The Gawler Craton in South Australia consists of an Archaean to Palaeoproterozoic core surrounded and intruded by a series of Palaeo- to Mesoproterozoic metasediments and igneous suites. The region has experienced a protracted c. 1700 Myr tectonic history from the Archaean through to the Mesoproterozoic, experiencing numerous cycles of deformation, magmatism and basin development. Despite hosting a number of mineral deposits, including the immense Olympic Dam iron oxide-copper-gold deposit, the tectonothermal evolution of the Gawler Craton remains poorly constrained. A significant ambiguity in our current understanding of the geological framework of the Gawler Craton revolves around the timing and spatial distribution of the tectonic events within the craton and their metamorphic evolution. This study addresses some of this ambiguity by unravelling the timing and tectonothermal evolution of the reworked southern Gawler Craton, using a combination of structural and metamorphic analysis, coupled with targeted geochronology. These methods have been applied to three locations representing different lithologies across the southern Gawler Craton. Putting absolute time into structural and metamorphic analysis is a vital tool for unravelling the development of ancient and modern orogenic systems. Electron Probe Micro-Analysis (EPMA) chemical dating of monazite provides a useful method of obtaining good precision age data from monazite bearing assemblages. This technique was developed at the University of Adelaide in order to constrain the timing of reworked assemblages from the southern Gawler Craton. EPMA measurements carried out on samples of known age, from Palaeoproterozoic to Ordovician, produce ages which are within error of the isotopically determined ages, indicating the validity of the developed setup. This technique, together with SHRIMP monazite and titanite and garnet Sm-Nd geochronology, was used on selected samples from the southern Gawler Craton to determine the timing of high-grade metamorphism and deformation. The results show that the Sleaford Complex records evidence of an early D₁event during the c. 2450 Ma Sleaford Orogeny recorded within structural boudins. The majority of the data indicates that the region underwent subsequent reworking and thorough overprinting during the 1725–1690 Ma Kimban Orogeny. In the Coffin Bay region, Palaeoproterozoic peraluminous granites of the Dutton Suite are reworked by a series of migmatitic and mylonitic shear zones during the Kimban Orogeny. Peak metamorphic conditions recorded in mafic assemblages indicate conditions of 10 kbar at 730°C. The post-peak evolution is constrained by partial to complete replacement of garnet – clinopyroxene bearing mafic assemblages by hornblende – plagioclase symplectites, which record conditions of c. 6 kbar at 700°C, implying a steeply decompressional exhumation path. The Shoal Point region consists of a series of reworked granulite-facies metapelitic and metaigneous units which belong to the late Archaean Sleaford Complex. Structural evidence indicates three phases of fabric development with D₁retained within boudins, D₂consisting of a series upright open to isoclinal folds producing an axial planar fabric and D₃, a highly planar vertical high-strain fabric which overprints the D₂ fabric. Geochronology constrains the D₁ event to the c. 2450 Ma Sleafordian Orogeny while the D₂the D₃events are constrained to the 1730–1690 Ma Kimban Orogeny. P-T pseudosections constrain the metamorphic conditions for the Sleafordian Orogeny to between 4.5–6 kbar and 750–780 °C. Subsequent Kimban-aged reworking reached peak metamorphic conditions of 8–9 kbar at 820–850 °C during the D₂ event. Followed by near isothermal decompression to metamorphic conditions <6 kbar and 790–850 °C associated with the development of the D₃high-strain fabric. The Pt Neill and Mine Creek regions are located in the core and on the flank of the crustal scale Kalinjala Shear Zone, which forms the main structural element of the poorly exposed Kimban Orogen. Samples record a similar structural development with a dextrally transpressive system resulting in a layer parallel migmatitic gneissic to mylonitic KS₁ fabric which was subsequently deformed and reworked by upright folds and discrete KD₂ east-side-down sub-solidus mylonitic shear zones during east-west compression. Geochronology constrains the timing of deformation and metamorphism to the Kimban Orogeny between 1720 and 1700 Ma. Metamorphic P-T analysis and pseudosections constrain the peak M₁ conditions in the core of the shear zone to 10–11 kbar at c. 800 °C reflecting lower crustal conditions at depths of up to 30 km. On the flank of the shear zone the M₁ conditions reached 6–7 kbar at 750 °C followed by sub-solidus reworking