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Gas turbine vanes find themselves in very hostile environments – extremely high temperature combustion gases, much exceeding material melting temperatures, flowing over them at enormous pressures. It is necessitated due to the increased efficiency and power output at these conditions. However, this also means that, in spite of the technological advancements made, these parts need frequent repairing compared to parts placed in milder environments. Primarily due to economic reasons, gas turbine parts are repaired by companies other than the original equipment manufacturer (OEM). While multitude of condition monitoring techniques have been developed and are used in the industry for regular maintenance checks, there is no easy way to characterize the impact on thermal performance of the repairing processes involved. This thesis reports the development of a technique to address this issue. It also chronicles the test rig design, experiments conducted, development and significance of the thermal performance metric. Heated air (250 ̊C – 300 ̊C) is flown through the internal cooling passages of 8 samples each of OEM and repaired parts at two different pressure ratios (vane inlet over ambient pressure), 1.1 and 1.3. First, steady state mass flow rates through each airfoil (one part is a cluster of 4 airfoils) is experimentally determined and compared among the OEM and repaired sample sets. Second, a transient experiment is run and the surface temperatures of the airfoils are measured using multiple infrared cameras viewing both the pressure and suction side of the airfoils. A parameter involving localized vane surface temperature, airfoil inlet temperature and ambient temperature is formulated to characterize the vane thermal performance. Using statistical analysis, it is found that there is no significant difference between the OEM and repaired samples tested. The development of the discussed technique, it is expected, will help companies in the gas turbine vane repairing business to qualify their parts in a robust and efficient manner without the need to invest a lot of money in buying precision equipment, or, control chambers. Finally, a couple of further studies are recommended to further improve the qualifying procedure and thereby increase the efficiency of the technique. / Master of Science

The study of flow fields and heat transfer characteristics inside a gas turbine combustor provides one of the most serious challenges for gas turbine researchers because of the harsh environment at high temperatures. Design improvements of gas turbine combustors for higher efficiency, reduced pollutant emissions, safety and durability require better understanding of combustion in swirl flows and thermal energy transfer from the turbulent reacting flows to solid surfaces. Therefore, accurate measurement and prediction of the flows and heat loads are indispensable. This dissertation presents flow details and wall heat flux measurements for reacting flow conditions in a model gas turbine combustor. The objective is to experimentally investigate the effects of combustor operating conditions on the reacting swirl flows and heat transfer on the liner wall. The results shows the behavior of swirling flows inside a combustor generated by an industrial lean pre-mixed, axial swirl fuel nozzle and associated heat loads. Planar particle image velocimetry (PIV) data were analyzed to understand the characteristics of the flow field. Experiments were conducted with various air flow rates, equivalence ratios, pilot fuel split ratios, and inlet air temperatures. Methane and propane were used as fuel. Characterizing the impingement location on the liner, and the turbulent kinetic energy (TKE) distribution were a main part of the investigation. Proper orthogonal decomposition (POD) further analyzed the data to compare coherent structures in the reacting and non-reacting flows. Comparison between reacting and non-reacting flows yielded very striking differences. Self-similarity of the flow were observed at different operating conditions. Flow temperature measurements with a thermocouple scanning probe setup revealed the temperature distribution and flow structure. Features of premixed swirl flame were observed in the measurement. Non-uniformity of flow temperature near liner wall was observed ranging from 1000 K to 1400 K. The results provide insights on the driving mechanism of convection heat transfer. As a novel non-intrusive measurement technique for reacting flows, flame infrared radiation was measured with a thermographic camera. Features of the flame and swirl flow were observed from reconstructed map of measured IR radiation projection using Abel transformation. Flow structures in the infrared measurement agreed with observations of flame luminosity images and the temperature map. The effect of equivalence ratio on the IR radiation was observed. Liner wall temperature and heat transfer were measured with infrared thermographic camera. The combustor was operated under reacting condition to test realistic heat load inside the industrial combustors. Using quartz glass liner and KG2 filter glass, the IR camera could measure inner wall surface temperature through the glass at high temperature. Time resolved axial distributions of inner/outer wall temperature were obtained, and hot side heat flux distribution was also calculated from time accurate solution of finite difference method. The information about flows and wall heat transfer found in this work are beneficial for numerical simulations for optimized combustor cooling design. Measurement data of flow temperature, velocity field, infrared radiation, and heat transfer can be used as validation purpose or for direct inputs as boundary conditions. Time-independent location of peak location of liner wall temperature was found from time resolved wall temperature measurements and PIV flow measurements. This indicates the location where the cooling design should be able to compensate for the temperature increase in lean premixed swirl combustors. The characteristics on the swirl flows found in this study points out that the reacting changes the flow structure significantly, while the operating conditions has minor effect on the structure. The limitation of non-reacting testing must be well considered for experimental combustor studies. However, reacting testing can be performed cost-effectively for reduced number of conditions, utilizing self-similar characteristics of the flows found in this study. / Ph. D.

