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Dust and hybrid mixture explosions continue to occur in industrial processes that handle fine powders and flammable gases. Considerable research is therefore conducted throughout the world with the objective of both preventing the occurrence and mitigating the consequences of such events. In the current work, research has been undertaken to help advance the field of dust explosion prevention and mitigation from an emphasis on hazards to a focus on risk. Employing the principles of quantitative risk assessment (QRA) of dust and hybrid mixture explosions, a methodological framework for the management of these risks has been developed. The Quantitative Risk Management Framework (QRMF) is based on hazard identification via credible accident scenarios for dust explosions, followed by probabilistic Fault Tree Analysis (using Relex – Reliability Excellence – software) and consequence severity analysis, represented by maximum explosion pressure, (using DESC – Dust Explosion Simulation Code – software). Identification of risk reduction measures in the framework is accomplished in a hierarchical manner by considering inherent safety measures, passive and active engineered devices, and procedural measures. Dust explosion tests to determine icing and granulated sugar dust explosibility characteristics have been achieved in a 20-L Siwek chamber, and, accordingly, DESC fuel files were built and DESC has validated. Three industrial case studies are presented to show how the QRMF could has been helpful in reducing dust and hybrid mixture explosion risk at the Imperial Sugar refinery, the Semabla grain storage silo, and a hypothetical 400-m3 polyethylene storage silo. DESC simulations and Probit equation for structural damage provide the destructive percentage of each pressure zone in the simulations, followed by probabilistic FTA that were achieved for the first two case studies, before and after applying the framework. Detailed individual and societal risks calculations were made and F-N curves plotted for the two processes. The polyethylene silo case study is presented to show how inherent safety measures can be helpful in reducing dust and hybrid mixture explosion risk. The framework showed significant risk reduction to the point where the residual risks are acceptable for both processes. Finally, assessment results are compared and improvements measured. / The research main objective is: to manage the risks of any expected dust or hybrid mixture explosion in industrial complexes (large-scale).

Call number: LD2668 .T4 1985 S562 / Master of Science

Research with heterogeneous mixtures involving solid particulate in closed, constant-volume bombs is typically limited by the powder dispersion technique. This work details the development of an experimental apparatus that promotes ideal conditions, namely a quiescent atmosphere and uniform particle distribution, for measuring laminar, heterogeneous flame propagation. In this thesis, two methods of dispersing particles are investigated. In the first, heterogeneous mixtures are made in a secondary vessel that is connected to the main experiment. Particles are dispersed into the secondary vessel by adapting a piston-driven particle injector, which has been shown to produce uniform particle distributions. The heterogeneous mixture is then transferred to the main bomb facility and ignited after laminar conditions are achieved. In the second method of dispersion, particles are directly injected into the main experimental facility using a strong blast of compressed air. As with the first approach, enough time is given (~4 minutes) for the mixture to become quiescent before ignition occurs. An extinction diagnostic is also applied to the secondary mixing vessel as well as the primary experimental facility (for both dispersion methods) to provide a qualitative understanding of the dispersion technique. To perform this diagnostic a 632.8-nm, 5-mW Helium-Neon (HeNe) laser was employed. Aluminum nano-particles with an average diameter of 100 nm were used in this study. It was found that for typical dust loadings produced with both dispersion techniques, a pure dust-air system would not ignite due to the current spark ignition system. Thus, a hybrid mixture of Al/CH4/O2/N2 was employed to achieve the project goal of demonstrating a system for controlled laminar flame speed measurements in aerosol mixtures. With the hybrid mixture, the combustion characteristics were studied both with and without the presence of nano-Al particles. Based on the experimental results, the simplicity of the "direct-injection" methodology compared to that of the "side-vessel" is desirable and will be further investigated as a viable alternative, or improvement, to the side-vessel technology.

