Yes / Polypropylene is one type of plastic that is widely used in our everyday life. This study focuses on the identification and justification of the optimum process parameters for polypropylene production in a novel pilot plant based fluidized bed reactor. This first-of-its-kind statistical modeling with experimental validation for the process parameters of polypropylene production was conducted by applying ANNOVA (Analysis of variance) method to Response Surface Methodology (RSM). Three important process variables i.e., reaction temperature, system pressure and hydrogen percentage were considered as the important input factors for the polypropylene production in the analysis performed. In order to examine the effect of process parameters and their interactions, the ANOVA method was utilized among a range of other statistical diagnostic tools such as the correlation between actual and predicted values, the residuals and predicted response, outlier t plot, 3D response surface and contour analysis plots. The statistical analysis showed that the proposed quadratic model had a good fit with the experimental results. At optimum conditions with temperature of 75 °C, system pressure of 25 bar and hydrogen percentage of 2%, the highest polypropylene production obtained is 5.82% per pass. Hence it is concluded that the developed experimental design and proposed model can be successfully employed with over a 95% confidence level for optimum polypropylene production in a fluidized bed catalytic reactor (FBCR).

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In this thesis a number of improvements have been established for specific methods which utilize sequential Monte Carlo (SMC), aka. Particle filtering (PF) techniques. The first problem is the Bayesian multi-target tracking (MTT) problem for which we propose the use of non-parametric Bayesian models that are based on time varying extension of Dirichlet process (DP) models. The second problem studied in this thesis is an important application area for the proposed DP based MTT method / the tracking of vocal tract resonance frequencies of the speech signals. Lastly, we investigate SMC based parameter estimation problem of nonlinear non-Gaussian state space models in which we provide a performance improvement for the path density based methods by utilizing regularization techniques.

Aus der Einleitung: "Verschiedene Zielkonflikte zwischen den Anforderungen bzgl. Sicherheit, Wirtschaftlichkeit und Umweltverträglichkeit resultieren aus den Spannungsfeldern Umwelt, Wirtschaft und Technik (Busche 2014, Braess & Seiffert 2013). Richtungsentscheidungen bei der Festlegung der Anforderungen im Entwicklungsprozess auf Grundlage weniger Informationen bergen die Gefahr fehlerhafter Entscheidungen (Feldhusen & Grote 2013). Wird dies im weiteren Verlauf der Entwicklungsprozesse bemerkt sind Iterationsschleifen verbunden mit hohen Kosten notwendig, um dort nachzubessern (Ehrlenspiel et al. 2007). Der Grund für das große Informationsdefizit am Anfang des Entwicklungsprozesses sind die unbekannten Auswirkungen der Parametervariationen auf die Eigenschaften (Ehrlenspiel 2009). Diese resultieren u.a. aus den restriktiven Anforderungen, neuen Technologien oder alternativen Werkstoffen (Braess & Seiffert 2013). Muss das Nachfolgefahrzeug bspw. länger und flacher, bei gleicher Fahrdynamik werden oder leichter bei schärferen NVH- und Crash-Eigenschaften sein, müssen neue Strukturen, Materialien und Verfahren eingesetzt werden (Prinz 2011, Busche 2014). Bei Neukonstruktionen ist der Anteil unbekannter Auswirkungen noch höher (Ehrlenspiel 2009). ..."

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Binomial AR(1) process is a model for integer-valued time series with a fi- nite range and discrete time. It has the binomial marginal distribution and the AR(1)-like autocorrelation structure. This thesis deals with deriving some ba- sic properties of this process, methods of parameter estimation and goodness of fit testing. Three methods of parameter estimation are presented: Yule-Walker, the conditional least squares and the maximum likelihood method together with proofs of their asymptotical properties. Next, the goodness of fit testing is pre- sented. At first, two known methods based on the marginal distribution and the autocorrelation function are summarized. Then our own method is added, based on the probability generating function. Several simulations are provided to show the properties of all tests. The application of this model is illustrated on a real dataset. 1

Material utilisation is of importance in the manufacturing industry formaking the most of each material, minimising waste and increasing cost-effectiveness. In this thesis, samples of Waspaloy built with the method of L-DED-P has been analysed in order to investigate how process pa-rameters influence the build quality and geometrical accuracy in as-builtobjects. The samples analysed was built in single rows of one, three,five and fifteen layers. A build process was used in which the sampleswere built with individual combinations of the process parameters laserpower, scanning speed, and powder flow. Each combination of processparameters was used to build one track for each layer height.Analysis included defect analysis with light optical microscopy, andpost-processing with ImageJ for automatic identification, quantification,and collection of measurements. A qualitative analysis was performed andthe sample properties and characteristics was described in terms of theamount of defects, including a descriptive assessment of defect severity.Etched samples revealed a columnar grain structure in samples, which was apparent in builds with at least three layers.The results presented show a difference in build height, quantity andsize of pores, and the presence or absence of other defects such as lack of fusion. Sample 3 which was built with high laser power, slow scan-ning speed, and high powder feed show promising results with one ofthe highest build rates of all samples, combined with a low normalisedpore distribution. The sample experiences partial hardening, with hard-ness values reaching 320 HV, but still promisingly show no sign of crackformation.It is concluded that powder feed relates primarily to the build rateof the samples, and the scanning speed together with the laser power influence the quality of the build, where high laser power and low scanningspeed tends to form well behaving samples with few defects, whilst other combinations increase the risk of defects.