Energy conservation, efficiency, and environmental responsibility are priorities for modern energy technologies. The ever increasing demands for lower pollutants and higher performance have driven the development of low-emission gas turbine engines, operating at lean equivalence ratios and at increasingly higher turbine inlet temperatures. This has placed new constraints on gas turbine combustor design, particularly in regards to the cooling technologies available for the combustor liner walls. To optimize combustor thermal management, and in turn optimize overall engine performance, detailed measurements of the flame side heat transfer are required. However, given the challenging environment at which gas turbine combustors operate, there are currently only limited studies that quantify flame side combustor heat transfer; in particular at reacting conditions. The objective of the present work was to develop methodologies to measure heat transfer within a reacting gas turbine combustor. To accomplish this, an optically accessible research combustor system was designed and constructed at Virginia Tech, capable of operating at 650 K inlet temperature, maximum air mass flow rates of 1.3 kg/s, and flame temperatures over 1800 K. Flow and heat transfer measurements at non-reacting and reacting conditions were carried out for Reynolds numbers (Re) with respect to the combustor diameter ranging from ~11 500 to ~140 000 (depending on the condition). Particle Image Velocimetry (PIV) was used to measure the non-reacting flow field within the burner, leading to the identification of coherent structures in the flow that accounted for over 30% of the flow fluctuation kinetic energy along the swirling jet shear layers. The capability of infrared (IR) thermography to image surface temperatures through a fused silica (quartz) glass was demonstrated at non-reacting conditions. IR thermography was then used to measure the non-reacting steady state heat transfer along the combustor liner. A peak in heat transfer was identified at ~1 nozzle diameter downstream of the combustor dome plate. The peak Nusselt number along the liner was over 18 times higher than that predicted from fully developed turbulent pipe flow correlations, which have traditionally been used to estimate flame side combustor heat transfer. For the reacting measurements, a novel time-dependent heat transfer methodology was developed that allowed for the investigation of transient heat loads, including those occurring during engine ignition and shutdown. The methodology was validated at non-reacting conditions, by comparing results from an experiment with changing flow temperature, to the results obtained at steady state. The difference between the time-dependent and the steady state measurements were between 3% and 17.3% for different mass flow conditions. The time-dependent methodology was applied to reacting conditions for combustor Reynolds numbers of ~12 000 and ~24 000. At an equivalence ratio of ~0.5 and a combustor Reynolds number of ~12 000, the peak heat load location in reaction was shifted downstream by 0.2 nozzle diameters compared to the non-reacting cases. At higher equivalence ratios, and more visibly at a Reynolds number of ~24 000, the heat transfer distribution along the combustor liner exhibited two peaks, upstream and downstream of the impingement location (X/DN=0.8-1.0 and X/DN=2.5). Reacting PIV was performed at Re=12 000 showing the presence of a strong corner recirculation, which could potentially convect reactants upstream of the impingement point, leading to the double peak structure observed. The methodologies developed have provided insight into heat transfer within gas turbine combustors. The methods can be used to explore additional conditions and expand the dataset beyond what is presented, to fully characterize reacting combustor heat transfer. / Ph. D.

