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In this thesis, the a-PMT (amorphous lead magnesium titanate) membranes have been prepared by sol-gel technique as H+ ion sensitive layers. The C-V measurements of the a-PMT/SiO2/Si EIS structures prepared by spin-on coating are used for examining the fabrication parameters and sensing properties. There exhibits the quasi-Nerstain response of 55¡V59 mV/pH in the range of pH 2¡V12, fabricated with the Mg-modified content of 4 mole%, the firing temperature of about 400 ¢J and the thickness of about 0.5

Weight reduction is a hot topic in automotive industry. Both the applications of tube hydroforming technique and magnesium alloys offer a large potential for reducing the weight of automotive components. In this research, the relationship between forming pressure and bulge height, the maximum forming pressure and the forming limit during the tube hydraulic bulging process are first analysed. A self-designed warm hydraulic bulge forming equipment and the seamlessly extruted magnesium alloy AZ61 tubes, are used for carrying out a series of warm hydraulic bulge tests, and discussing the formalibility of the magnesium tubes at various temperatures. Furthermore, the flow stress curves are determined by the mathematical model in this paper with the bulge forming test results. Then the validity of the analytical model is verified by comparing the forming pressure and bulge height between analytical and experimental values.

Magnesium alloy tubes have good formability at elevated temperatures. In this study, a finite element code DEFORM 3D is used to simulate the result of T-shape hydroforming at working temperatures 150¢J and 250¢J with magnesium alloy AZ61 tubes and then conducts the hydroforming experiments. By modifying the loading paths, products with uniform thickness and branch height are obtained 49mm. The results of simulation are compared with the experimental results to verify the validity of this modeling. On the other hand, the effects of the die fillet radius on tube formability during y-shape hydroforming are discussed. With the right die fillet radius r1¡×10mm and the left die fillet radius r2¡×30mm, a better formability of the tube is obtained.

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This study involves analyses and experiments of magnesium¡¦s hot extrusion of thin sheets and tubes. At first, hot compression tests are conducted to obtain the magnesium¡¦s plastic flow stresses in high tempearatures, which will be used in the finite element analysis. In the FE simulations of thin sheet extrusion, the flow pattern of the magnesium billet within the die, the temperature history at die exit and the elastic deformation of the die is analyzed. Sound and good thin sheets are obtained by appropriate die design, initial billet temperature and extrusion velocity¡¦s control. The goal of constant temperature extrusion is expected to achieved by controlling the extrusion velocity which will influences the billet temperature at die exit. In FE simulations of thin tube extrusion, the flow pattern of the magnesium billet within the port-holes, welding chamber and die bearing is analyzed. The elastic deformation of the die is dicussed. Extrusion of sound thin tubes is achieved by appropriate extrusion conditions. Finally, hot extrusion experiments are conducted and the experimental values of the extrusion load and dimensions of the products are compared with the analytical values to verify the validity of the analytical models.

Thesis (Ph.D)--Materials Science and Engineering, Georgia Institute of Technology, 2006. / Ken Sandhage - Committee Chair, Robert Snyder - Committee Co-Chair, G. Paul Neitzel - Committee Member, Preet Singh - Committee Member, Robert Speyer - Committee Member Part of the SMARTech Electronic Thesis and Dissertation Collection.

Thesis (M. Phil.)--University of Hong Kong, 2002. / Includes bibliographical references (leaves 75-77).

Magnesium sheet alloys, such as wrought AZ31, have material properties that make them an attractive option for use in automotive and aircraft components. However, the low ductility of magnesium alloys at room temperature necessitates the use of high-temperature forming to manufacture complex components. Finite-element-method (FEM) simulations can assist in determining the optimum processing parameters for high-temperature forming, but only if an accurate material constitutive model is used. New material constitutive models describing the deformation behavior of AZ31 sheet at 450°C are proposed. These models account for both active deformation mechanisms at this temperature: grain-boundary-sliding creep and five-power dislocation-climb creep. Phenomena affecting these deformation mechanisms, such as material anisotropy and grain growth, are also investigated. This physics-based approach represents an improvement over previous material models, which require nonphysical parameters and can only predict forming for a limited range of conditions. Tensile tests are conducted to obtain data used in fitting constitutive models. New models are used in FEM simulations of both tensile tests and biaxial gas-pressure bulge tests. Simulation results are compared to experimental data for validation and determination of model accuracy. / text

Coarse aggregate is often one of the largest volume occupying components in a portland cement concrete system. With increases in transportation costs and depletion of many of the aggregate sources currently in use the need to reevaluate the performance of aggregates in concrete has arisen. Current aggregate testing requirements for many organizations have not been updated in decades, even with the advancements in aggregate testing equipment that are currently available. This research project investigates current used and potential test methods for evaluating coarse aggregate for use in portland cement concrete. Testing focused on determining the most appropriate aggregate property to evaluate and then determining the correlation to mechanical concrete properties. Relationships between potential aggregate tests and currently used aggregate tests were evaluated to determine if compatible relationships between methods were evident. For this purpose concrete mixtures were made at a fixed aggregate volume to establish if a link was evident between aggregate test properties and concrete. To establish a link between laboratory and real world performance field sites with known distress were visited to better establish limits for aggregate testing requirements. Results obtained provided the basis for recommendations for testing requirements and limits to be used for aggregates in portland cement concrete. / text