during KD₂ at conditions of 3–4 kbar at 600–660 °C, suggesting a maximum burial of <24 km. Cooling rates suggest that the core of the shear zone cooled at rates in excess of 40–80 °CMa⁻¹ while the flank underwent much slower cooling at < 10°CMa⁻¹. The rapid cooling and inferred decompression in the core of the shear zone reflects rapid burial and exhumation of lower-crustal material into the mid-crust along the Kalinjala Shear Zone. The absence of evidence for extension indicates that differential exhumation and the extrusion of lower-crustal material into the mid-crust was driven by transpression along the shear zone and highlights the role of transpression in creating large variations in vertical exhumation over relatively short lateral extents. Garnet is a vital mineral for determining constrained P-T-t paths as it can give both the P-T and t information directly. However, estimates of the closure temperature of the Sm-Nd system in garnet vary considerably leading to significant uncertainties in the timing of peak conditions. Five igneous garnets of varying size from an undeformed 2414 ± 6 Ma garnet – cordierite bearing s-type granite from the Coffin Bay region, that were subjected to high-T reworking during the Kimban Orogeny, have been dated to examine their diffusional behaviour in the Sm-Nd system. Garnets were compositionally profiled and then dated. A direct correlation exists between grain size and amount of resetting highlighting the effect of grain size on closure temperature. Major element and REE traverses reveal homogonous major element profiles and relict igneous REE profiles. The retention of REE zoning and homogenisation of major element zoning suggests that diffusion rates of REE’s are considerably slower than that of the major cations, in disagreement with recent experimental determinations of the diffusion rates of REE in garnet. The retention of REE zoning and the lack of resetting in the largest grains suggests that Sm-Nd closure temperature in garnet is a function of grain-size, thermal history and REE zoning in garnet. The findings of this study provide the first temporally constrained tectonothermal model of the evolution of the southern Gawler Craton. The P-T conditions obtained from the earliest D₁ fabric provide the first quantitative constraints on the P-T conditions of the southern Sleafordian Orogeny. The P-T-t evolution determined for the 1725–1690 Ma Kimban Orogeny indicate it developed along a clockwise P-T path, and dominates the structural and metamorphic character of the southern Gawler Craton. The large variations in exhumation over short lateral extents reflect the exhumation of lower crustal rocks during the Kimban Orogeny driven by transpression during the development of a regional transpressional ‘flower structure’. / http://proxy.library.adelaide.edu.au/login?url= http://library.adelaide.edu.au/cgi-bin/Pwebrecon.cgi?BBID=1372052 / Thesis (Ph.D.) - University of Adelaide, School of Earth and Environmental Sciences, 2009

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The Gawler Craton in South Australia consists of an Archaean to Palaeoproterozoic core surrounded and intruded by a series of Palaeo- to Mesoproterozoic metasediments and igneous suites. The region has experienced a protracted c. 1700 Myr tectonic history from the Archaean through to the Mesoproterozoic, experiencing numerous cycles of deformation, magmatism and basin development. Despite hosting a number of mineral deposits, including the immense Olympic Dam iron oxide-copper-gold deposit, the tectonothermal evolution of the Gawler Craton remains poorly constrained. A significant ambiguity in our current understanding of the geological framework of the Gawler Craton revolves around the timing and spatial distribution of the tectonic events within the craton and their metamorphic evolution. This study addresses some of this ambiguity by unravelling the timing and tectonothermal evolution of the reworked southern Gawler Craton, using a combination of structural and metamorphic analysis, coupled with targeted geochronology. These methods have been applied to three locations representing different lithologies across the southern Gawler Craton. Putting absolute time into structural and metamorphic analysis is a vital tool for unravelling the development of ancient and modern orogenic systems. Electron Probe Micro-Analysis (EPMA) chemical dating of monazite provides a useful method of obtaining good precision age data from monazite bearing assemblages. This technique was developed at the University of Adelaide in order to constrain the timing of reworked assemblages from the southern Gawler Craton. EPMA measurements carried out on samples of known age, from Palaeoproterozoic to Ordovician, produce ages which are within