Skin temperature plays an important role in human thermoregulation together with core temperature. Skin temperature varies to a large extent across the body and this is especially pronounced in cold environments. The variations of skin temperature are also involved in the generation of regional thermal perceptions that can lead to behavioural adjustments. Whilst the temporal and inter-individual variations of skin temperature have been well studied using contact sensors, the knowledge of spatial variations has received less attention in the literature. Infrared thermography is a specific imaging technique particularly valuable for the exploration of the topography or pattern of skin temperature across the body. Most research using this technique has only been case studies or experiments focused in one specific body region. However, extensive regional skin temperature data over the whole-body can be proven useful for different types of applications including the sport clothing industry in combination with other body-mapping data. The primary aim of this thesis was to develop an original and standardised method using infrared thermography enabling whole-body skin temperature data to be compared for the assessment of spatial, temporal and inter-individual variations. A specific methodology for infrared data collection and data processing was successfully developed in order to combine data from a variety of participants varying in anthropometrical characteristics. The main outcomes were the production of several skin temperature body maps, either absolute maps to show the magnitude of the temporal or inter-individual effects, and normalised maps (relative to mean skin temperature) allowing for topographical comparisons between protocol stages, populations or interventions. The second aim of the thesis was to extend the understanding of the skin temperature patterns and how these could relate with thermal perceptions. The body-mapping method gave the opportunity to investigate a large amount of conditions, where various internal or external determinants of skin temperature were be involved. This was mainly done in cool to cold environments (5°C to 20°C) where skin temperature is not uniform but is associated with local and overall comfort. Studies were firstly performed in semi-nude conditions (Chapter 3, 4, 5) and then in clothed conditions (Chapter 6 and 7). The semi-nude studies were designed to explore the potential sexdifferences in regional skin temperature responses whilst running (Chapter 3) with a special interest in the role of skinfold thickness, this was further extended with a group of males at rest having a large variety of fat content and thickness (Chapter 4). The influence of exercise type and air temperature on skin temperature patterns was studied with a rowing exercise (Chapter 5). Studies were then performed in clothed conditions (Chapter 5, 6). The influence of real-life conditions on skin temperature patterns and associated perceptual responses was observed during a hiking scenario (Chapter 6). Following these descriptive studies, manipulation of skin temperature patterns was performed using clothing in order to determine the presence of any relevant effect on thermal comfort (Chapter 7). Our results demonstrated that the skin temperature pattern over the whole-body is relatively universal with several features being consistently found regardless of the conditions or the populations. The upper body is usually warmer than the lower body and the body creases (orbital, elbow regions etc.) are also warmer than surrounding regions. A Y-shape of colder temperatures has been highlighted over the anterior torso as well as a T- or Y-shape of warmer temperature over the posterior torso. There are yet some specificities that can be displayed due to active muscles during exercise such as the warmer skin overlying the trapezius and biceps muscles in rowing (Chapter 5), the influence of the backpack construction with up to 3°C warmer skin temperature in the lower back (Chapter 6) or the importance of additional clothing insulation minimizing the anterior Y-shape of colder skin temperatures (Chapter 7). Beyond the thermal patterns, absolute skin temperature differences have been observed between sexes with females displaying 2°C colder skin during semi-nude running (Chapter 3) and 1°C colder skin during clothed walking (Chapter 6)compared to males. The skin temperature difference can also be as large as 6°C colder skin for an obese male compared to a very lean male (40% vs 7% body fat). Despite these differences, there were almost no significant differences in overall and regional thermal sensations and comfort between sexes or between males with varying body fat. Our results focused on body fat revealed that overall fat content and sum of skinfolds was inversely associated with the mean skin temperature response during various protocols (Chapter 4, 6, 7). Local skinfold thickness explained the inter-individual variability of local skin temperature for resting (Chapter 4) and exercising males (Chapter 7) in most body regions. In terms of intra-individual variations, the distribution of skinfold thickness across the anterior torso explained the distribution of skin temperature in this segment solely in conditions with strong regional contrasts (Chapter 3, 4 and 7). When the whole-body skin temperature pattern is considered, our body-mapping approach failed to show relationships between skin temperature distribution across the body and regional skinfold thickness distribution neither at rest nor during exercise. The relative contribution of other internal determinants such as local heat production,local blood flow distribution and local anthropometry should be further investigated to fully elucidate the spatial skin temperature variations depending on the climate, clothing and the body thermal state. Lastly, there was a trend towards improved thermal comfort during rest and exercise in the cold through a manipulation of skin temperature patterns targeting the naturally cold body regions with high insulation, therefore obtaining a more homogeneous skin temperature distribution across the body (Chapter 7). The present work will benefit the sport goods industry. The descriptive results of skin temperature variations will be useful in order to validate multi-segmental model of human thermoregulation. Further work can include pattern predictions for exercise types and conditions not covered by the present thesis. The skin temperature maps will mainly feed the general body-mapping approach for clothing design taking into account several other body mapping data such as sweat mapping and the combination of cold, warm and wetness sensitivity mappings. Lastly, the present results have highlighted the interest for targeted solutions and also the need for more evolutive systems in the field of cold weather apparel.

