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京都大学 / 新制・課程博士 / 博士(工学) / 甲第24605号 / 工博第5111号 / 新制||工||1978(附属図書館) / 京都大学大学院工学研究科機械理工学専攻 / (主査)教授 平山 朋子, 教授 松原 厚, 教授 小森 雅晴 / 学位規則第4条第1項該当 / Doctor of Philosophy (Engineering) / Kyoto University / DFAM

<p>Optical beam steering is of significant importance for various emerging applications such as light detection and ranging (LiDAR), free space optical communication, and holographic display. However, the development of schemes for dynamic spatio-temporal beam steering has been limited in the past. A previous study achieved dynamic and continuous angular beam steering of isolated ultrashort pulses from a mode-locked laser by using a passive metasurface emulating a diffraction grating followed by a lens. In this thesis, we experimentally demonstrate dynamic spatio-temporal steering of high repetition rate pulse trains using a spatial array of frequency combs with a uniform gradient in their carrier-envelope offsets. To accomplish this, we leverage the capabilities of a virtually imaged phased array (VIPA), which is a side-entrance Fabry-Perot etalon, and employ successive spatial Fourier transforms facilitated by a 4f optical lens system. Our experimental results successfully demonstrate the periodic scanning of ultrashort pulse trains generated from an electro-optic comb at a repetition rate of ~10 GHz. The scanning occurs in discrete steps of ~115 μm and ~20 ps in the spatial and temporal domains, respectively.</p>

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We investigate the spatial evolution of an intense laser pulse as it generates high-order harmonics in a long gas cell, filled with 80 torr of helium. A thin foil separates the gas-filled region of the cell from a subsequent evacuated region. The exit plane of the gas cell can be scanned along the laser axis so that the evolution of the laser throughout the focus can be observed (full scanning range of 9 cm). We constructed an apparatus that images the laser radial energy profile as it exits the cell. The high harmonics, odd orders ranging from 45 to 91, are observed at the same time that the laser spot is characterized. Re-absorption of the harmonics within the gas cell restricts the region of harmonic emission to the final centimeter (or less) of the cell. We present the first direct evidence (to our knowledge) of laser filamentation under conditions ideal for high-order harmonic generation. The 30 fs, 4 mJ, laser pulses were observed to undergo double focusing within the gas cell, with about 4 cm separating the two foci. The region with best harmonic emission occurs midway between the two foci. The radial profile of the laser focus, 150-200 microns in diameter, evolves from a Gaussian-like profile to a more square-top profile as it propagates over several centimeters. The filamentation phenomenon as well as the brightness of the harmonics improves when an aperture is partially closed on the laser beam before reaching the focusing mirror. A spectral sampling of the imaged laser focus revealed a 4 nm blue-shift associated with the generation of plasma in the gas cell. The blue-shifting occurs primarily in the center of the laser beam and less at the wider radii. The initial laser pulse had a spectrum centered at 800 nm with a 35 nm bandwidth. The energy associated with each of the observed 26 harmonic beams was found to be approximately 1 nJ, yielding a conversion efficiency of approximately 2e−7.