error of the isotopically determined ages, indicating the validity of the developed setup. This technique, together with SHRIMP monazite and titanite and garnet Sm-Nd geochronology, was used on selected samples from the southern Gawler Craton to determine the timing of high-grade metamorphism and deformation. The results show that the Sleaford Complex records evidence of an early D₁event during the c. 2450 Ma Sleaford Orogeny recorded within structural boudins. The majority of the data indicates that the region underwent subsequent reworking and thorough overprinting during the 1725–1690 Ma Kimban Orogeny. In the Coffin Bay region, Palaeoproterozoic peraluminous granites of the Dutton Suite are reworked by a series of migmatitic and mylonitic shear zones during the Kimban Orogeny. Peak metamorphic conditions recorded in mafic assemblages indicate conditions of 10 kbar at 730°C. The post-peak evolution is constrained by partial to complete replacement of garnet – clinopyroxene bearing mafic assemblages by hornblende – plagioclase symplectites, which record conditions of c. 6 kbar at 700°C, implying a steeply decompressional exhumation path. The Shoal Point region consists of a series of reworked granulite-facies metapelitic and metaigneous units which belong to the late Archaean Sleaford Complex. Structural evidence indicates three phases of fabric development with D₁retained within boudins, D₂consisting of a series upright open to isoclinal folds producing an axial planar fabric and D₃, a highly planar vertical high-strain fabric which overprints the D₂ fabric. Geochronology constrains the D₁ event to the c. 2450 Ma Sleafordian Orogeny while the D₂the D₃events are constrained to the 1730–1690 Ma Kimban Orogeny. P-T pseudosections constrain the metamorphic conditions for the Sleafordian Orogeny to between 4.5–6 kbar and 750–780 °C. Subsequent Kimban-aged reworking reached peak metamorphic conditions of 8–9 kbar at 820–850 °C during the D₂ event. Followed by near isothermal decompression to metamorphic conditions <6 kbar and 790–850 °C associated with the development of the D₃high-strain fabric. The Pt Neill and Mine Creek regions are located in the core and on the flank of the crustal scale Kalinjala Shear Zone, which forms the main structural element of the poorly exposed Kimban Orogen. Samples record a similar structural development with a dextrally transpressive system resulting in a layer parallel migmatitic gneissic to mylonitic KS₁ fabric which was subsequently deformed and reworked by upright folds and discrete KD₂ east-side-down sub-solidus mylonitic shear zones during east-west compression. Geochronology constrains the timing of deformation and metamorphism to the Kimban Orogeny between 1720 and 1700 Ma. Metamorphic P-T analysis and pseudosections constrain the peak M₁ conditions in the core of the shear zone to 10–11 kbar at c. 800 °C reflecting lower crustal conditions at depths of up to 30 km. On the flank of the shear zone the M₁ conditions reached 6–7 kbar at 750 °C followed by sub-solidus reworking during KD₂ at conditions of 3–4 kbar at 600–660 °C, suggesting a maximum burial of <24 km. Cooling rates suggest that the core of the shear zone cooled at rates in excess of 40–80 °CMa⁻¹ while the flank underwent much slower cooling at < 10°CMa⁻¹. The rapid cooling and inferred decompression in the core of the shear zone reflects rapid burial and exhumation of lower-crustal material into the mid-crust along the Kalinjala Shear Zone. The absence of evidence for extension indicates that differential exhumation and the extrusion of lower-crustal material into the mid-crust was driven by transpression along the shear zone and highlights the role of transpression in creating large variations in vertical exhumation over relatively short lateral extents. Garnet is a vital mineral for determining constrained P-T-t paths as it can give both the P-T and t information directly. However, estimates of the closure temperature of the Sm-Nd system in garnet vary considerably leading to significant uncertainties in the timing of peak conditions. Five igneous garnets of varying size from an undeformed 2414 ± 6 Ma garnet – cordierite bearing s-type granite from the Coffin Bay region, that were subjected to high-T reworking during the Kimban Orogeny, have been dated to examine their diffusional behaviour in the Sm-Nd system. Garnets were compositionally profiled and then dated. A direct correlation exists between grain size and amount of resetting highlighting the effect of grain size on closure temperature. Major element and REE traverses reveal homogonous major element profiles and relict igneous REE profiles. The retention of REE zoning and homogenisation of major element zoning suggests that diffusion rates of REE’s are considerably