Bien que l’amorçage de fissure joue un rôle important en fatigue, ses mécanismes ne sont pas encore pleinement compris. Des critères d'amorçage basés sur des mécanismes physiques de déformation plastique ont été proposés mais ne sont pas faciles à utiliser et à valider, car ils nécessitent des variables locales à l'échelle du grain. L'étude présente vise à établir un critère d'amorçage en fatigue oligocyclique, utilisable sous chargement d'amplitude variable.Le comportement mécanique de l'acier inoxydable AISI 316L étudié a été caractérisé en fatigue oligocyclique. Il a été modélisé par un schéma autocohérent utilisant une loi de plasticité cristalline basée sur l'évolution des densités de dislocations. L'endommagement de surface a été suivi pendant un essai de fatigue à l'aide d'un dispositif de microscopie optique in situ. Les fissures présentes après 2000 cycles ont été analysées et leurs caractéristiques cristallographiques calculées.Comme les grains de surface montrent une déformation plus importante à cause d'un moindre confinement par les grains voisins, il est nécessaire de définir une loi de localisation spécifique aux grains de surface. La forme proposée fait intervenir une variable d'accommodation intergranulaire, sur le modèle de la loi de localisation de Cailletaud-Pilvin. Elle a été identifiée à partir de simulations par éléments finis. L'état des contraintes et des déformations dans les grains de surface a alors été simulé. Des indicateurs d'amorçage potentiels ont ensuite été comparés sur une même base expérimentale. Deux indicateurs pertinents de l'endommagement en fatigue ont pu être obtenus. / Although crack initiation is proved to play an important role in fatigue, its mechanisms have not been fully understood. Some crack initiation criteria based on physical mechanisms of plastic deformation have been defined. However, these criteria are not easy to use and valid, as they need local variables at the grain scale. The present study aims at establishing a crack initiation criterion in low-cycle fatigue, which should be usable under variable amplitude loading conditions.Tension-compression fatigue tests were first carried out to characterize the mechanical behavior of the stainless steel AISI 316L studied. The mechanical behavior was simulated using a self-consistent model using a crystalline plastic law based on dislocation densities. The evolution of surface damage was observed during a fatigue test using an in situ optical microscopic device. Cracks were analyzed after 2000 cycles and their crystallographic characteristics calculated. As surface grains exhibit larger strain because they are less constraint by neighbor grains, a specific numerical frame is necessary to determine stress state in surface grains. A localization law specific to surface grains under cyclic loading was identified from finite element simulations. The proposed form needs an intergranular accommodation variable, on the pattern of the localization law of Cailletaud-Pilvin. Stress-strain state in surface grains was simulated. Potential indicators for crack initiation were then compared on a same experimental data base. Indicators based on the equivalent plastic strain were found to be suitable indicators of fatigue damage.

Un protocole expérimental a été développé dans cette thèse pour étudier l'influence de la microstructure héritée du procédé de fonderie dit Procédé à Modèle Perdu sur le comportement en fatigue oligocyclique des alliages Al-Si à température ambiante. Dans un premier temps, la microstructure des alliages étudiés a été caractérisée à la fois en 2D et en 3D. Les éprouvettes les plus appropriées et les plus représentatives et les régions d’intérêt où le suivi in-situ est réalisé (ROIs) ont été sélectionnées par une caractérisation préliminaire en tomographie aux rayons X. Cette caractérisation 3D est également nécessaire pour comprendre les mécanismes d’endommagement après rupture de l’éprouvette. Les observations in-situ réalisées en surface en utilisant un microscope longue distance (Questar) et en volume avec la tomographie aux rayons X permettent de suivre l’amorçage et la propagation des fissures et ainsi d'identifier la relation entre les mécanismes d’endommagement et les microstructures moulées. Les champs de déplacement et de déformation en 2D/3D mesurés à l'aide de la Corrélation d'Images Numériques et la Corrélation d’Images Volumiques permettent d'analyser la relation entre les champs mesurés et les mécanismes d'endommagement. L'analyse post-mortem et la simulation éléments finis ont permis de compléter l’analyse des mécanismes d’endommagement. Les grands pores favorisent l'amorçage de fissures car ils augmentent fortement le niveau de contrainte locale. Les inclusions dures (phase Si, intermétalliques au fer et phases au cuivre) jouent un rôle important dans l’amorçage et la propagation des fissures en raison des localisations de déformation sur ces inclusions / An experimental protocol was developed in this thesis in order to study the influence of casting microstructure on the fatigue behavior in Lost Foam Casting Al-Si alloys in tension and in Low Cycle Fatigue at room temperature. First of all, the microstructures of studied alloys were thoroughly characterized both in 2D and in 3D. The most suitable and representative specimens and Region of Interest (ROIs) where the in-situ monitoring was performed were selected through a preliminary characterization using X-ray tomography, which is also necessary to understand damage mechanisms after failure. In-situ observations performed on surface using Questar long distance microscope and in volume using X-ray tomography allow following cracks initiations and their propagations and thus allow identifying the relation between damage mechanisms and casting microstructure. 2D/3D displacement and strain fields measured using Digital Image Correlation and Digital Volume Correlation allows analyzing the relation between measured fields and damage mechanisms. Postmortem analysis and FEM simulation gave more information for the damage mechanisms. Large pores favor crack initiation as they strongly increase local stress level. Hard inclusions (Si phase, iron intermetallics and copper containing phases) also play an important role in crack initiation and propagation due to strain localizations at these inclusions