Vanadium dioxide (VO_2) is a material of particular interest due to its exhibited metal to insulator phase transition at 68°C that is accompanied by an abrupt and significant change in its electronic and optical properties. Since this material can exhibit a reversible drop in resistivity of up to five orders of magnitude and a reversible drop in infrared optical transmission of up to 80%, this material holds promise in several technological applications. Solid phase crystallization of VO_2 thin films was obtained by a post-deposition annealing process of a VO_{x,x approx 2} amorphous film sputtered on an amorphous silicon dioxide (SiO_2) layer. Scanning electron microscopy (SEM) and electron-backscattered diffraction (EBSD) were utilized to study the morphology of the solid phase crystallization that resulted from this post-deposition annealing process. The annealing parameters ranged in temperature from 300°C up to 1000°C and in time from 5 minutes up to 12 hours. Depending on the annealing parameters, EBSD showed that this process yielded polycrystalline vanadium dioxide thin films, semi-continuous thin films, and films of isolated single-crystal particles. In addition to these films on SiO_2, other VO_2 thin films were deposited onto a-, c-, and r-cuts of sapphire and on TiO_2(001) heated single-crystal substrates by pulsed-laser deposition (PLD). The temperature of the substrates was kept at ~500°C during deposition. EBSD maps and orientation imaging microscopy were used to study the epitaxy and orientation of the VO_2 grains deposited on the single crystal substrates, as well as on the amorphous SiO_2 layer. The EBSD/OIM results showed that: 1) For all the sapphire substrates analyzed, there is a predominant family of crystallographic relationships wherein the rutile VO_2{001} planes tend to lie parallel to the sapphire's {10-10} and the rutile VO_2{100} planes lie parallel to the sapphire's {1-210} and {0001}. Furthermore, while this family of relationships accounts for the majority of the VO_2 grains observed, due to the sapphire substrate's geometry there were variations within these rules that changed the orientation of VO_2 grains with respect to the substrate's normal direction. 2) For the TiO_2, a substrate with a lower lattice mismatch, we observe the expected relationship where the rutile VO_2 [100], [110], and [001] crystal directions lie parallel to the TiO_2 substrate's [100], [110], and [001] crystal directions respectively. 3) For the amorphous SiO_2 layer, all VO_2 crystals that were measurable (those that grew to the thickness of the deposited film) had a preferred orientation with the the rutile VO_2[001] crystal direction tending to lie parallel to the plane of the specimen. The use of transmission electron microscopy (TEM) is presented as a tool for further characterization studies of this material and its applications. In this work TEM diffraction patterns taken from cross-sections of particles of the a- and r-cut sapphire substrates not only solidified the predominant family mentioned, but also helped lift the ambiguity present in the rutile VO_2{100} axes. Finally, a focused-ion beam technique for preparation of cross-sectional TEM samples of metallic thin films deposited on polymer substrates is demonstrated.

The electrostatic ion beam trap (EIBT) was designed by D. Zajfman during the previous decade. This ion trap combines many properties of the Fourier-transform ion cyclotron resonance (FTICR) mass analyzer and time-of-flight (TOF) mass analyzer. There are several advantages for the electrostatic ion beam trap. First, large mass-to-charge particles in an electrostatic field could be easier to analyze. Second, there is a folded flight path, which could make the mass analyzer smaller compared to conventional TOF mass analyzer. This principle of operation of this ion trap is analogous to an optical resonator. The ions are trapped in a voltage valley and oscillate between the two parallel sets of mirror electrodes with high voltages. In this thesis, I first describe a new type of miniaturized electrostatic ion beam trap mass analyzer that consists of two printed circuit boards (PCBs). The facing surfaces of these boards are imprinted with copper electrodes. The center of the boards is field free and at ground potential with ion mirrors and Einzel lenses on either side. A charge detector is attached to the center for recording the time-dependant motion of the ions in the field. The PCB-based EIBT design is easier to construct than the original EIBT mass analyzer. The electrostatic fields are optimized by adjusting the potential on the mirror electrodes as well as the geometry of the electrodes. Although nondestructive charge detection is much less sensitive for small ions, this detection is ideal for analysis of large ions. The planar electrostatic ion beam trap is inexpensive, small, and simple to operate. The PCB EIBT device was designed, built, and tested using metal samples such as copper and nickel. The electric field of the PCB EIBT is not the same as that of the original EIBT. Unfortunately, there were no ion signals captured in image charge detector. Another new type of miniaturized electrostatic ion beam trap was made by depositing electrodes onto Kapton film. Seven thin tin/copper traces (1 mm wide by 0.015 mm thick) were deposited onto each side of a flat, flexible circuit board substrate (Kapton film 0.15 mm thickness). The film was rolled to form a cylinder. The flexible EIBT is small (4.5 cm × 8 cm), and lightweight (~1 g). This device was tested using laser ablation of CsI. The CsI signals were detected by the charge detector, amplified and sent to the oscilloscope. Fourier transformation was used to convert the data to the frequency domain spectrum. The resolution of Cs+ is around 1000 (m/Δm) from initial flexible EIBT test. The mass accuracy of the Cs+ peak is better than 0.1%.

The primary purpose of this study is to give simple and detailed instructions for building a log cabin by the post-and-beam method. The data were gathered from three sources: (1) library research, (2) interviews with experienced builders of cabins, and (3) personal experience in cabin construction. A step-by-step guide for building a cabin is given in Chapters II and III, which explain in depth how to construct each section of the cabin, from laying the foundation to putting on the finishing touches. It is believed that any serious builder can follow the directions and construct his own log cabin for less than one-third the cost of a similar commercially built cabin.