<p>Microscale environments provide significant resolution and distortion challenges with respect to measurement techniques; however, with improvements to existing techniques, it is possible to gather relevant data to better understand the thermal and fluidic mechanisms at such small scales in evaporating droplets.</p> <p> </p> <p>Infrared thermography provides several unique challenges at small scales. A primary issue is that the low native resolution of traditional infrared cameras significantly hamper the collection of details of microscale features. Furthermore, surfaces exhibiting vastly different emissivities, results in inaccurate temperature measurements that can only be corrected with irradiance-based emissivity maps of the surface; however, due to the resolution limitations of infrared thermography, these emissivity maps can also display significant errors. These issues are overcome through the use of multi-frame super-resolution. The enhanced resolution allows for better capture of microscale features, therefore, enhancing the emissivity map. A quantitative error analysis of the system is conducted to quantify the feature size resolution improvement as well as the smoothing effect of super-resolution reconstruction. Furthermore, a sensitivity analysis is conducted to quantify the impact of registration uncertainty on the accuracy of the reconstruction. Finally, the improved emissivity map from super-resolution is demonstrated to show the increased accuracy over low-resolution mapping.</p> <p> </p> <p>When applied to water droplets, particularly on nonwetting surfaces, infrared thermography is confounded by the presence of nonuniform reflectivities due to the spherical curvature of the liquid-air interface. Thus, when measuring the temperature along the vertical axis of a water droplet, it is necessary to correct the reflection. Using a controlled background environment, in conjunction with the Fresnel equations, it is possible to correct the reflective effects on the interface and calculate the actual temperature profile. This allows for a better understanding of the governing mechanisms that determine the thermal transport within the droplet. While thermal conduction is the primary transport mechanism along the vertical axis of the droplet, it is determined that the temperature drop is partially dampened by the convective transport from the ambient air to the liquid interface. From this understanding revealed by the measurements, the vapor-diffusion-based model for evaporation was enhanced to better predict evaporation rates.</p> <p> </p> <p>Further exploration into the mechanisms behind droplet evaporation on nonwetting surfaces requires accurate knowledge of the internal flow behavior. In addition, the influence of the working fluid can have a significant impact on the governing mechanisms driving the flow and the magnitude of the flowrate. While water droplet evaporation has been shown to be governed by buoyancy-driven convection on nonwetting substrates, similar studies on organic liquid droplets are lacking. Particle image velocimetry is effective at generating a velocity flow field, but droplets introduce distortion due to the refraction from the spherical interface of the droplet. As such, velocity correction using a ray-tracing approach was conducted to correct the velocity magnitudes and direction. With the velocity measurements, the flow was determined to be surface-tension-driven and showed speeds that are an order of magnitude higher than those seen in buoyancy-driven flow in water droplets. This resulted in the discovery that advection plays a significant role in the transport within the droplet. As such, the vapor-diffusion-governed evaporation model was adjusted to show a dramatic improvement at predicting the temperature gradient along the vertical axis of the droplet.