Multiple step tests under cyclic strain control have been performed using cylindrical specimens of cast polycrystalline Inconel 738LC superalloy at 23, 700, 500, 800 and 900 °C in laboratory atmosphere to obtain cyclic stress-strain curves. During cyclic straining of specimen were obtained cyclic hardening-softening curves. Their progress changed with temperature and strain amplitude. Evaluated cyclic stress-strain curves are shifted to lower stresses with increasing temperature. Surface relief was observed in fatigued specimens under SEM and metalography under optic microscopy. Slip markings were studied on specimen surface fatigued at 700 °C .Stress-strain response is compared and discussed in relation to the surface observations - persistent slip markings.

The main aim of this thesis is to define material parameters of Chaboche model of plasticity. Adjustment of the parameters has to correspond to the experimental datas. These datas are represented by an uniaxial strain controlled test curve for fewer than two cycles and also by cyclic stress-strain curve. After that, an cyclic tension-compresion test for various parameters of Chaboche´s model of plasticity is simulated in an ANSYS software. Finally, the most suitable configuration of Chaboche´s model of plasticity is used for cylindrical thick-walled body. Cylindrical body represents a simplified model of high-pressure tank of fuel (diesel) – rail in Common Rail system.

Ti-6Al-4V manufactured by electron beam melting Keywords: Additive manufacturing, high-temperature tensile properties, low cycle fatigue, neutron diffraction, fatigue crack growth ISBN: 978-91-89325-27-2 (Printed) 978-91-89325-26-5 (Electronic) Ti-6Al-4V is the most widely used α+β titanium alloy in aerospace engine applications due to its high specific strength. Typically, the alloy is manufactured as castings or forgings and then machined to final geometry. These conventional manufacturing processes do however generate a lot of waste material, whereas additive manufacturing (AM) can potentially produce a near-net-shape geometry directly from the feedstock. In the past decade, electron beam melting (EBM), one of the powder bed fusion techniques, has been widely researched to build Ti[1]6Al-4V components. Still, the as-built material can contain defects such as gas pores that require post-processing, such as hot isostatic pressing (HIP) to produce nearly fully dense components. HIP treatment of conventionally cast Ti-6Al-4V is normally performed at 920 ˚C, 100 MPa for 2 hours. This same HIP treatment has then been adapted also for EBM-manufactured Ti-6Al-4V, which however results in coarsening of α laths and reduction of yield strength. Therefore, finding a more appropriate HIP treatment for this new type of Ti-6Al-4V material, i.e. EBM manufactured, would be of great benefit for the industry. Lowering the HIP treatment temperature to 800 ˚C and increasing the pressure to 200 MPa has recently been proven to close the porosity to a high degree while sustaining the high yield strength. In this thesis, the high-temperature tensile properties of EBM-manufactured Ti[1]6Al-4V subjected to a low-temperature (800 ˚C) HIP treatment were evaluated and compared with standard HIP-treated (920 ˚C) materials. Metallurgical characterization of the as-built, HIP-treated materials have been carried out to understand the effect of temperature on the microstructures. The standard HIP[1]treated material measured about 1.4x - 1.7x wider α laths than those in the low[1]temperature HIP treated and as-built samples, respectively. The standard HIP[1]treated material showed about 10 - 14% lower yield strength than other HIP treated materials. At 350 ˚C the yield strength decreases to about 65% compared to the room temperature strength for all tested materials. An increase in ductility vi programvaran NASGRO där livsförutsägelserna visade god överensstämmelse med experimentella livscykler i de flesta fall. vii Abstract Title: Microstructure and mechanical properties of low-temperature hot isostatic pressed Ti-6Al-4V manufactured by electron beam melting Keywords: Additive manufacturing, high-temperature tensile properties, low cycle fatigue, neutron diffraction, fatigue crack growth ISBN: 978-91-89325-27-2 (Printed) 978-91-89325-26-5 (Electronic) Ti-6Al-4V is the most widely used α+β titanium alloy in aerospace engine applications due to its high specific strength. Typically, the alloy is manufactured as castings or forgings and then machined to final geometry. These conventional manufacturing processes do however generate a lot of waste material, whereas additive manufacturing (AM) can potentially produce a near-net-shape geometry directly from the feedstock. In the past decade, electron beam melting (EBM), one of the powder bed fusion techniques, has been widely researched to build Ti[1]6Al-4V components. Still, the as-built material can contain defects such as gas pores that require post-processing, such as hot isostatic pressing (HIP) to produce nearly fully dense components. HIP