This thesis describes the design of a magnetometer for recording geomagnetic micropulsations. The nuclear magnetic resonance phenomenon of hydrogen nuclei in water is utilized in the sensing unit of a feedback system, the feedback current being recorded as a measure of the geomagnetic variation. The thesis establishes the feasibility of a feedback system magnetometer. The system transfer function is derived and from it the sensitivity, stability, steady state error and dynamic range are determined. The dispersion mode signal of nuclear magnetic resonance obtained experimentally is shown and compared with that predicted theoretically. The advantages of a feedback system are indicated. The difficulty in closing the feedback loop is discussed and methods for overcoming this problem are suggested. / Science, Faculty of / Physics and Astronomy, Department of / Graduate

Title: Preparation and characterization of bi-phasic magnetic nanoparticles Author: Bc. Adam Alemayehu Department: Department of Innorganic Chemistry Supervisors: doc. RNDr. Daniel Nižňanský, Ph.D. RNDr. Václav Tyrpekl, Ph.D. Consultant: M.Sc. Dominika Zákutná Abstract The work is focusing on the magnetic properties of ferrimagnetic spinel ferrites before and after the introduction of a shell on a core particle with different magnetic properties. The core nanoparticles were prepared by hydrothermal decomposition of oleate precursors. The introduction of shell was carried out by hydrothermal treatment of the already prepared core particles. The phase composition, spinel structure and the sizes of the prepared samples were investigated by powder X-ray diffraction and by transmission electron microscopy. Formation of the shell on top of the core particle was determined indirectly, using Mössbauer spectroscopy at room temperature. The interparticle interactions and the particle shape was studied by small angle X-ray scattering. The magnetic properties of the prepared samples were measured on a SQUID magnetometer. Key words: magnetic nanoparticles, core, shell, spinel structure, powder X-ray diffraction, Mössbauer spectroscopy, magnetic measurements, TEM

The previous data acquisiton system developed for the electrical impedance imaging via contactless measurements is improved to obtain measurements with a faster scanning speed of 0.15 sec/mm2. This system uses magnetic excitation to induce currents inside the body and measures the magnetic fields of the induced currents with an axial gradiometer. Gradiometer consists of two differentially connected 10000-turn coils with diameter of 30 mm and a transmitter coil of 100-turn coil of diameter 30 mm placed and magnetically coupled between them. Transmitter coil is driven by a sinusoidal current of 200 mA (peak) whose frequency is 14.1 kHz. A Data Acquisition Card (DAcC) is designed and constructed on PCB, thus elliminates the use of the Lock-In Amplifier Instrument (LIAI) in the phase sensitive measurements. User interface programs to control the scanning experiments via PC (MATLAB Scanner 1.0, HP VEE Scanner 1.0) and to analyze the acquired data (Data Observer 1.0) are prepared. System performance tests for the DAcC are made. Error in the phase sensitive measurements is measured to be 0.6% of the test signals. Minimum magnetic field density that can be detected is found to be 7 DT. Output stage performance of the DAcC is improved by using an integrator instead of an amplifier in the output stage. In this manner, maximum linearity error is measured as 6.60*10-4 % of the full scale for the integrator circuit. Thermally generated voltage drift at the sensor output is measured to be 0.5 mV/minute in the ambient temperature. Overall normalized standard deviation at the output of the data acquisition system is observed as to be in the order of 10-4. Mathematical relation between the resistive rings and conductive phantoms is studied. It is derived that maximum resistor value that can be distinguished in the resistive ring experiment which is 461 F, corresponds to the phantom conductivity of 2.7 S/m. Field profiles (i.e., the voltage measurements) for the human left hand is obtained for the first time in literature, employing the LIAI. Agar objects with conductivity value of 1 S/m in a saline solution of 0.2 S/m are scanned and the field profiles are obtained using the DAcC. Image profiles of the scan fit well with the actual locations, geometries, and relative dimensions of the agar objects. A coil winding machine is prepared which enables the operator to design and wind up coils under self-controlled environment and conditions.

The work assesses progress in the design of measuring workplace for measuring low level magnetic fields of low frequencies. The thesis describes the basic method of spreading of electromagnetic waves in free losslees ambience. Further is described effect with low level of ultra-low-frequency magnetic fields in the frequency band from 0.01 to 30 Hz for an individual or group of people and also the draft measuring methods for indicating or measuring changes in magnetic fields. Thesis deals with individual blocks of measuring workstation.

