The diploma thesis deals with the design of an asphalt mixture for an abrasive layer with a standard R-material content (20 %) without the use of other softening additives, while the properties of the aged asphalt binder in the mixture were compensated by dosing "softer binder 70/100". Asphalt mixtures type ACO 11+ are designed to meet the requirements ČSN 73 6121: 2019. The aim of the work is to verify the expected properties of the asphalt mixture performed functional and empirical tests according to the standards for asphalt mixtures of the ČSN EN 12697 series.

Finding innovative technologies for building our roads has always been of paramount importance. From moving to warm mix asphalt to decrease our indulgence in high energy consumption to substituting fly ash for asphalt binders to reduce dependence on pure asphalt binders from petroleum, engineers have painstakingly tried to develop new ways to improve the ways that flexible pavements are made. The major problem facing the next generation of civil engineers is sustainable practices on the field. Over the years, significant progress has been made in this regard on the impacts of building pavements on the environment. Characterizing these improvements tends to be difficult, and that is where Life Cycle Assessment (LCA) comes in. LCA is a technique used to analyze and quantify the environmental impacts of a product, system, or process. LCA shows where the significant impacts occur and how improvements can be made while recommending better practices. Even with its many advantages, its use is very constrained, especially in the United States, as it is still a very novel approach in design coupled with limited datasets and protocol for its operation. With modern technologies of substitute materials for binders like bio-oil from food waste, reclaimed asphalt pavement (RAP), and fly ash, there is a need to understand their environmental impacts. Furthermore, in this regard is where LCA can help using three significant areas: selection of materials, normalization, and characterization. Characterization refers to the identification and quantification of the relationships between the life cycle results and the environmental impacts. This research explores the environmental impacts of substituting other materials for asphalt binders using LCA. With variations in modifying levels of substitutes, results show promising levels in emissions of harmful gasses to both the air and water. This study explores ways used in normalizing this process as well as setting up a pathway for other asphalt binder substitutes. / Civil Engineering

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När priset på naturtillgångar ökar samt att industrier måste ställa om till en mer hållbar verksamhet innebär detta även en omställning för asfaltsindustrin. Ett sätt för att använda mer återvunnet material i asfaltsindustri är att använda bindemedlet från gammal asfaltsmassa (eng.: reclaimed asphalt pavement, RAP). Detta kan dock inte göras utan komplikationer och därför måste bindemedlet föryngras innan för att kompensera för faktorer så som hög styvhet, låg krakning och trötthetsförmåga samt dålig anti-åldring förmåga hos RAPen. I det här projektet har två olika typer av föryngringsmedel använts; ett växtoljebaserat och ett petroleumbaserat mjukbitumen. Detta för att se om det var möjligt att använda förnybart och återvunnet material i bindemedlet men fortfarande uppnå samma prestanda som konventionellt bindemedel. Två blandningar gjordes hjälp av de två olika föryngringsmedlen och RAPen och analyserades parallellt med ett referensmaterial. Analyserna delades upp i två kategorier: reologi och kemi. Analyserna som föll under reologikategorin var mjukpunkt- och penetrationsanalyser, samt analyser med en dynamisk skjuvning reometer (eng.: dynamic shear rheometer, DSR) och en böjbalksreometer (eng.: bending beam rheometer, BBR). Under kemikategorin fanns analysmetoderna tunnskiktskromatografi med flamjoniseringsdetektor (TLC-FID) och Fourier transform infraröd spektroskopi (FTIR). Resultaten påvisar att åldring påverkas mycket av vilket föryngringsmedel som används, vilket blev tydligt när den reologiska förmågan testades. De kemiska analyserna gav stort sett liknade resultat oberoende av bindemedel. Blandningen som innehöll RAP och mjukbitumen visade sig vara mer mottagligt för åldring jämfört med den andra blandningen som innehöll växtolja, trots att den blandningen innehåller längre halt av RAPen. Vidare visar resultaten att blandningar kan prestera likt referensmaterialet när det kommer till reologi. Från den kemiska aspekten, uppvisar alla bindemedelsmaterial liknande egenskaper. Därför kan slutsatsen att RAPen var återvunnen med framgång när växtolja och mjukbitumen användes. / In recent years there has been a lot of focus on reduction of carbon footprint and sustainable development. For the asphalt industries, a way of doing this is to use reclaimed asphalt pavement (RAP) binders. This cannot be done without any complications and therefore, the RAP binder is normally rejuvenated to compensate for its high stiffness, and other poor properties like susceptibility to low temperature cracking and fatigue damage. In this project, two different ways of using RAP binder are investigated: one vegetable oil-based rejuvenator and one soft bitumen. Using the rejuvenator and soft bitumen together with a RAP binder, two different blends were made and compared to a reference bitumen which is commonly used in Sweden. The blends were made in such a way that the penetration values were close to the reference sample. Aging tests were performed by RTFOT and PAV. The testing of the non-aged and aged binder materials was divided into two sections: rheology and chemistry. The rheology testing included softening point, needle penetration, analysis with dynamic shear rheometer (DSR) and bending beam rheometer (BBR) whereas the chemistry testing included thin layer chromatography with flame ionization detector (TLC-FID) and Fourier transform infrared spectroscopy (FTIR). The results indicated that the ageing resistance of the binder materials is affected by the type of rejuvenator used which especially affects the rheological performance. The chemical performance was almost the same in each blend. The blend containing RAP binder and soft bitumen was more susceptible to ageing compared to the other blend containing oil-based rejuvenator even though the blend contained less of the RAP binder. The results also shows that the blends can perform equal to the reference sample for a rheological point of view. From a chemical point of view, the binders, including the reference, have the same properties. Therefore, the RAP binder was successfully recycled using both a bio-oil rejuvenator and soft bitumen.