Les explosions de mélanges de gaz inflammables/solides combustibles ne sont pas bien comprises en raison de la complexité des transferts thermiques, des mécanismes de cinétiques et des interactions entre la turbulence /combustion. L'objectif principal de ce travail est d'étudier la sévérité des explosions des nanoparticules de carbone noir/méthane afin de comprendre l'influence de l'insertion des nanoparticules sur les explosions de gaz. Des tests ont été effectués sur ces mélanges dans un tube de propagation de la flamme et dans une sphère d'explosion standard de 20 L. L'influence de la turbulence initiale et de la taille de particule élémentaire du noir de carbone a également été étudiée. Il semble que l'insertion de nanoparticules de noir de carbone augmente d'environ 10% la sévérité de l’explosion pour les mélanges pauvres en méthane. Par conséquent, il semble que les nanoparticules ont un impact sur la sévérité de l'explosion même pour les systèmes à basse turbulence, contrairement aux systèmes impliquant des poudres de taille micrométrique qui nécessitent une dispersion à des niveaux élevés de turbulence. L'augmentation de la vitesse maximale de montée en pression est plus élevée pour des poudres avec un petit diamètre de particule, notamment en raison des phénomènes de fragmentation. En outre, un modèle numérique de propagation de front de flamme associé à un mélange gaz/noir de carbone a été développé pour examiner l'influence du noir de carbone sur la propagation de la flamme. Les résultats du modèle numérique suggèrent que la contribution de la chaleur radiative favorise l'accélération de la flamme. Ces résultats sont en accord avec les résultats expérimentaux de sévérité de l'explosion pour certains mélanges hybrides / Flammable gas/solid hybrid mixture explosions are not well understood because of the interaction of the thermal transfer process, the combustion kinetics mechanisms and the interactions between turbulence and combustion. The main objective on this work is to study the explosion severity and flame burning velocities of carbon black nanoparticles/methane to better understand the influence of added nanopowders in gas explosions. Tests have been performed in a flame propagation tube and in the standard 20 L explosion sphere. The influence of carbon black particles on the explosions severity and in the front flame propagation has been appreciated by comparing the results obtained for pure gas mixtures. It appeared that the carbon black nanoparticles insertion increases around 10% the explosion severity for lean methane mixtures. Therefore, it seems that nanoparticles has an impact on the severity of the explosion even for quiescent systems, contrary to systems involving micro-sized powders that requires a dispersion at high turbulence levels. The increment on the maximum rate of pressure rise is higher for powders with lower elementary particle diameter, which is notably due to the fragmentation phenomena. A flame propagation numerical model associated to a gas/carbon black mixture has been developed to examine the influence of carbon blacks on the flame propagation. The results of the numerical model suggest that the radiative heat contribution promotes the flame acceleration. This result is consistent with the experimental increase on the explosion severity for some hybrid mixtures

Examination of seismic records during the time interval of the Sago Mine disaster in 2006 revealed a small amplitude signal possibly associated with an event in the mine. Although the epicenter of the signature was located in the vicinity where the explosion occurred, it could not be unequivocally attributed to the explosion. More needs to be understood about the seismicity from mine explosions in order to properly interpret critical seismic information. A seismic monitoring system located at NIOSH's Lake Lynn Experimental Mine has monitored nineteen experimental methane and dust based explosions. The objective of the study was to analyze seismic signatures generated by the methane and dust explosions to begin understanding their characteristics at different distances away from the source. The seismic signatures from these different events were analyzed using standard waveform analysis procedures in order to estimate the moment magnitude and radiated seismic energy. The procedures used to analyze the data were conducted using self-produced programs not available with existing commercial software. The signatures of the explosions were found to be extremely complex due a combination of mine geometry and experimental design, both of which could not be controlled for the purposes of the study. Geophones located approximately 600 m (1970 ft) and over from the source collected limited data because of the attenuation of the seismic waves generated by the methane explosion. A combination of the methods used to characterize the seismic signatures allowed for differentiation between experimental designs and the size of the explosion. The factors having the largest impact on the signatures were the mine geometry, size of the methane explosion, construction of the mine seal and location of the mine seal. A relationship was derived to correlate the radiated seismic energy to the size of the explosion. Recommendations were made, based upon the limitations of this study, on methods for better collection of seismic data in the future. / Ph. D.

Šiame baigiamajame darbe apžvelgtos dulkių sprogimų atsiradimo priežastys bei sprogimų plitimų mechanizmas. Aprašyti sprogimų žemės ūkio įmonėse padariniai. Aptartos techninės priemonės, įgalinančias lokalizuoti pirminius silpnus dulkių sprogimus ir taip išvengiant stiprių, griaunamosios jėgos sprogimų. Išanalizuotos ugnį užtveriančių ir technologinių universaliųjų sklendžių tiesiaeiges elektros pavaros. Naudojant programinį modeliavimo paketą Matlab Simulink sudarytas universaliosios sklendės tiesiaeigės pavaros modelis ir gautos dinaminių charakteristikų imitacijos kreives. Naudojant programinį paketą SolidWorks sumodeliuota universalioji sklendė ir gauta smūginės bangos slėgio veikiamo sklendės judamojo elemento deformacija ir judamojo elemento deformacija, kai induktoriaus aktyviojoje zonoje įtaisyti papildomi atraminiai guoliai. Baigiamojo darbo pabaigoje pateiktos išvados ir pasiūlymai. / The final work of master analyses the causes of dust explosions and explosions spread mechanism. A short overview of the explosions effects in the agro - industry is presented. Technical devices enabling the localization of primary weak dust explosions and so avoiding the strong, destructive force explosions are discussed. Fire blocking and universal linear electric drives are analyzed. Using software package Matlab Simulink model of universal linear electric drive is created and dynamic characteristics are gained. Using software package SolidWorks model of universal linear electric drive is created and valves mobile element deformation and deformation of the mobile element, when there are installed additional supporting bearings in the inductor active zone are obtained when mobile element is affected by the pressure of the explosion wave. Concluding part presents inferences and suggestions.