O polietileno de média densidade (PEMD) é um polímero termoplástico parcialmente cristalino, cujo uso tem crescido bastante em aplicações de engenharia, como em tubos plásticos para sistemas de distribuição de água e de gás. Sob carga constante, entretanto, este material pode eventualmente apresentar fratura por fluência, por meio de um mecanismo de crescimento lento de trincas, provocando acentuadas perdas por vazamento nos sistemas. Os métodos atuais empregados pela indústria para estimar a durabilidade dos tubos são caros, demorados, pouco práticos e imprecisos. Busca-se o desenvolvimento de técnicas mais eficientes, sendo que os métodos da mecânica da fratura são promissores no sentido de descrever a etapa de propagação da trinca. Ensaios de mecânica da fratura, entretanto, requerem a introdução de pré-trincas nos corpos de prova. Sabe-se que as técnicas artificiais de introdução de pré-trincas causam algum tipo de dano na matriz polimérica, que pode ou não afetar os resultados dos ensaios, dependendo dos eventos que ocorrerem após o carregamento inicial. A principal propriedade requerida de um método de introdução de pré-trinca, portanto, é reprodutibilidade. Neste estudo foram aplicados três importantes métodos de mecânica da fratura ao PEMD e investigados os efeitos de diferentes técnicas de introdução de pré-trincas sobre os resultados dos ensaios e sobre as estruturas de deformação na matriz do material na ponta da trinca. Os ensaios de tenacidade à fratura no estado plano de deformação - KIc - foram realizados em condições criogênicas, em vista do comportamento dúctil do material à temperatura ambiente, sendo que a estratégia mostrou-se satisfatória. Os resultados dos ensaios de Integral-J sugerem que o método pode não ser aplicável ao PEMD, devido ao peculiar mecanismo de fratura do material. O método do trabalho essencial de fratura - EWF - se aplica bem ao PEMD. Os resultados dos ensaios de KIc e EWF demonstraram que diferentes técnicas de introdução de pré-trincas provocam diferentes estruturas de deformação no material na ponta da trinca e afetam os resultados de ensaios de fratura no PEMD. Os resultados de EWF demonstraram ainda que o processamento também afeta as propriedades de fratura do material. É proposta uma nova técnica para a introdução de pré-trincas, com características mais naturais, a qual requer estudos complementares para seu aperfeiçoamento. / Medium density polyethylene (MDPE) is a semicrystalline thermoplastic polymer that has been increasingly used in engineering applications, as plastic pipes for water and gas distribution systems. Under constant load, however, this material may occasionally present creep failure, by means of a mechanism of slow crack growth, leading to leakage losses in the systems. Current methods used by industry to estimate durability of pipes are expensive, time consuming, non practical and inaccurate. The development of more efficient methods is a common target and fracture mechanics methods are promising in describing the crack propagation stage. Fracture mechanics testing methods, however, require the introduction of pre-cracks into the specimens. It is known that artificial methods of introducing pre-cracks produce some damage on the polymeric matrix, which may or not affect the results of tests, depending on the events that occur after the initial loading. Main propriety required of a pre-crack introducing method, therefore, is reproducibility. In this study three important fracture mechanics methods were applied to MDPE and the effects of different methods of pre-cracking over test results and over deformation structures of material matrix at the crack tip were investigated. Plane-strain fracture toughness - KIc tests were performed under cryogenic conditions, in view of the ductile behavior of material at room temperature and this strategy was well succeed. Results of Integral-J tests suggest that this method may not be applicable to MDPE, due to the peculiar fracture mechanism of the material. The essential work of fracture method EWF is well suited to study MDPE. The results of KIc and EWF tests showed that different pre-cracking methods cause different deformation structures in the material at the crack tip and affect the fracture tests with MDPE. EWF results showed also that the processing affect the fracture properties of materials too. It is proposed a new method for introducing pre-cracks, with more natural characteristics that requires complementary studies for its improving.