treatment of conventionally cast Ti-6Al-4V is normally performed at 920 ˚C, 100 MPa for 2 hours. This same HIP treatment has then been adapted also for EBM-manufactured Ti-6Al-4V, which however results in coarsening of α laths and reduction of yield strength. Therefore, finding a more appropriate HIP treatment for this new type of Ti-6Al-4V material, i.e. EBM manufactured, would be of great benefit for the industry. Lowering the HIP treatment temperature to 800 ˚C and increasing the pressure to 200 MPa has recently been proven to close the porosity to a high degree while sustaining the high yield strength. In this thesis, the high-temperature tensile properties of EBM-manufactured Ti[1]6Al-4V subjected to a low-temperature (800 ˚C) HIP treatment were evaluated and compared with standard HIP-treated (920 ˚C) materials. Metallurgical characterization of the as-built, HIP-treated materials have been carried out to understand the effect of temperature on the microstructures. The standard HIP[1]treated material measured about 1.4x - 1.7x wider α laths than those in the low[1]temperature HIP treated and as-built samples, respectively. The standard HIP[1]treated material showed about 10 - 14% lower yield strength than other HIP treated materials. At 350 ˚C the yield strength decreases to about 65% compared to the room temperature strength for all tested materials. An increase in ductility viii was observed at 150 ˚C compared to that at room temperature, but the ductility decreased between 150 - 350 ˚C because of activation of different slip systems. The low cycle fatigue (LCF) behavior of such a modified HIP (low-temperature HIP) material is assessed at two different strain levels and compared with the corresponding LCF properties for the standard HIP material. Even though the modified HIP material had lowest minimum life cycles to failure, the overall fatigue performance is comparable with that of the standard HIP material. Also, fatigue life predictions were made from the measured defect size at the crack initiation site using NASGRO. The calculated life predictions showed good agreement with the experimental values in most cases. In-situ neutron diffraction measurements on tensile test specimens were conducted, at both room temperature and at 350˚ C, for the standard and modified HIP-treated materials. The objective was to gain essential insights on how the crystal lattice strains relate to the macroscopic strengths in these specific microstructures. This investigation helped to understand the load partitioning between different slip planes and constituent phases in the microstructure at different temperatures. / Ti-6Al-4V är den mest använda α+β titanlegeringen i flygmotortillämpningar på grund av sin höga specifika hållfasthet. Vanligtvis tillverkas legeringen som gjutgods eller smide och bearbetas sedan till slutlig geometri. Dessa konventionella tillverkningsprocesser genererar dock en hel del avfallsmaterial, medan additiv tillverkning (AM) potentiellt kan producera en nästan slutgiltlig geometri direkt från råvaran. Under det senaste decenniet har elektronstrålesmältning (EBM), en av pulverbäddsfusionsteknikerna, undersökts mycket för att bygga Ti-6Al-4V-komponenter. Ändå kan det byggda materialet innehålla defekter såsom gasporer som kräver efterbearbetning, såsom varm isostatisk pressning (HIP) för att producera nästan helt täta komponenter. HIP[1]behandling av konventionellt gjutet Ti-6Al-4V utförs normalt vid 920 ˚C, 100 MPa under 2 timmar. Samma HIP-behandling har sedan anpassats även för EBM[1]tillverkat Ti-6Al-4V, vilket dock resulterar i förgrovning av α-lameller och minskning av sträckgränsen. Att hitta en mer lämplig HIP-behandling för denna nya typ av Ti-6Al-4V-material, dvs EBM-tillverkat, skulle därför vara till stor fördel för industrin. Att sänka HIP-behandlingstemperaturen till 800 ˚C och öka trycket till 200 MPa har nyligen visat sig stänga porositeten i hög grad samtidigt som den höga sträckgränsen bibehålls. Ti-6Al-4V används huvudsakligen i applikationer för flygmotorer upp till en maximal driftstemperatur på 300 ˚C. Därför studerades högtemperaturdragegenskaperna hos de olika HIP-behandlade EBM[1]byggmaterialen i detta forskningsarbete. Denna studie visade att duktiliteten påverkas av aktiveringen av olika glidsystem baserat på temperatur. Ytterligare neutrondiffraktionsexperiment utfördes tillsammans med in-situ dragprovning för att bestämma det aktiva glidsystemet vid en specifik temperatur. Utmattningsbeteendet hos det lågtemperaturbehandlade HIP-materialet utvärderas också genom lågcykelutmattningstestning och utmattningsspricktillväxttest. Utmattningsprestandan för det modifierade HIP[1]materialet utvärderades mot standard HIP- material och visade sig ha jämförbara utmattningsegenskaper. Förutsägelser om utmattningsliv utfördes med hjälp av vi programvaran NASGRO där livsförutsägelserna visade god överensstämmelse med experimentella livscykler i de flesta fall. / <p>Submitted papers or manuscripts have been excluded from the fulltext file.</p>