slower than that of the major cations, in disagreement with recent experimental determinations of the diffusion rates of REE in garnet. The retention of REE zoning and the lack of resetting in the largest grains suggests that Sm-Nd closure temperature in garnet is a function of grain-size, thermal history and REE zoning in garnet. The findings of this study provide the first temporally constrained tectonothermal model of the evolution of the southern Gawler Craton. The P-T conditions obtained from the earliest D₁ fabric provide the first quantitative constraints on the P-T conditions of the southern Sleafordian Orogeny. The P-T-t evolution determined for the 1725–1690 Ma Kimban Orogeny indicate it developed along a clockwise P-T path, and dominates the structural and metamorphic character of the southern Gawler Craton. The large variations in exhumation over short lateral extents reflect the exhumation of lower crustal rocks during the Kimban Orogeny driven by transpression during the development of a regional transpressional ‘flower structure’. / http://proxy.library.adelaide.edu.au/login?url= http://library.adelaide.edu.au/cgi-bin/Pwebrecon.cgi?BBID=1372052 / Thesis (Ph.D.) - University of Adelaide, School of Earth and Environmental Sciences, 2009

Kyrgyzstan is the single most seismically active country in the world. Accessing the past, and therefore future hazard of faults, necessitates a high-resolution understanding of the timing of different geologic events. With no radiometrically datable rocks from the Neogene of Kyrgyzstan, I herein present the first work formally describing Neogene vertebrate faunas from the Kochkor Basin of Kyrgyzstan. I utilize a combination of biostratigraphy and magnetostratigraphy to constrain the timing of when the vertebrate assemblages were emplaced, and have dated the three bone beds to all fall in the latest Miocene, spanning 9-5 million years ago. All four bone beds represent mass death assemblages, inferred to be from drought-caused mortality. The timing of the deposits corresponds to uplift in the Pamirs, Himalayan, and greater Tibetan Plateau, which would have blocked the Indian monsoon from reaching Central Asia, forever altering the climate and biota of the region. This change is reflected in the shifting mammals faunas, as evidenced by the novel rhinocerotid I describe in a phylogeographic context.

abstract: The collision of India and Eurasia constructed the Himalayan Mountains. Questions remain regarding how subsequent exhumation by climatic and tectonic processes shaped the landscape throughout the Late Cenozoic to create the complex architecture observed today. The Mount Everest region underwent tectonic denudation by extension and bestrides one of the world’s most significant rain shadows. Also, glacial and fluvial processes eroded the Everest massif over shorter timescales. In this work, I review new bedrock and detrital thermochronological and geochronological data and both one- and two-dimensional thermal-mechanical modeling that provides insights on the age range and rates of tectonic and erosional processes in this region. A strand of the South Tibetan detachment system (STDS), a series of prominent normal-sense structures that dip to the north and strike along the Himalayan spine, is exposed in the Rongbuk valley near Everest. Using thermochronometric techniques, thermal-kinematic modeling, and published (U-Th)/Pb geochronology, I show exhumation rates were high (~3-4 mm/a) from at least 20 to 13 Ma because of slip on the STDS. Subsequently, exhumation rates dropped drastically to ≤ 0.5 mm/a and remain low today. However, thermochronometric datasets and thermal-kinematic modeling results from Nepal south of Everest reveal a sharp transition in cooling ages and exhumation rates across a major knickpoint in the river profile, corresponding to the modern-day Himalayan rainfall transition. To the north of this transition, exhumation histories are similar to those in Tibet. Conversely, < 3 km south of the transition, exhumation rates were relatively low until the Pliocene, when they increased to ~4 mm/a before slowing at ~3 Ma. Such contrasting exhumation histories over a short distance suggest that bedrock exhumation rates correlate with modern precipitation patterns in deep time, however, there are competing interpretations regarding this correlation. My work also provides insights regarding how processes of glacial erosion act in a glacio-fluvial valley north of Everest. Integrated laser ablation U/Pb and (U-Th)/He dating of detrital zircon from fluvial and moraine sediments reveal sourcing from distinctive areas of the catchment. In general, the glacial advances eroded material from lower elevations, while the glacial outwash system carries material from higher elevations. / Dissertation/Thesis / Doctoral Dissertation Geological Sciences 2017