</p> <p> </p> <p>Armed with the knowledge of flow behavior inside droplets, it is expected that droplets with aqueous solutions should exhibit buoyancy-driven convection. The final part of this work, therefore, leverages this phenomenon to enhance mixing during reactions. Colorimetry is a technique that is widely utilized to measure the concentration of a desired sample within some liquid; the sample reacts with a reagent dye the color change is measured, usually through absorbance measurements. In particular, the Bradford assay is used to measure protein concentration by reacting the protein to a Coomassie^TM Brilliant Blue G-250. The absorbance of the dye increases, most significantly at the 590 nm wavelength, allowing for precise quantitation of the amount of protein in the solution. A droplet-based reaction chamber with buoyancy-enhanced mixing has the potential to speed up the measurement process by removing the need for a separate pre-mixing step. Furthermore, the reduced volume makes the process more efficient in terms of reactant usage. Experimental results of premixed solutions of protein sample and reagent dye show that the absorbance measurement through a droplet tracks strongly with the protein concentration. When the protein sample and dye reagent are mixed <i>in situ</i>, the complex interaction between the reactants, the mixing, and the adsorption of protein onto the substrate creates a unique temporal evolution in the measured absorbance of the droplet. The characteristic peaks and valleys of this evolution track strongly with concentration and provide the framework for measurement of concentration in a droplet-based system.</p> <p> </p> <p>This thesis extends knowledge about droplet thermal and fluidic behavior through enhanced measurement techniques. This knowledge is then leveraged in a novel application to create a simple, buoyancy-driven colorimetric reaction setup. Overall, this study contributes to the field of miniaturized, efficient reaction and measurement devices.</p>

Cette étude présente une analyse thermomécanique du comportement en fatigue oligocyclique du polyamide 6.6 vierge et renforcé de fibres de verre courtes. Des bilans d'énergie sont réalisés en utilisant, de façon combinée, des techniques d'imagerie quantitative visible et infrarouge. Les champs de température sont obtenus par thermographie et les champs de déformation par corrélation d'images. Sur un cycle de chargement, on montre comment il est possible d'estimer séparément les sources de chaleurs moyennes par cycle, sources associées aux mécanismes dissipatifs et induites par les effets de couplage thermomécanique. On montre ensuite, pour différentes fréquences de chargement, l'évolution du bilan de puissance moyen par cycle sur une zone matérielle correspondant à la partie utile de l'éprouvette. Ce bilan prend en compte le taux de l'énergie de déformation, les chaleurs mises en jeu et les variations d'énergie interne. On observe que la forme du bilan de puissance est très fortement dépendante, pour un rapport de charge donné, à la fréquence de sollicitation, à la teneur en eau, à l'orientation des fibres de verre mais aussi aux niveaux de contrainte appliqués. / This study presents a thermomechanical analysis of fatigue behavior of pure and short glass- fiber reinforced polyamide 6.6. The energy balances are drew up using the combined application of visible and infrared quantitative imaging techniques. Temperature fields are obtained by thermography and strain fields by image correlation. Over one complete cycle, we show how it is possible to separately estimate the heat sources averaged over the cycle, associated with dissipative mechanisms and induced by thermomechanical coupling source effets. Then we show, for different loading rates, the time courses of the energy rate balance for a physical area corresponding to the gage part of the specimen. This balance takes into account the deformation energy rate, the heat sources and the internal energy variations. It is observed that the shape of the energy rate balance is highly dependent, for a given load ratio, to the load rate, the water content, the orientation of the glass fibers and the applied stress levels.