In this thesis an experimental method to calculate cohesive characteristics for an adhesive layer in a End Notched Flexure (ENF) specimen is presented and evaluated. The method is based on the path independent J-integral where the energy release rate (ERR) for the adhesive is derived as a function of the applied forces and the rotational displacements at the loading point and at the supports of the specimen. The major advantage with the method in comparison with existing theory known by the job initiator is that it is still applicable with ENF specimens that are subjected to yielding of the adherends. The structure of this thesis is disposed so that the theory behind the J-integral method is shortly described and then an evaluation of the method is performed by aid of finite element simulations using beam and cohesive elements. The finite element simulations indicates that the ERR can be determined with good accuracy for an ENF specimen where a small scale yielding of the adherends has occurred. However when a fully cross sectional yielding of the adherends is reached the ERR starts diverging from the exact value and generates a too high ERR according to input data in the simulations, i.e. the exact values. The importance in length of the adhesive process zone is also shown to be irrelevant to the ERR measured according to the J-integral method. Simulation performed with continuum elements indicates that a more reality based FE- simulation implies a higher value of the applied load in order to create crack propagation. This is an effect of that the specimen is allowed to roll on the supports which makes the effective length between the supports shorter than the initial value when the specimen is deformed. This results in a stiffer specimen and thus a higher applied force is needed to create crack propagation in the adhesive layer. An experimental set up of an ENF specimen is created and the sample data from the experiments are evaluated with the J-integral method. For measuring the rotational displacements of the specimen which are needed for the J-integral equation an image system is developed by the author and validated by use of linear elastic beam theory. The system calculates the three rotational displacements of the specimen by aid of images taken by a high resolution SLR camera and the system for measuring the rotations may also be used in other applications than for a specific ENF geometry. The validation of the image system shows that the rotations calculated by the image system diverge from beam theory with less than 2.2 % which is a quite good accuracy in comparison with the accuracies for the rest of the used surveying equipment. The results from the experiment indicates that the used, about 0.36 mm thick SikaPower 498, adhesive has an maximum shear strength of 37.3 MPa and a critical shear deformation of 482 µm. The fracture energy is for this thickness of the adhesive is determined as 12.9 kJ/m2. This report ends with a conclusion- and a suggested future work- chapter.

The main objective of this study is to evaluate mixed mode stress intensity factors for inclined embedded cracks in functionally graded materials. Fracture analysis of inclined cracks requires the calculation of both Mode I and Mode II stress intensity factors ( I K , II K ). In this study, k J -integral is used to calculate I K and II K . Equivalent domain integral approach is utilized to evaluate the k J - integral around the crack tip. The present study aims at developing a finite element model to study inclined crack problems in graded media under thermomechanical loading. A two dimensional finite element model is developed for inclined cracks located in a functionally graded medium. Structural and thermal problems are solved using two dimensional finite elements namely 8- noded triangles. Material properties are sampled directly at the integration points of the elements, as required by the numerical integral evaluation. The main results of the study are the stress intensity factors at the crack tip for functionally graded materials subjected to thermomechanical loading.

This study aims to develop a computer program to perform finite elements based fracture mechanics analyses of three dimensional surface cracks in T-welded joints of construction machinery. The geometrical complexity of the finite elements models and the requirement of large computer resources for the analyses necessitate the use of shell elements for general stress distribution optimization. A sub-modeling technique, together with a shell to solid conversion method, enables the user to model a local region and analyze it by defining the weld and crack parameters. It is assumed that the weld material is the same with the sheet metal material and the surface cracks are considered to occur on two weld toes and weld root. The surface cracks are assumed to have a semi elliptical crack front profile. In order to simulate the square-root strain singularity around the crack front, collapsed 20-node three dimensional brick elements are utilized. The rest of the local model is modeled by using 20-node three dimensional brick elements. The main objective of this work is to calculate the mixed mode energy release rates around the crack front for a sub-model of a global shell model by using J-integral method.

