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Degradační testy polymerních materiálů vystavených klimatickým podmínkám / Degradation test of polymer materialChleboun, Jiří January 2013 (has links)
Basic knowledge of photovoltaic energy transformation, devices and materials, used in photovoltaics are summarized in this master’s thesis. Sort of degradation factors and its consequences of the photovoltaic panels are described there. Detail reviews of degradation tests are processed at the end of theoretical part. The main purpose of this research is selected covering materials dielectric properties change monitoring. These covering materials were influenced of accelerated thermal aging and increased humidity.
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Influence of the Non-linear Effects in the Design of Viscous Dampers for Bridge CablesAcar, Yalda, Jingstål, Pontus January 2014 (has links)
In this master thesis the performance of external viscous dampers attached to cables in cable-stayed bridges have been studied. A comparison has been performed between a linear and a non-linear cable model. The comparison was carried out for two bridge cables, one from the Dubrovnik Bridge and the other from the Normandie Bridge. The performance of the dampers have been measured in terms of maximum achieved damping ratio and minimum amplitude of vibration. The analysis was performed using the finite element method. The damping ratio was measured using both the half-power bandwidth method and by calculating the loss factor. The half-power bandwidth method can only be applied to a linear system. Therefore, the loss factor was evaluated for the linear model and compared to the results obtained using the half-power bandwidth method. From the comparison, it was concluded that the damping ratio evaluated using the loss factor was similar to the results obtained when using the half-power bandwidth method. However, when calculating the loss factor, it was of great importance that the resonance frequency of the system was accurately determined. The loss factor was then calculated for the non-linear model and compared to the results obtained for the linear model. Since the loss factor measures the energy dissipated in a system, it could be utilised for the non-linear model. When computing the strain energy for the non-linear model an approximate method was used to take into consideration the strain energy caused by the static deformation of the cable. From the comparison between the linear and non-linear cable models, it was concluded that the optimal damper coefficients obtained by both models are not significantly different. However, there is an uncertainty in the results due to the fact that an approximate method was used when calculating the strain energy for the nonlinear model. It was also observed that a very accurate evaluation of the system’s resonance frequency was needed to calculate the loss factor. It was also observed that the variation in amplitude of vibration for varying damper coefficient was small for all modes of vibration for the Dubrovnik Bridge Cable as well as for the first mode of vibration for the Normandie Bridge Cable. The difference in the results between the two bridge cables needs to be investigated further in order to get a better understanding of the results.
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Evaluating Thermal and Mechanical Properties of Electrically Conductive Adhesives for Electronic ApplicationsXu, Shuangyan 26 April 2002 (has links)
The objective of this study was to evaluate and gain a better understanding of the short-term impact performance and the long-term durability of electrically conductive adhesives for electronic interconnection applications. Three model conductive adhesives, designated as ECA1, ECA2 and ECA3, supplied by Emerson & Cuming, were investigated, in conjunction with printed circuit board (PCB) substrates with metallizations of Au/Ni/Cu and Cu, manufactured by Triad Circuit Inc.
Effects of environmental aging on the durability of conductive adhesives and their joints were evaluated. All the samples for both mechanical tests and thermal tests were aged at 85%, 100%RH for periods of up to 50 days. Studies of bulk conductive adhesives suggested that both plasticization, which is reversible and further crosslinking and thermal degradation, which are irreversible, might have occurred upon exposure of ECAs to the hot/wet environment. The durability of electrically conductive adhesive joints was then investigated utilizing the double cantilever beam (DCB) test. It was observed that the conductive adhesive joint was significantly weakened following hydrothermal aging, and there was a transition from cohesive failure to interfacial failure as aging continued. A comparative study of the durability of different conductive adhesive and substrate metallization combinations suggested that the resistance of the adhesive joints to moisture attack is related to the adhesive properties, as well as the substrate metallizations. It was noted that the gold/adhesive interface had better resistance to moisture attack than the copper/adhesive interface. A reasonable explanation of this phenomenon was given based upon the concept of surface free energy and interfacial free energy. XPS analysis was performed on the fractured surfaces of DCB samples. For adhesive joints with copper metallization, copper oxide was detected on the failed surfaces upon exposure of the conductive adhesive joints following aging. XPS analysis on the fractured surfaces of adhesive joints with Au metallization suggested that diffusion of Cu to the Au surface might have happened on the Au/Ni/Cu plated PCB substrates during aging.