The aim of this dissertation work is the evaluation of the influence of nickel alloying on the structure and mechanical properties, both monotonic and dynamic, of nodular cast iron with ferritic and bainitic matrix. Two chock melts with 0.5 and 2.7 % Ni were used to study the nickel influence. The quantitative evaluation of structure of these melts using image analysis was done and basic tensile mechanical properties were determined. Subsequently, the time optimization of two-stage ferritic annealing and isothermal austempered heat treatment at 375 °C was performed with the aim to obtain optimal ferritic and bainitic structures with best static and dynamic mechanical properties. After ferritic annealing the nickel alloying contributes to substitution hardening of ferritic matrix which positively affects its strength and other mechanical properties. The higher nickel content in the bainitic structure causes the shift of phase transformation times to longer times which results in restricted production of small carbides and in bigger volume of retained austenite. These features were confirmed by observation in transmission electron microscope. Precise tensile and low cycle fatigue tests at temperatures 23 and – 45 °C were performed on the optimized structures of both nodular cast irons. As a result of the notch effect of graphite nodules, microplastic deformation of both nodular cast irons was observed at stresses which were lower than the yield stress. The Hollomon's equation very well describes the individual parts of tensile curves for both nodular cast irons including their mutual comparison. From the low cycle fatigue tests, the cyclic hardening/softening curves, the evolution of elastic modulus and hysteresis loop shape parameters, cyclic stress-strain curves and fatigue life curves were obtained for both temperatures and materials. Moreover, the decrease of retained austenite volume was measured by neutron diffraction and the evolution of surface relief was characterized during cyclic straining for both austempered nodular cast irons at both temperatures. On the basis of these results both cyclic plasticity and fatigue degradation mechanisms in relation to the cyclic strain localization were described for both nodular cast irons.