Ce travail de thèse porte sur la recherche géophysique de la proche sub-surface appliquée aux objets et structures archéologiques. L'objectif est de définir une méthodologie d'étude géophysique de sites archéologiques dans un contexte Méditerranéen : en France et en Tunisie, ainsi que " l'empreinte géophysique " des principaux objets archéologiques. La méthode géophysique principale utilisée est la méthode magnétique. Les cartographies magnétiques obtenues sont couplées aux cartographies et mesures électromagnétiques et aux tomographies électriques (ERT) et sismiques. Ce volet de prospection sur le terrain est corrélé aux mesures magnétiques de laboratoire, permettant une meilleure contrainte des modélisations directes et synthétiques proposées pour les différents objets étudiés. Dans une première partie, la thèse se concentre sur les structures et objets archéologiques de combustion. Cette partie précise la signature magnétique de ces objets et souligne son rehaussement dû à l'effet du feu. Dans un second temps, la thèse fait porter l'analyse sur l'empreinte géophysiques des structures d'aménagement et sa variation reliée aux différents matériaux et techniques utilisés ainsi qu'aux propriétés du terrain encaissant. D'autres objets sont par la suite étudiés pour une meilleure compréhension des anomalies magnétiques potentiellement produites. La diminution de la qualité du signal magnétique et donc du rapport signal sur bruit est traité vers la fin. / This dissertation deals with the applied geophysics to archaeological objects and structures in the close subsurface. The aims are to define a geophysical methodology for the study of archeological sites in a Mediterranean context : in France and in Tunisia, and also the geophysical signature of the main archaeological features. The main geophysical method used is the magnetic method. The obtained magnetic mappings are coupled with the electromagnetic cartographies and measurements, and with the electrical tomographies (ERT) and the seismic surveys. This ground prospecting is correlated with the magnetic measurements of laboratory, allowing a better constraint of the forward and synthetic modelling, proposed for the various studied features. First, the thesis concentrates on the study of the archaeological structures of combustion. This part specifies the magnetic signature of these objects and underlines the raising owed to the effect of the fire. Secondly, this work analyzes the geophysical imprint of the building structures and its variation connected with the various materials and techniques used as well as the surrounding ground properties. Other objects are afterward studied for a better understanding of the potentially produced magnetic anomalies. Last but not least, the decrease of the quality of the magnetic signal and thus the signal-to-noise ratio, is handled.

This thesis deals with the analysis of magnetic losses in electrical machines and the possibilities of their measurement. Magnetically soft and hard materials are very prone to changing magnetic properties. They can be changed simply by changing the temperature of the material or different stresses induced in the material, resulting in different results. These changes are important to keep in mind when an electric machine is being designed. The original parameters of the affected materials can be restored by annealing or grinding. These methods release the induced stresses within the material. Due to these effects, it is also important to know how to measure magnetic parameters. Each way has its own specifics and has a certain error of the measurement. When the machines for higher efficiency, rpm or higher temperatures are designed, it is advisable to know how their magnetic properties changed. This thesis deals with the properties of different materials, their measurements and finally simulation of the chosen electric machine with the application of the measured results.

Presents results of research in the field of low-level electromagnetic fields interacting with the higher organisms, in the frequency band from 0,01 to 30 Hz effect on the individual or social group. Provides a description of the methodology of measuring and evaluating the impact of workplace assembled measuring low-level electromagnetic fields, extremely low frequency (ELF) on a sample of respondents. It was proposed measuring device for monitoring and evaluating how respondents' reactions to changes in the geomagnetic or external - external magnetic / electromagnetic field and to work for the measurement and evaluation of changes in external magnetic fields very low levels (ELF). This work is designed to process and evaluate implemented within experimental research into the influence of low-level magnetic fields in the Earth's resonator psychophysiological parameters of human organism and its behavior and decision-making. The work confirmed the influence of low-level magnetic fields on the psychophysiological parameters of the organism to be simultaneously confirmed the hypothesis established in accordance with the objectives of work.

Small satellites are gaining popularity in a wide range of applications where attitude systems require high precision performance. One of the main sources of errors, in case of magnetic attitude control systems, is the residual magnetic moment (RMM) of the spacecraft. To keep the RMM low and stable, mitigation methods shall be applied based on the satellite’s magnetic dipole moment (MDM) characterization, which shall be measured accurately. For small satellites, the most common technique involves the generation of a field-free region for the magnetic measurements using a test bed. The test bed measurement setup is normally mechanical, where measurements from the device under test (DUT) are very tedious. Optical magnetic test beds (OMTB) are being developed for MDM characterization providing simpler set ups and faster measurements than mechanical test beds. In this work, accuracy of OMTB of Aalto University has been evaluated by measuring three permanent magnets in two configurations. The measurements show a relationship between the estimation accuracy and the DUT’s marker area seen by the camera. Moreover, it was observed that the field-free region generated by Helmholtz coil cage can generate false data points. Based on these observations, the detection of the marker’s positions have been evaluated using the view area (VA) and the pointing angle (PA). The analysis shows that there is a consistent pattern depending on the combination of the VA and PA. Hence, the method of data acquisition was improved in order to prioritize the markers which position allow better accuracy. The achieved improvement of MDM estimation results is 2 %, and the test bed’s overall error evaluated is a 13 % in MDM position estimation and 23 % in MDM magnitude estimation. The improved OMTB was used to characterize the MDM of four magnetic attitude coils of Foresail-1 satellite. The measurements results are consistent with design parameters, showing three dipole configuration in all coils with a MDM magnitude order of 10−2 A·m2. / Foresail-1

電磁応用機器の特性向上に繋がる基礎的知見を得ることを目的とし，電磁鋼板および鉄心内部の局所的な磁気特性の分布に着目した研究を行った。方向性電磁鋼板については，鋼板内部の局所領域の磁気特性の測定手法を開発し，磁気特性の不均一分布の原因を解明した。無方向性電磁鋼板においては，打抜き，カシメ，応力といった鉄心製造に関わる因子の影響を評価し，鉄心での磁気特性劣化の機構を明らかにした。 / 博士(工学) / Doctor of Philosophy in Engineering / 同志社大学 / Doshisha University