The impact performance of conductive adhesives was quantitatively determined using a falling wedge test. This unique impact resistance testing method could serve as a useful tool to screen conductive adhesives at the materials level for bonding purpose. Moreover, this test could also provide some useful information for conductive adhesive development. This study revealed that the viscoelastic energy, which is a result of the internal friction created by chain motions within the adhesive material, played an important role in the impact fracture behavior of the conductive adhesives. This study also demonstrated that the loss factor, evaluated at the impact environment conditions, is a good indicator of a conductive adhesive's ability to withstand impact loading. / Ph. D.
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NOVEL SOLIS STATE PROPERTIES OF DRUGS, POLYMERS AND VARIOUS CHEMICALS BY THERMAL AND ANALYTICAL TECHNIQUESMantheni, Dhruthiman Reddy January 2012 (has links)
No description available.
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Výpočtové modelování vysokofrekvenčního hluku v kabině letounu EV-55M / Computational modelling of high-frequency noise inside cabin of aircraft EV-55MStraka, Martin January 2013 (has links)
This thesis describes methods of high frequency noise and vibrations computation of cabin part of EV–55M (aircraft developed by Evektor Kunovice). There is a brief summary of methods used for determining high frequency noise and vibrations in the first part of the thesis. Detailed explanation is given for Statistical Energy Analysis (SEA) which is nowadays the most dominant method in this area. The energy balance equation is derived in this chapter and SEA parameters such as modal density, damping loss factor, coupling loss factor and power input are introduced here. Next part deals with main noise sources of propeller driven and jet aircraft and passive and active noise controls are discussed. Practical part of this thesis deals with modeling aircraft EV–55M fuselage using VA One SEA module. Two models were created. First of them is only an outside fuselage with aircraft flooring and the second one is extended by interior trim panels and is applicable for simulation of noise control treatments. Computational modeling is accompanied by experimental measurement of passive noise control material characteristics. Postprocessing of information obtained from impedance tube measurement was performed in FOAM – X. Determined characteristics of porous material were used as inputs to VA One and reduction of sound pressure level in fuselage cavities by using noise control treatment was found. In conclusion there is a summary of noise transmission paths from sources to interior cavity and some treatments of them are simulated
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Vliv etherů celulózy na reologické vlastnosti vápna / Influence of cellulose ethers on rheological properties of limeHegrová, Michaela January 2018 (has links)
The subject of this diploma thesis is a study of the influence of cellulose ethers on the rheological properties of lime. The theoretical part focuses on rheological parameters, techniques and test equipment used in rheology measurements. Various types of cellulose ethers and their influence on the rheological properties of fresh mortars are described. The practical part deals with the study of the influence of different types and quantities of cellulose ethers on the properties of fresh lime pastes and mortars. The results were obtained from measurements on a rotational rheometer with a special geometry for building materials. Measuring methods used were flow and oscillatory tests. Yield stress, viscosity and flow index were determined by the flow measurement. The stability and stiffness of fresh materials were determined during the oscillation measurements. The measured results are then evaluated and compared.
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Měření elektrických parametrů vysokonapěťových komponentů pomocí elektronického můstku / Measurement of HV equipments by electronic bridge.Kumičák, Ivan January 2019 (has links)
The main idea of this thesis is measurements of dielectric materials by using a device Tettex. The thesis is about basic physic properties of dielectric materials. The determination of a dielectric material is considered. The behavior of these materials in electrical fields and reasons, those can have an influence on it, are considered as well. In the text are described measuring methods of chosen parameters of dielectric materials by device Tettex and its functional principles. There are an evaluation of measurements, which were done, and a discussion about achieved results.
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Dielektrické vlastnosti epoxidové pryskyřice plněné nanočásticemi / Dielectric properties of epoxy with nano particleRáček, Tomáš January 2010 (has links)
This diploma thesis is focused on the analysis of basic problematics of dielectrics and nanocomposites. It describes the fabrication of experimental samples of nanocomposites from sealing epoxy resin and nanoparticles of titanium dioxide with various weight filling. Further, the thesis deals with measuring and evaluation of dielectric properties of the samples. It examines the influence of weight filling, temperature and frequency of the electric field on volume resistivity, relative permitivity and loss factor.