<p>In this thesis an experimental method to calculate cohesive characteristics for an adhesive layer in a End Notched Flexure (ENF) specimen is presented and evaluated. The method is based on the path independent J-integral where the energy release rate (ERR) for the adhesive is derived as a function of the applied forces and the rotational displacements at the loading point and at the supports of the specimen. The major advantage with the method in comparison with existing theory known by the job initiator is that it is still applicable with ENF specimens that are subjected to yielding of the adherends.</p><p>The structure of this thesis is disposed so that the theory behind the J-integral method is shortly described and then an evaluation of the method is performed by aid of finite element simulations using beam and cohesive elements. The finite element simulations indicates that the ERR can be determined with good accuracy for an ENF specimen where a small scale yielding of the adherends has occurred. However when a fully cross sectional yielding of the adherends is reached the ERR starts diverging from the exact value and generates a too high ERR according to input data in the simulations, i.e. the exact values. The importance in length of the adhesive process zone is also shown to be irrelevant to the ERR measured according to the J-integral method.</p><p>Simulation performed with continuum elements indicates that a more reality based FE- simulation implies a higher value of the applied load in order to create crack propagation. This is an effect of that the specimen is allowed to roll on the supports which makes the effective length between the supports shorter than the initial value when the specimen is deformed. This results in a stiffer specimen and thus a higher applied force is needed to create crack propagation in the adhesive layer.</p><p>An experimental set up of an ENF specimen is created and the sample data from the experiments are evaluated with the J-integral method. For measuring the rotational displacements of the specimen which are needed for the J-integral equation an image system is developed by the author and validated by use of linear elastic beam theory. The system calculates the three rotational displacements of the specimen by aid of images taken by a high resolution SLR camera and the system for measuring the rotations may also be used in other applications than for a specific ENF geometry. The validation of the image system shows that the rotations calculated by the image system diverge from beam theory with less than 2.2 % which is a quite good accuracy in comparison with the accuracies for the rest of the used surveying equipment.</p><p>The results from the experiment indicates that the used, about 0.36 mm thick SikaPower 498, adhesive has an maximum shear strength of 37.3 MPa and a critical shear deformation of 482 µm. The fracture energy is for this thickness of the adhesive is determined as 12.9 kJ/m².</p><p>This report ends with a conclusion- and a suggested future work- chapter.</p>

Das geometrische In-plane-Moireverfahren wird benutzt, um das Deformationsfeld um einen Riss in einem geschweißten Verbund zweier unterschiedlicher Metalle sowie in homogenen Proben dieser Materialien zu untersuchen. Konkret werden Vierpunktbiegeproben benutzt, wobei die Grenzflächen der Verbundproben durch Explosionsschweißen (Sprengplattieren) hergestellt werden. In Verbindung mit der digitalen Bildverarbeitung wird das Feld der Verschiebungen zum Zeitpunkt der Rissinitiierung als primäres Resultat aus den Isothetenfeldern ermittelt. Aus diesen Verschiebungsfeldern lassen sich mittels eines Approximationsverfahrens weitere Größen wie Verzerrungen und Spannungsgrößen an der Oberfläche ableiten. Zusätzlich werden dreidimensionale elastisch-plastische FEM-Berechnungen für die homogenen Proben und die Proben mit Grenzflächenriss durchgeführt. Das J-Integral wird aufgrund der experimentell und numerisch gewonnenen Daten für den Rissinitiierungszeitpunkt berechnet. Außerdem findet ein Vergleich mit J-Integralwerten statt, die mit Methoden der Materialprüfnormen bestimmt werden.

Bauteile mit Rissen können mit Hilfe der Bruchmechanik bewertet werden. Da die Ermittlung der Rissspitzenbeanspruchung nicht immer analytisch gelingt, ist die Nutzung numerischer Verfahren von Vorteil. Nach einer kurzen Einführung in die Bruchmechanik wird an zwei Beispielen die Vorgehensweise diskutiert.