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This study focused on the material characterization of granular materials containing different percentages of “RAP”. A series of laboratory tests results were carried out to determine the physical and mechanical properties of natural aggregates and various aggregate-RAP blends. The results were used to evaluate methods to develop high-performance granular layer for pavement construction through proper compaction and control of RAP usage. The resilient modulus and accumulative deformation characteristics were determined in relation to RAP content, relative density, compaction method, stress level, stress state and the number of load applications. The effects of RAP content and density on the CBR values of aggregate-RAP blends under various conditions were also investigated. In addition, the effect of small strain cyclic loading on shear strength of aggregate-RAP blends was observed in laboratory tests. Results from this investigation demonstrated that: 1) adding RAP to natural aggregates may increase the resilient modulus of natural aggregates, and optimum content can be found to achieve the highest resilient modulus; 2) resilient modulus generally increases with density; higher density of aggregate-RAP blends can be achieved by using methods combining vibration and static loading. 3) deviatoric stress has more pronounced influence on accumulative deformation than confining pressure. 4) proper compaction method can reduce accumulative deformation of samples. 5) addition of RAP into aggregates results in little change in accumulative deformation when the RAP content is less than a threshold. 6) CBR value decreases with increasing RAP content and decreasing compaction effort or compacted dry density. 7) shear strength of an aggregate-RAP blend tends to increase after small strain cyclic loading. / Thesis / Master of Applied Science (MASc)

This thesis broadly addresses the issue of materials sustainability in the production of Portland cement concrete. Two methods are presented, both aimed at achieving more sustainable concrete through the use of waste and recycled materials. The first method involves utilizing reclaimed asphalt pavement (RAP) as an aggregate in structural concrete, and the second method involves utilizing waste quarry fines as partial replacement of Portland cement in concrete mixes. Many efforts have been made in recent years to justify the use of RAP aggregates in concrete. All previous efforts appear to unanimously report a reduction in concrete performance with varying proportions of RAP usage. The poor performance of RAP aggregates in concrete is attributed mainly to a larger, more porous interfacial transition zone (ITZ) and to the cohesive failure of the asphalt. It is hypothesized that the detrimental impact on the ITZ is attributable to organic compounds leached from the asphalt in the high pH pore solution. This study proves the presence of organic compounds in the pore solution and demonstrates that there is an apparent retardation of cement hydration. This study also attempted to pretreat the RAP in a sodium hydroxide (NaOH) solution to pre-leach the organic compounds. The pretreatment demonstrated that organic compounds were leached and that NaOH modified the asphalt surface chemistry. However, only a marginal improvement in compressive strength was observed by completing the pretreatment. Replacement of Portland cement by filler products is a practice aimed at reducing the carbon footprint of concrete, such as is common with Type IL Portland limestone cement. This study investigates the impact of replacing cement with seven different quarry fines materials. The quarry fines were used to replace cement at 5% to 20% by volume in either cement paste or mortar samples that were then analyzed for various physicochemical properties. It was found that all the quarry fines had detrimental impact on the hydration kinetics of cement pastes. The inclusion of quarry fines was also found to cause varying degrees of reduction in mortar compressive strength. While further analyses of the quarry fines are required, quarry fines 2, 5 and 7 did display encouraging signs to suggest the potential for use as a filler material in blended cements. / Master of Science / This thesis broadly addresses the issue of sustainability in the cement and concrete industry. Sustainability is a significant problem for the cement and concrete industry due to the large amount of carbon emissions produced in the manufacturing process of Portland cement. One method to reduce the carbon footprint of concrete is to use recycled aggregates, and reclaimed asphalt pavement (RAP) is investigated in this thesis as a recycled aggregate option. Previous studies have shown that the use of RAP in concrete results in poor mechanical performance when compared to conventional concrete. In this thesis, the RAP was pretreated by soaking it in sodium hydroxide (NaOH) to see if any improvement is noted. It was determined that the pretreatment resulted in marginal improvements in concrete performance. Another method to reduce the carbon footprint of concrete is through the use of substitutions of Portland cement. In this thesis, quarry fines from around Virginia were investigated for potential as substitutive material. Quarry fines are a by-product from quarrying operations and are often considered a waste material because they have limited applications. This study analyzed the performance of cementitious materials prepared with various substitutive percentages of quarry fines and found that, in general, the inclusion of quarry fines resulted in a decrease of mechanical performance. In total, seven quarry fines were tested and only two showed potential for use as a substitution in Portland cement concrete. These two investigations are essential in reaching the goal of reducing the carbon footprint of the cement and concrete industry.