Grâce à l'utilisation d'un porteur liquide, la projection plasma de suspension (SPS) permet la fabrication de revêtements finement structurés. Comme pour la projection plasma conventionnelle (APS), les microstructures des revêtements SPS peuvent être adaptées en contrôlant les conditions de projection. Cependant, le procédé SPS est plus compliqué que le procédé APS par son nombre de paramètres modifiables.Cette thèse vise à apporter une compréhension plus fondamentale de la relation entre les paramètres du procédé SPS et les propriétés des revêtements YSZ en identifiant des modèles génériques basés sur l’utilisation de méthodes statistiques mathématiques pour l'étude de l'influence et de la sensibilité de paramètres individuels.Des expériences systématiques ont été menées pour étudier l'influence de six paramètres (puissance du plasma, charge massique de suspension, taille de la poudre, distance de projection, pas de projection et rugosité du substrat) sur la microstructure des revêtements qui ont aussi été analysés en terme de propriétés d’usage (mécanique, thermique, tribologique, etc.). La porosité des revêtements a fait l’objet d’une étude approfondie et les mesures ont été réalisées par trois techniques différentes : la méthode par analyse d’images, la transmission RX et la méthode USAXS (Ultra-Small Angle X-ray Scattering). Des analyses multivariées sur les données expérimentales recueillies ont été effectuées et plusieurs modèles mathématiques ont été proposés afin de prédire les propriétés des revêtements et guider ensuite vers une optimisation de la microstructure du revêtement en vu d'applications spécifiques.Dans ce contexte d'optimisation des performances mécaniques et tribologiques de ces revêtements céramiques, différentes quantités et tailles de poudre h-BN ont été ajoutées dans la suspension YSZ. Les revêtements composites YSZ / h-BN ont été fabriqués et leur analyse a montré une nette réduction du coefficient de frottement et du taux d'usure lorsque la taille et la quantité de poudre d’ajout sont optimisées l'une avec l'autre. Trois mécanismes d’usure ont finalement été identifiés et seront discutés. / Thanks to the using of liquid carrier, suspension plasma spray (SPS) enables the manufacture of finely structured coatings. As for conventional plasma spraying (APS), the microstructures of SPS coatings can be tailored by controlling the spray conditions. However, SPS is more complicated than APS due to its number of modifiable parameters.This thesis aims to provide a more fundamental understanding of the relationship between SPS process parameters and the properties of YSZ coatings by identifying generic models based on the use of mathematical statistical methods for the study of influence and sensitivity of the individual parameters.Systematic experiments were carried out to study the influence of six parameters (plasma power, suspension mass load, powder size, projection distance, projection step and substrate roughness) on the microstructure of coatings which were also analyzed in terms of the properties (mechanical, thermal, tribological, etc.). The porosity of the coatings was studied in detail and the measurements were carried out using three different techniques: the image analysis method, the X-ray transmission and the USAXS (Ultra-Small Angle X-ray Scattering) method. Multivariate analyzes of the collected experimental data were performed and several mathematical models were proposed to predict the properties of the coatings and then guide towards an optimization of the microstructure of the coating for specific applications.In this context of optimizing the mechanical and tribological performance of ceramic coatings, different amounts and sizes of h-BN powder have been added in the YSZ suspension. The YSZ/h-BN composite coatings were manufactured by SPS process and their analysis showed a clear reduction in the coefficient of friction and the wear rate when the size and the amount of addition powder are optimized together. Three wear mechanisms have finally been identified and been discussed.

This thesis illustrates analysis of the influence of the non-machining processes on product quality by experimental design and statistical analysis. For the analysis objective / dishwasher production in Arcelik Dishwasher plant is examined. Sheet metal forming processes of dishwasher production constitutes the greatest portion of production cost and using the Pareto analysis technique / four pieces among twenty six pieces are determined to be investigated. These four pieces are the U Sheet, L Sheet, Inner Door and Side Panel of the dishwasher. By the help of the flow diagrams production process of the determined pieces are defined. Brainstorming technique and cause&amp / effect diagrams are used to determine which non-machining process parameters can cause pieces to be scrapped. These parameters are used as control factors in experimental design. Taguchi&amp / #8217 / s L16(215) orthogonal array, Taguchi&amp / #8217 / s L16(215) orthogonal array using S/N transformation and 28-4 fractional factorial design are used on purpose. With repetitions and confirmation experiments the effective parameters are determined and optimum level of these parameters are defined for the improvements on scrap quantity and quality of production.

This thesis illustrates parameter optimization of compressive strength, flexural strength and impact resistance of steel fiber reinforced high strength concrete (SFRHSC) by statistical design and analysis of experiments. Among several factors affecting the compressive strength, flexural strength and impact resistance of SFRHSC, five parameters that maximize all of the responses have been chosen as the most important ones as age of testing, binder type, binder amount, curing type and steel fiber volume fraction. Taguchi and regression analysis techniques have been used to evaluate L27(313) Taguchi&amp / #65533 / s orthogonal array and 3421 full factorial experimental design results. Signal to noise ratio transformation and ANOVA have been applied to the results of experiments in Taguchi analysis. Response surface methodology has been employed to optimize the best regression model selected for all the three responses. In this study Charpy Impact Test, which is a different kind of impact test, have been applied to SFRHSC for the first time. The mean of compressive strength, flexural strength and impact resistance have been observed as around 125 MPa, 14.5 MPa and 9.5 kgf.m respectively which are very close to the desired values. Moreover, this study is unique in the sense that the derived models enable the identification of underlying primary factors and their interactions that influence the modeled responses of steel fiber reinforced high strength concrete.