The Tatric crystalline unit of the Western Carpathians in northern Slovakia displays an inverted metamorphic sequence where high-grade migmatite and orthogneiss units are overlying lower-grade mica schists. Enclosed within the migmatites are lenses of eclogite-bearing amphibolites. Conventional geothermobarometry coupled with isochemical modeling constrained P-T paths that exhibit contrasting metamorphic histories for rock units that are now heterogeneously interleaved. Relict eclogite facies assemblages with occasionally preserved omphacite record post-peak pressure conditions of 1.7-1.8 GPa followed by near isothermal decompression at ~750 °C leading to intensive re-equilibration of eclogites at high-pressure granulite facies conditions and development of diopside + plagioclase symplectitic textures. New ID-TIMS Sm-Nd dating of garnet separated from the omphacite-bearing eclogite yields a whole rock-garnet isochron age of 337 ± 10 Ma, with an epsilon Nd isotopic composition of +8.3. While major element profiles across the garnets display little variation, the trace element distribution shows a typical HREE enrichment profile and a slight core to rim disparity with LREE and MREE concentrations higher in the cores and higher HREE in the rims. Granulite-facies migmatites that host the eclogite boudins record lower pressure metamorphic conditions of 1.2 GPa at ~750 °C and a similar retrograde path. The lower-grade micaschists reached metamorphic conditions of 0.8 GPa at ~650 °C. Monazite U-Pb analysis from a migmatite surrounding the eclogite boudins yields one population of ca. 380 Ma age. Another migmatite away from the eclogite yields two populations monazite ages. A robust 340 ± 11 Ma monazite U-Pb age is indistinguishable from our garnet age and U-Pb SIMS age of zircons in the anatectic leucosome of the migmatite (347 ± 7 Ma). We interpret the ca. 340 Ma ages to represent the exhumation of the deep crustal root of the Variscan orogen into the middle crust coeval with anatexis. A younger monazite U-Pb age of 300 ± 16 Ma is consistent with 40Ar/39Ar thermochronology data of ca. 310 Ma that is likely indicative of the Late Carboniferous I-type magmatism and cooling in the Tatric block. Cooling rates calculated by garnet diffusion modeling yield estimates of ~30 °/Ma. This exhumation was likely tectonically forced by the action of a rigid indentor which prompted the weak lower crust to be heterogeneously extruded to mid-crustal levels at a time coeval with anatexis and subsequently extruded with mid-crustal material to the upper crust.

The Archean North Caribou greenstone belt (NCGB) possesses abundant transpressive deformation zones on its northern margins, which appear to have formed under amphibolite facies conditions. Protracted deformation and regional metamorphism are coeval with widespread magmatism and accretion events in the Superior Province, yet the importance of these shear zones in the tectonic evolution of the NCGB is equivocal. Structural analyses support a transpressive system that strongly implicates horizontal tectonism. This is partly in contrast with some currently proposed models for Archean greenstone belts suggesting synchronous vertical and horizontal movements. Geochemical and microstructural analyses from shear zones indicate heterogeneous deformation/fluids conditions on a km-scale. Monazite and mica geochronological ages indicate metamorphism and deformation occurring during the amalgamation of the Superior craton from ca. 2.75 to 2.4 Ga. The high metamorphic grade background may obscure tectonic signatures, yet some structural and geochemical characteristics remain consistent with other greenstone belts where vertical and horizontal displacement are recorded.

High precision 147Sm-143Nd geochronology of garnet is performed in two localities to solve problems in tectonics. In Chapter 1, the age of the basal amphibolite unit of the Ballantrae Ophiolite complex in Scotland is dated at 477.6 ± 1.9 million years old. This age constrains the duration of Grampian orogenesis to 12.6 ± 3.1 million years and allows us to conclude that classic metamorphism by overthickening of continental crust cannot account for the very short-lived event in this region. In Chapter 2, we report ages from a Variscan relict (318 ± 130 Ma) to a range of Cenozoic ages from 35.5 ± 2.1 Ma to 9 ± 10 Ma in the Betic Cordillera of southern Spain. This alone indicates prolonged orogenesis in the region. These ages are linked directly to a microstructure known as a Foliation Intersection Axis (FIA). Results are inconclusive, but they generally indicate that there may be a relationship between broad scale plate motion and FIA orientations at a regional scale.