The thesis is focused on assessment of fatigue behaviour of austempered ductile iron with nodular graphite. Optimal period of transformation was determined based on the best combination of stress and strain characteristics established by tensile test. Cyclic response and low-cycle fatigue life were studied under both stress-control and longitudinal strain-control mode at room temperature. For both modes, shapes of cyclic hardening curves are dependent on stress amplitude. Cyclic deformation curves (CDC) were fitted by power regression function. Results were compared with CDC established by multiple step test in both modes with verification of the influence of cyclic creep (high stress levels, stress-control mode). Experimental data of S-N curves are in agreement with the Manson-Coffin and the Basquin law. Fatigue and cyclic parameters were compared. Fatigue life time in high-cycle fatigue region was determined. Experimental data were fitted by suitable regression functions. Regression parameters and fatigue limit were established by means of each regression function. Experimental data in low- and high-cycle fatigue regions were used to construct S-N curve and to determine relevant parameters. Discontinuity of experimental data was not observed. Low-cycle fatigue behaviour was predicted. Approximation of tolerance bands was realized in high-cycle and both high and low cycle fatigue regions.

No description available.

Fatigue testing of stretch sensors often focuses on high amplitude, low-cycle fatigue (LCF) behavior; however, when used for orthopaedic, athletic, or ergonomic assessments, stretch sensors are subjected to low amplitude, high-cycle fatigue (HCF) conditions. As an added layer of complexity, the fatigue testing of stretch sensors is not only focused on the life of the material comprising the sensor, but also on the reliability of the signal produced during the extension and relaxation of the sensor. Research into the development of a smart sock that can be used to measure the range of motion (ROM) of the ankle joint during athletic practices and competitions using stretch sensors is ongoing at Mississippi State University. The current smart sock prototype utilizes StretchSense™ StretchFABRIC capacitive dielectric elastomer sensors. These sensors are no longer manufactured, and FlexSense stretch sensors are being investigated as a potential replacement. To assess the reliability of the signal of the StretchFABRIC sensors currently used in the prototype, two sensors were subjected to 25,000 cycles of fatigue, under with simultaneous capture of the capacitance. The capacitances of the fatigued sensors were then compared to the capacitance of an unfatigued StretchFABRIC sensor during participant trials. Participants completed four static movements and six dynamic gait trials using either the fatigued or unfatigued sensor. Following completion of the initial static and dynamic movements, the movements were repeated using the opposite sensor. Comparison of the fatigued sensor to the unfatigued sensor revealed an upward drift in the capacitance of the fatigued sensor for all trials. Two FlexSense sensors were then subjected to either 450,000 or 250,000 cycles of fatigue with simultaneous capture of the signal from the sensor. To assess the signal, the peak capacitance recorded during the fatigue test was compared to the peak stretch percentage produced by the sensor. The peak displacement remained tight about the mean, while the peak stretch percentage exhibited a high level of scatter. From a materials standpoint, the sensors conformed to the Rabinowitz-Beardmore model of polymer fatigue where an initial monotonic overload of the material is followed by a transition to cyclic stability of the material.

Ultrafeinkörnige metallische Werkstoffe haben verstärkt wissenschaftliche Bedeutung erlangt. Um dieser neuartigen Werkstoffklasse über die grundlagenorientierte Forschung hinaus einen Einsatz in technischen Anwendungen zu ermöglichen, ist es notwendig, deren Verhalten unter verschiedenen einsatzrelevanten Belastungsbedingungen vorhersagen zu können. In der vorliegenden Arbeit wird das Schädigungsverhalten einer ultrafeinkörnigen Aluminiumlegierung in den Bereichen der hochzyklischen (HCF) und niedrigzyklischen (LCF) Ermüdung sowie des Rissfortschritts untersucht. Im Mittelpunkt steht dabei die Identifikation der mikrostrukturell wirksamen Mechanismen bei der Entstehung und Ausbreitung von Ermüdungsrissen. Es werden ein homogen ultrafeinkörniger und ein bimodaler Zustand sowie verschiedene duktilitätsoptimierte Zustände betrachtet und systematisch der Einfluss der Korngröße, der Korngrößenverteilung, der Ausscheidungscharakteristik sowie der Festigkeit und Duktilität auf das Ermüdungs- und Rissfortschrittsverhalten ermittelt. Die Untersuchungen zeigen, dass das Schädigungsverhalten der ultrafeinkörnigen Aluminiumlegierung insbesondere durch die Korngröße und Korngrößenverteilung sowie den Kohärenzgrad der festigkeitssteigernden Ausscheidungen beeinflusst wird.