Thesis (Ph. D.)--University of Missouri-Columbia, 1997. / TM in title is superscripted on title page. Typescript. Vita. Includes bibliographical references (leaves 100-103). Also available on the Internet.

Thesis (Ph. D.)--University of Missouri-Columbia, 1997. / TM in title is superscripted on title page. Typescript. Vita. Includes bibliographical references (leaves 100-103). Also available on the Internet.

Thesis (Ph. D.)--University of Texas at Austin, 2008. / Vita. Includes bibliographical references.

Thesis (M.S. in Mechanical Engineering)--Naval Postgraduate School, June 2004. / Thesis Advisor(s): Terry McNelley. Includes bibliographical references (p. 41-43). Also available online.

Thesis (Ph. D.)--University of Texas at Austin, 2004. / Supervisor: Eric M. Taleff. Vita. Includes bibliographical references.

Some metals, such as Ti-6Al-4V, have a high elongation to failure when strained at certain rates and temperatures. Superplastic forming is the utilisation of this property, and it can be used to form thin, geometrically complex components. Superplastic forming is a slow process, and this is one of the reasons why it is an expensive manufacturing process. Localised thinning occurs if the specimen is strained too quickly, and components with locally thin wall thickness fail prematurely. The goal of this study is to find a technique that can be used to minimise the forming time while limiting the minimum final thickness. The superplastic forming process is investigated with the finite element method. The finite element method requires a material model which describes the superplastic behaviour of the metal. Several material models are investigated in order to select a material model that can show localised thinning at higher strain rates. The material models are calibrated with stress-strain data, grain size-time data and strain rate sensitivity-strain data. The digitised data from literature is for Ti-6Al-4V with three different initial grain sizes strained at different strain rates at 927 C. The optimisation of the forming time is done with an approximate optimisation algorithm. This algorithm involves fitting a metamodel to simulated data, and using the metamodels to find the optimum instead of using the finite element model directly. One metamodel is fitted to the final forming time results, and another metamodel is fitted to the final minimum thickness results. A regressive radial basis function method is used to construct the metamodels. The interpolating radial basis function method proved to be unreliable at the design space boundaries due to non-smooth finite element results. The non-smooth results are due to the problem being path dependent. The final forming time of the superplastic forming of a rectangular box was successfully minimised while limiting the final minimum thickness. The metamodels predicted that allowing a 4% decrease in the minimum allowable thickness (1.0 mm to 0.96 mm) and a 1 mm gap between the sheet and the die corner the forming time is decreased by 28.84%. The finite element verification indicates that the final minimum thickness reduced by 3.8% and that the gap between the sheet and the die corner is less than 1 mm, resulting in the forming time being reduced by 28.81%. / Dissertation (MEng)--University of Pretoria, 2017. / Mechanical and Aeronautical Engineering / MEng / Unrestricted

<p>The field of superplasticity is reviewed, with particular reference to the mode of deformation and viability for industrial application. Superplastic and conventional Zn-Al eutectoid alloys are compared with regard to the pressures and time required and the problems associated with the production of shaped hollow components from billet material, using extrusion followed by pressure forming. A possible industrial process is suggested and economically assessed in a Supplement to the Dissertation. </p> / Thesis / Master of Engineering (ME)

Approved for public release, distribution is unlimited / This study evaluated dome test samples of a superplastic AA5083 aluminum alloy deformed at nominally constant strain rates under biaxial strain conditions. Dome test samples resulted from gas-pressure forming of sheet material; for this study, samples were deformed at strain rates corresponding either to grain boundary sliding or dislocation creep control of deformation. Orientation Imaging Microscopy was utilized to determine texture development, grain size and grain-to-grain misorientation angle distributions for locations located along a line of latitude of the dome samples. The goal was to identify the location of the transition from grain boundary sliding to dislocation creep. Grain boundary sliding, which dominates at lower strain rates, can be recognized by a randomized texture and a higher concentration of high disorientation angles. Dislocation creep, which dominates at higher strain rates, is characterized by fiber texture formation and development of a peak at lower angles in the grain-to-grain misorientation angle distribution. / Ensign, United States Navy