Laminados compósitos com matrizes poliméricas, respectivamente termorrígida e termoplástica, reforçadas com fibras contínuas de carbono foram submetidos a impacto único transversal com diferentes níveis de energia. Os danos imprimidos aos materiais estruturais foram avaliados por termografia ativa infravermelha na modalidade transmissão. Em geral, os termogramas do laminado termoplástico apresentaram indicações mais claras e bem definidas dos danos causados por impacto, se comparados aos do compósito termorrígido. O aquecimento convectivo das amostras por fluxo controlado de ar se mostrou mais eficaz que o realizado por irradiação, empregando-se lâmpadas incadecentes. Observou-se também que tempos mais longos de aquecimento favoreceram a visualização dos danos. O posicionamento da face impactada do espécime, relativamente à câmera infravermelha e à fonte de calor, não afetou a qualidade dos termogramas no caso do laminado termorrígido, enquanto que influenciou significativamente os termogramas do compósito termoplástico. Os resultados permitiram concluir que a termografia infravermelha é um método de ensaio não-destrutivo simples, robusto e confiável para a detecção de danos por impacto inferior à 5 Joules em laminados compósitos poliméricos reforçados com fibras de carbono. / Continuous carbon fiber-reinforced thermosetting and thermoplastic composite laminates were exposed to single transversal impact with different energy levels. The damages marked to the structural materials were evaluated by active infrared thermography in transmission mode. In general, the thermoplastic laminate thermograms showed more clear and delineated damage indications when compared to the ones from thermosetting composite. The convective heating of the samples by controlled hot air flow was more efficient than via irradiation using lamp. It was also observed that longer heating times improved the damage visualization. The positioning of the specimen´s impacted face regarding the infrared camera and the heating source did not affect the thermo-imaging of thermosetting specimens, whereas it substantially influenced the thermograms of thermoplastic laminates. The results allow concluding that infrared thermography is a simple, robust and trustworthy methodology for detecting impact damages as light as 5 Joules in carbon fiber composite laminates.

Os dados do MinistÃrio da SaÃde apontam a hipertensÃo arterial (HA) como a maior causa de morte materna no Brasil, sendo responsÃvel por 35% da taxa de 140-160 mortes maternas por 100.000 nascidos vivos, sendo sua origem, ainda, motivo de discussÃo. Com a finalidade de buscar novos elementos que permitam o entendimento desta patologia, comparamos as mÃdias das temperaturas das polpas digitais (Tp) de 81 gestantes, 50 normotensas (grupo A) e 31 hipertensas (grupo B), obtidas com termografia de infravermelho. O coeficiente de Pearson mostrou correlaÃÃo positiva entre a pressÃo arterial mÃdia e a pressÃo arterial sistÃlica (r= 0,95), pressÃo arterial diastÃlica (r=0,98) e para a mÃdia das temperaturas cutÃneas das polpas digitais (r=0,98 ). O teste t de student usado para comparaÃÃo de Tp dos grupos A e B foi estatisticamente significante (p = 0,002). A sensibilidade foi de 80%, especificidade de 48%, o VPP de 49%, o VPN de 80%, acurÃcia de 60,5%. A chance de uma paciente estar hipertensa para uma Tp acima de 34,1ÂC à de 1,6 vezes maior. ConcluÃmos a partir dos dados analisados que a mÃdia das Tp de gestantes normotensas à significativamente menor que as mÃdias das Tp de gestantes hipertensas, e que a Tp medida com termografia de infravermelho pode ser um bom preditor para triagem de pacientes normotensas que podem tornar-se hipertensas no decorrer da gravidez. / The Brasilian Healt Ministry data points out arterial hypertension (AH) as the major cause of maternal death, representing 35% of 140-160 maternal deaths for 100.000 alive newborns. Its origin remains a cause for discussion. Looking for new elements that may improve the understanding of that pathology, we studied the skin fingertips mean temperature (Tp) of pregnant women, 50 normotense (group A) and 31 hypertense (group B). The values of temperature were obtained using infrared thermography. Pearson correlation coefficient showed positive relationship between mean arterial pressure and systolic pressure (r= 0,95), diastolic arterial pressure (r=0,98) and for Tp (r=0,98 ). Student t test was statistically significant (p = 0,002) when comparing means of groups A and B. Other statistical tests obtained were: sensibility 80%, specificity de 48%, positive predictive value 49%, negative predictive value 80% and accuracy 60,5%. The chance of a pregnant woman become hypertensive is 1,6 times higher when her Tp is equal or higher then 34,1ÂC. The analyzed data indicate that Tp values of pregnant women measured with infrared thermography is statistically smaller in the group of non hypertense and that may it might become a good method to detect pregnant women with high risk to become hypertensive during pregnancy.