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Dielektrická relaxační spektroskopie kompozitních soustav / Dielectric Relaxation Spectroscopy of Composite SystemsHolcman, Vladimír January 2008 (has links)
The subject of this doctoral thesis is the study of dielectric properties of a binary composite made up of a polymer matrix and metallic filler. Properties of such composites have been extensively examined in the past and they turned out to depend on temperature, frequency and in particular on filler concentration. The objective of this work was first to experimentally establish and second to describe quantitatively the effect of the size of metallic particles on the properties of the composite concerned, yet at the same filler concentration. This study was carried out on the model system ethylene-vinylacetate copolymer – nickel. The acquisition of experimental results required extensive measurements in a wide frequency and temperature interval, as well as a manufacture and preparation of a large set of samples with different concentrations and Ni filler sizes. Measurements were in part carried out at the Centre for Electronic Correlations and Magnetism, Institute of Experimental Physics V of the University of Augsburg (Germany) and, after the installation of a new cryogenic system, at the Department of Physics at FEEC, BUT Brno. Measurements were performed on a number of meters (Alpha-Analyzer of Novocontrol, HP4284A and HP4285A of Hewlett Packard and E4991A of Agilent) in the frequency range 1 Hz – 1 MHz and in the temperature interval 10 K – 300 K. The nickel concentration in systems studied varied from 0 % to 75 % and nickel particles were of a spherical shape with diameters between 35 and 115 m. The measurement results have shown that in the above frequency and temperature window just a single relaxation and a single conductivity mechanism occur. It was also proved that the frequency dependence of complex permittivity is for different Ni particle sizes at the same concentration different. These results have been quantified and a simple mathematical formula based on the Lichtenecker mixture rule has been proposed for their description. The physical origin of the effect of particle size at the same total nickel concentration is sought in different surface areas of internal interfaces between nickel and polymer in the composite
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Dielektrická spektroskopie karboxymetylcelulózy v časové oblasti / Time-domain Dielectric Spectroscopy of CarboxymethylcellulosePalai-Dany, Tomáš January 2009 (has links)
The dissertation deals with the time-domain dielectric relaxation spectroscopy of carboxymethylcellulose. The main attention was paid to the experimental part of research, mainly to the design and subsequent development of an experimental setup for the measurement of discharge currents and for their processing and analysis. The subject of the measurement is carboxymethylcellulose (CMC), which is a simple polysaccharide used in wide range of applications, among else also in biomedical engineering. The study of CMC properties has required the development of a new experimental set-up of original design, which includes the equilibration (short-circuiting) of a sample before the measurement, charging and discharging at defined time intervals, switching between these two modes, recording of measurement, adjustments and processing of measured signals up to Fourier transformation into the frequency domain and, finally, calculation of complex permittivity of the sample. The frequency dependence of complex permittivity or its imaginary part, obtained by Fourier transformation of discharge current in time domain, is then referred to as the dielectric spectrum. In view of the fact that current measurements were done at very low levels of measured signal (below 10-12 A) the whole measurement was no easy matter. The framework of the work also necessitated studies and subsequent resolution of problems associated with shielding, grounding, presence of noise and sensitivity to various ambient influences. The research work focused on a reliable and trustworthy measurement of very low discharge currents and, subsequently, mathematical processing of noise present in them, i.e., operations with the original, experimentally established signal in time domain, leading in principle to a digital filtration of measured dielectric data. A further pursued objective is the explanation of dielectric parameters of tested carboxymethylcellulose sample in the widest possible frequency spectrum. The integral part of the research was the selection and application of the method for the transformation of the adjusted signal to the frequency domain. The experimental works, including data processing, were carried out in the Department of Physics, Brno FEEC BUT. Measurements were done with Keithley 617 Electrometer, HP4284A Frequency Analyzer and Janis CCS-400-204 cryogenic system. The results were completed with results obtained at the V Department of Experimental Physics, Centre for Electronic Correlations and Magnetism, University of Augsburg, Germany.
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