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O polietileno de média densidade (PEMD) é um polímero termoplástico parcialmente cristalino, cujo uso tem crescido bastante em aplicações de engenharia, como em tubos plásticos para sistemas de distribuição de água e de gás. Sob carga constante, entretanto, este material pode eventualmente apresentar fratura por fluência, por meio de um mecanismo de crescimento lento de trincas, provocando acentuadas perdas por vazamento nos sistemas. Os métodos atuais empregados pela indústria para estimar a durabilidade dos tubos são caros, demorados, pouco práticos e imprecisos. Busca-se o desenvolvimento de técnicas mais eficientes, sendo que os métodos da mecânica da fratura são promissores no sentido de descrever a etapa de propagação da trinca. Ensaios de mecânica da fratura, entretanto, requerem a introdução de pré-trincas nos corpos de prova. Sabe-se que as técnicas artificiais de introdução de pré-trincas causam algum tipo de dano na matriz polimérica, que pode ou não afetar os resultados dos ensaios, dependendo dos eventos que ocorrerem após o carregamento inicial. A principal propriedade requerida de um método de introdução de pré-trinca, portanto, é reprodutibilidade. Neste estudo foram aplicados três importantes métodos de mecânica da fratura ao PEMD e investigados os efeitos de diferentes técnicas de introdução de pré-trincas sobre os resultados dos ensaios e sobre as estruturas de deformação na matriz do material na ponta da trinca. Os ensaios de tenacidade à fratura no estado plano de deformação - KIc - foram realizados em condições criogênicas, em vista do comportamento dúctil do material à temperatura ambiente, sendo que a estratégia mostrou-se satisfatória. Os resultados dos ensaios de Integral-J sugerem que o método pode não ser aplicável ao PEMD, devido ao peculiar mecanismo de fratura do material. O método do trabalho essencial de fratura - EWF - se aplica bem ao PEMD. Os resultados dos ensaios de KIc e EWF demonstraram que diferentes técnicas de introdução de pré-trincas provocam diferentes estruturas de deformação no material na ponta da trinca e afetam os resultados de ensaios de fratura no PEMD. Os resultados de EWF demonstraram ainda que o processamento também afeta as propriedades de fratura do material. É proposta uma nova técnica para a introdução de pré-trincas, com características mais naturais, a qual requer estudos complementares para seu aperfeiçoamento. / Medium density polyethylene (MDPE) is a semicrystalline thermoplastic polymer that has been increasingly used in engineering applications, as plastic pipes for water and gas distribution systems. Under constant load, however, this material may occasionally present creep failure, by means of a mechanism of slow crack growth, leading to leakage losses in the systems. Current methods used by industry to estimate durability of pipes are expensive, time consuming, non practical and inaccurate. The development of more efficient methods is a common target and fracture mechanics methods are promising in describing the crack propagation stage. Fracture mechanics testing methods, however, require the introduction of pre-cracks into the specimens. It is known that artificial methods of introducing pre-cracks produce some damage on the polymeric matrix, which may or not affect the results of tests, depending on the events that occur after the initial loading. Main propriety required of a pre-crack introducing method, therefore, is reproducibility. In this study three important fracture mechanics methods were applied to MDPE and the effects of different methods of pre-cracking over test results and over deformation structures of material matrix at the crack tip were investigated. Plane-strain fracture toughness - KIc tests were performed under cryogenic conditions, in view of the ductile behavior of material at room temperature and this strategy was well succeed. Results of Integral-J tests suggest that this method may not be applicable to MDPE, due to the peculiar fracture mechanism of the material. The essential work of fracture method EWF is well suited to study MDPE. The results of KIc and EWF tests showed that different pre-cracking methods cause different deformation structures in the material at the crack tip and affect the fracture tests with MDPE. EWF results showed also that the processing affect the fracture properties of materials too. It is proposed a new method for introducing pre-cracks, with more natural characteristics that requires complementary studies for its improving.