mechanical parameters is studied.