This thesis was developed in the frame of a Brazil-France cooperation agreement between the École des Mines d\'Albi-Carmaux and the Polytechnic School of Engineering of the University of Sao Paulo (EPUSP). It aims to contribute to the study of the mechanical behaviour of Ti6Al4V alloys especially in terms of superplastic forming. The general objective of this research is to develop non-conventional forming processes for new titanium alloys applied to aerospace components Therefore, in accordance of the equipment\'s available in the two groups, the work will be conducted either at the Ecole des Mines d\'Albi-Carmaux and either at EPUSP. This thesis aims to answer questions such as what are the implications in relation to the microstructural and mechanical behaviour of these alloys during superplastic and hot forming in order to establish a behaviour law for these alloys based on titanium. This requires a good knowledge of the properties of materials used in the superplastic and hot forming domain to control the parameters governing the phenomenon of superplasticity or high temperature plasticity. For this, a testing strategy and characterization methodology of those new titanium alloys was developed. The tests include high temperature uniaxial tensile tests on several Ti6Al4V alloys showing different initial grain sizes. Special focus was made on the microstructural evolution prior to testing (i.e. during specimen temperature increase and stabilization) and during testing. Testing range was chosen to cover the hot forming and superplastic deformation domain. Grain growth is depending on alloy initial microstructures but also on the duration of the test at testing temperature (static growth) and testing strain rate (dynamic growth). After testing microstructural evolutions of the alloys will be observed by optical micrograph or SEM and results are used to increase behaviour model accuracy. Advanced unified behaviour models where introduced in order to cover the whole strain rate and temperature range: kinematic hardening, strain rate sensitive and grain growth features are included in the model. In order to get validation of the behaviour model, it was introduced in ABAQUSR numerical simulation code and model predictions (especially macroscopic deformation and local grain growth) were compared, for one of the material investigated, to axisymmetric inflation forming tests of sheet metal parts, also known as bulge test. To obtain a simple control cycle, tests performed at IPT/LEL laboratory in San José Dos Campos in Brazil were operated with a constant strain rate. Results show a very good correlation with predictions and allows to conclude on an accuracy of the behaviour models of the titanium alloys in industrial forming conditions. / Esta tese desenvolvida dentro do acordo de cooperação internacional celebrado entre a Escola Politécnica da Universidade de São Paulo (EPUSP) e a École des Mines d\'Albi-Carmaux tem como tema principal a análise da influência da evolução microestrutural sobre o comportamento mecânico de chapa de liga de titânio - Ti-6Al- 4V sob condições superplásticas e trabalho a quente. O objetivo desta pesquisa é contribuir para o desenvolvimento de processos de conformação não convencional de chapas de ligas a base de titânio utilizadas na manufatura de componentes metálicos. Como objetivo específico, estabelecer uma correlação entre comportamento mecânico e a mudança microestrutural a partir de três tipos de ligas com diferentes tamanhos de grão iniciais (0.5, 3.0 e 4.9 ?m). Os testes foram realizados na faixa de temperatura de 700 a 950 °C combinados às taxas de deformação na faixa de 10-1 s-1 - 10-4 s-1. Para a metodologia, estabeleceu-se uma estratégia de ensaios mecânicos capaz de testar as hipóteses sobre o comportamento do material formuladas no início desta pesquisa. Em seguida, os ensaios mecânicos foram divididos em três partes. Na primeira, utilizou-se um simulador termomecânico modelo Gleeble 3800 para os ensaios a quente variando-se a taxa de deformação (??) entre 10-1 s-1 a 10-3 s-1 e temperaturas da ordem de 700 °C a 850 °C. Na segunda parte dos testes, priorizouse taxas de deformação mais lentas (10-2 s-1 - 10-4 s-1) e temperaturas mais elevadas (800 °C - 950 °C) objetivando atingir as deformações superplásticas do material, nesta etapa utilizou-se como equipamento uma máquina de tração modelo MTS 50kN com câmara de aquecimento acoplada. A terceira parte dos ensaios experimentais envolveu a conformação na condição superplástica por pressão hidrostática (Bulge test) realizadas no LEL-IPT de São José dos Campos. A partir da análise dos dados experimentais levantou-se os parâmetros introduzidos no modelo numérico de comportamento mecânico baseado na evolução da microestrutura da chapa testada permitindo a calibração do modelo numérico a partir das equações constituintes e finalmente introduzido no software de elementos finitos (ABAQUS 6.12) e construído a simulação numérica da conformação superplástica por pressão hidrostática. Os principais resultados indicaram uma forte correlação entre microestrutura inicial da conformação superplástica e a quente de onde se pode observar que tanto menor a microestrutura inicial maior será a quantidade do crescimento de grão. Os resultados da conformação superplástica de expansão multiaxial do domo hemisférico foram, então, comparados à simulação numérica permitindo confrontar os dados do modelo numérico do comportamento mecânico com a lei de comportamento estudada, o que possibilitou um melhor entendimento dos mecanismos da conformação plástica em condições de superplasticidade e também de trabalho a aquente do material.

Superplastic forming (SPF) is a near net-shape forming process which offers many advantages over conventional forming operations including low forming pressure due to low flow stress, low die cost, greater design flexibility, and the ability to shape hard metals and form complex shapes. However, low production rate due to slow forming process and limited predictive capabilities due to lack of accurate constitutive models for superplastic deformation, are the main obstacles to the widespread use of SPF. Recent advancements in finite element tools have helped in the analysis of complex superplastic forming operations. These tools can be utilized successfully in order to develop optimized superplastic forming techniques. In this work, an optimum variable strain rate scheme developed using a combined micromacro stability criterion is integrated with ABAQUS for the optimization of superplastic forming process. Finite element simulations of superplastic forming of Ti-6Al-4V sheet into a hemisphere and a box are carried out using two different forming approaches. The first approach is based on a constant strain rate scheme. The second one is based on the optimum variable strain rate scheme. It is shown that the forming time can be significantly reduced without compromising the uniformity of thickness distribution when using the proposed optimum approach. Further analysis is carried out to study the effects of strain rate, microstructural evolution and friction on the formed product. Finally the constitutive equations and stability criterion mentioned above are used to analyze the forming of dental implant superstructure, a modern industrial application of superplastic forming.