Philosophiae Doctor - PhD / The Sandamap gold prospect is a metaturbidite shear zone-hosted gold mineralization located in the Neoproterozoic Damara Orogen 30 km northwest of the town of Usakos in Namibia with an estimated gold content of 240 000 t at 3.6 g/t up to 40 m below surface. This research project was aimed at constraining the age, crustal level of formation, pressure-temperature conditions during formation, sources of the mineralizing fluids, and by implication, the metal sources of the Sandamap gold mineralization. Fluid inclusion, geochronological and isotopic studies were carried out on quartz veins hosting the ore. The presence of kaolinite, alunite and jarosite suggest post-hydrothermal weathering of sulfides. Various sources of data from this study, giving rise to depths of entrapment of 4 to 14 km, temperature range of entrapment of fluids of 187 – 594 °C, stable isotope data (δ13C and δ18O), δD values and a δD vs. δ18OH2O plot are all in favour of an orogenic gold deposit. Additionally, the dominant CO2-rich and CH4-rich fluids observed at Sandamap do not contradict this interpretation. The calculated depth of entrapment of mineralization covers the lower portion of the epizonal zone to the upper portion of the hypozonal zone of gold deposits. The Sandamap mineralization’s δD values of -35‰ to -49‰ fall within the range of most published data for typical orogenic gold deposits which varies from -20 to -80‰. Moreover, the calculated δ18Owater values of the ore-fluids (+6.6 to +11.3‰) of the higher temperature aqueous group from the Sandamap mineralization fall within the range observed in typical orogenic gold deposits found in Phanerozoic terrains (+7 to +13‰). The schist hosting the mineralized shear zone with a gold content of 0.05 ppm Au or its higher grade equivalent at depth, is a possible gold source candidate. Two mechanisms of deposition were possibly at play: (i) the cooling below 500 °C and possible sulfidation (resulting from fluid-rock interaction), lowered the solubility of pyrite causing S3- and Au(HS)S3- (possible main Au carriers) to breakdown resulting in decreased Au solubility and its subsequent deposition and (ii) the elevated amount of CO2 (e.g. trench 14 where CO2-rich fluid inclusions are dominant) led to a sharp decrease in the Au(HS)2- and Au(HS)S3- concentrations, causing decreased Au solubility and its subsequent deposition. The age of mineralization obtained from 40Ar/39Ar dating of the muscovite associated with the ore-hosting quartz veins is placed at 472 ± 3 Ma. The mineralization is younger than the shear zone, which acted as a conduit for ore-fluid migration and it has no age relationship with proximal plutonic bodies. The mineralization is younger than the foliated granite (FG), which exhibits a metamorphic fabric in the form of mineral segregation, but older than the non-foliated granite (GT) which hosts a mineralized xenolith.

Constraining the depositional age of Neoproterozoic stratigraphy in western North America has implications for correlating global glaciation and tectonic events. The depositional ages of the Neoproterozoic Mutual and Browns Hole formations of northern Utah are controlled by two conflicting datapoints. However, new U-Pb geochronological data from 95 detrital apatite grains refines the maximum depositional age of the volcanic member of the Browns Hole Formation to 613 ± 12 Ma (2σ). This places new restrictions on the time available for the deposition of underlying units. Due to debate regarding the age models for underlying stratigraphy, two scenarios for sediment accumulation rates are explored. These results highlight a need for further exploring regional unconformities. Evidence for several post-depositional fluid-rock interaction events are observed in the Mutual and Browns Hole formations. Cross-cutting relationships identified via petrography, scanning electron microscopy, and electron microprobe analysis show at least seven fluid mediated events: (1) early grain-rimming hematite cement, (2) quartz overgrowth and cement development, (3) feldspar dissolution, (4) phosphate dissolution, (5) partial quartz dissolution, (6) authigenic mineral precipitation in cluding clays, sericite, monazite, and apatite cement, and (7) later hematite cementation. Constraining the timing of these events is challenging due to a limited of datable material. Using basic geochemical modeling and consideration of expected mineral formation conditions, a paragenetic sequence is placed into context of the known geologic history.