This thesis investigates the effect of added asphalt binder content on the performance and volumetric properties of asphalt concrete mixes containing Reclaimed Asphalt Pavement (RAP). Mixes with three different percentages of RAP (0%, 20%, 40%) obtained from an asphalt producer and three different percentages of asphalt binder (design asphalt content, design +0.5%, and design +1.0%) were evaluated. Additionally, a laboratory produced mix containing 100% RAP with four asphalt binder contents (0.0%, 0.5%, 1.0% and 1.5%) was also evaluated in order to determine the binder level that optimizes mix performance for the extreme case in RAP utilization. Performance of the mixtures was evaluated based on three criteria: stiffness (dynamic modulus), fatigue resistance (flexural beam), and rutting resistance (flow number). Results showed that a 0.5% increase in binder content improved both the fatigue and rutting resistance of the 0% and 20% RAP mixes with only slight decreases in dynamic modulus. However, the addition of various amounts of binder to the 40% RAP mix led to a significant decrease in rutting resistance with little or no improvement to fatigue resistance. Volumetric analysis was performed on all of the mixes to determine how the added binder content affected mix volumetric properties. Results of volumetric testing, specifically asphalt content and Voids in the Total Mix (VTM) at the design compaction effort, Ndesign, revealed that the 40% RAP mix incorporated a significantly higher level of binder during plant production which very likely contributed to the decrease in rutting resistance once additional binder was added in the laboratory. Additionally, the gyratory compaction effort that would result in 4 percent VTM at the optimal binder content over the three performance tests, N4%, was calculated for each mix. Results indicated that the VTM for the optimally performing 20% and 40% RAP mixes were well below current Virginia Department of transportation (VDOT) production standards. In addition, N4%, for the optimally performing 20% and 40% RAP mixes was 50% or less than the current design compaction effort of 65 gyrations. / Master of Science

Master of Science / Department of Civil Engineering / Mustaque Hossain / The ultra-thin bonded bituminous surface (UBBS), popularly known as Novachip, is a thin hot-mix asphalt layer with high-quality, gap-graded aggregates bonded to the existing surface with a polymer-modified emulsion membrane. This thin surfacing improves ride quality, reduces road-tire noise, minimizes back spray, and increases visibility under wet conditions. The Kansas Department of Transportation (KDOT) has been using UBBS since 2002. Performance of this thin surface treatment strategy has been good in Kansas and elsewhere. However, some of these projects are now being rehabilitated. The objective of this study is to evaluate whether reclaimed asphalt pavement (RAP) materials from existing UBBS layers can be used in chip seal and Superpave mixtures. UBBS millings were studied with two different polymer-modified emulsions to assess their performance as precoated aggregates in chip seal. The ASTM D7000-04 sweep test was used to assess chip retention of UBBS millings. Three different mix designs were developed for both 12.5-mm and 9.5-mm nominal maximum aggregate size (NMAS)Superpave mixtures using a PG 70-22 asphalt binder and three different percentages (0%, 10%, and 20%) of reclaimed UBBS materials. The designed Superpave mixes were then tested for performance in terms of rutting and stripping using the Hamburg wheel tracking device (HWTD)and moisture sensitivity by modified Lottman tests. Sweep test results showed that UBBS millings did not improve chip retention. Superpave mix design data indicated volumetric properties of Superpave mixes with UBBS millings met all requirements specified by KDOT. HWTD and modified Lottman test results indicated all designed mixes performed better with the addition of UBBS millings as RAP materials. Field performance of UBBS projects was also evaluated. It was found that pavements treated with UBBS showed high variability in service life with majority serving six years. Before and after (BAA) studies showed that UBBS reduces pavement roughness, transverse and fatigue cracking one year after the treatment. However, no consistent improvement in rutting condition was found.