The detection and active monitoring of hydrogen gas levels is essential in many areas of industry including manufacturing, storage, and transport of this gas. Previously, methods used to detect hydrogen gas have relied upon monolithic technologies to create resistive-based sensors which are impractical for many applications requiring electrical isolation or operation in the presence of strong electromagnetic fields. Materials can be sputter deposited along cylindrical optical fiber-based sensors to create novel fiber-optic chemical sensors. Herein, the mechanisms allowing the detection of hydrogen gas using a modified Extrinsic Fabry-Perot Interferometric (EFPI) sensor are presented in this work. A new custom-designed, custom-built radio frequency (RF) magnetron sputtering system has been used to deposit thin films of palladium metal along with cylindrical substrates. The surface morphology of the deposited films are investigated using a variety of analytical tools, including Scanning Electron Microscopy (SEM), Energy Dispersive X-ray Spectroscopy (AES), and Auger Electron Spectroscopy (AES). The system is used to deposit thin films of palladium along a cylindrical EFPI fiber-optic sensor to produce a new fiber-optic hydrogen gas sensor. Experimental results obtained in a controlled hydrogen atmosphere are used to demonstrate the high resolution and fast response time associated with these new hybrid sensors. / Master of Science

Conventional fiber optic interferometric sensors employing a monochromatic source prove to be inadequate for applications requiring absolute, real-time value of magnitude and direction of the applied perturbation. This limitation can be overcome by using a broadband light source to extract unambiguous information from the sensor in the wavelength domain. Several variations in the signal processing techniques for white light interferometry are discussed and compared in terms of resolution, bandwidth and cost. A detailed analysis is made of the principle of operation and basic features of the commercially available absolute sensing system. This compact system is self calibrating, has a 100 micro-strain Ole) strain and 2°C temperature resolution and is ideal for applications in environments where the parameter to be measured is static or quasi-static. High finesse Fabry-Perot cavities are employed to obtain almost an order of magnitude sensitivity improvement over conventional low finesse cavities. The principle of white light interferometry is extended to absolute axial stain and temperature sensing in two-mode, elliptical-core fibers. Other novel applications, such as to operation of photo induced refractive index gratings and fiber characterization are proposed. / Master of Science

The use of optical sensors to perform health monitoring in fault-tolerant multicomputers can allow the multicomputer to detect imminent failure in a particular section of the interconnection network due to damaging strain. This detection method allows the rerouting of critical data before data link failure occurs. This thesis investigates the implementation of the extrinsic Fabry-Perot interferometer into an optical hybrid communications/sensing network. A testbed of personal computers, acting as nodes of a multicomputer, are used to monitor the integrity of the network to a high degree of accuracy. When a node determines that an adjacent data link is no longer reliable due to physical damage, communications are rerouted and the node is shut down. Results of experiments with the testbed have shown that redundant nodes can be used to share computational loads, increasing the performance of the multicomputer, until network failure forces redundant nodes to assume full responsibility for computational tasks. Multicomputer performance suffers as a result of network damage, but full functionality is retained with no occurrence of errors or unknown conditions due to data link failure. / Master of Science

Since the invention of Laser (in 1960) and low loss optical fiber (in 1966) [1], extensive research in fiber-optic sensing technology has made it a well-defined and matured field [1]. The measurement of physical parameters (such as temperature and pressure) in extremely harsh environment is one of the most intriguing challenges of this field, and is highly valued in the automobile industry, aerospace research, industrial process monitoring, etc. [2]. Although the semiconductor based sensors can operate at around 500oC, sapphire fiber sensors were demonstrated at even higher temperatures [3]. In this research, a novel sensor structure is proposed that can measure both pressure and temperature simultaneously. This work effort consists of design, fabrication, calibration, and laboratory testing of a novel structured temperature compensated pressure sensor. The aim of this research is to demonstrate an accurate temperature measurement, and pressure measurement using a composite Fabry-Perot interferometer. One interferometer measures the temperature and the other accurately measures pressure after temperature compensation using the temperature data from the first sensor. / Master of Science

Several techniques for measuring humidity are presented. The goal of the study is to use the electrostatic self-assembled monolayer synthesis process to fabricate a Fabry-Parot Cavity based optical fiber humidity sensor. The sensing scheme bases on the refractive index change with relative humidity of the film applied to the end of optical fiber. That is, the change in reflected optical power indicates certain humidity. To achieve this, some chemicals induce on specific coating materials were applied at the end of optical fiber. In this thesis, experimental results are given to prove that the humidity sensor has high sensitive and fast response time. Furthermore, we investigate the potential for the use of human breathing monitoring and air flow rate detection. Results from preliminary tests of each are given. / Master of Science

Due to their compact size, sensitivity, and ability to be multiplexed, intrinsic Fabry-Perot interferometers (IFPIs) are excellent candidates for almost any multi-point temperature or strain application, and it is well-known that using a single-mode lead-in fiber, a multi-mode fiber section as the Fabry-Perot cavity, and an additional single-mode fiber as the tail results in a structure that generates strong interference fringes while remaining robust. Though the basic principles behind these sensors are understood, to the best of the author's knowledge there hasn't been a thorough investigation into the design and fabrication of a chain of multiplexed IFPI sensors for industrial use in an environment where serious issues associated with the size of the test coupon, sensor placement, and mechanical reinforcement of the fiber could arise. This thesis details the preparation and results of this investigation. It turns out that fabricating a sensor chain with appropriate sensor spacing and excellent temperature response characteristics proved a significant challenge, and issues addressed include inter-sensor interference, high-temperature mechanical reinforcement for bare fiber sections, and high bending losses. After overcoming these problems, a final sensor chain was fabricated and characterized. This chain was then subjected to a battery of tests at the National Energy Technology Laboratory (NETL), where four multiplexed sensors were installed on a 2â x2â coupon in a simulated gas turbine environment. Final results are presented and analyzed. The work that went into developing this chain lays the foundation for future efforts in developing quasi-distributed temperature sensors by identifying potential obstacles and fundamental limitations for certain approaches. / Master of Science

A technology for fabricating fiber optic pressure sensors is described. This technology is based on intermediate-layer bonding of a fused silica ferrule to a patterned, micro-machined fused silica diaphragm, providing low temperature fabrication of optical pressure sensor heads that can operate at high temperature. Fused silica ferrules and fused silica diaphragms are chosen to reduce the temperature dependence. The fused silica diaphragms have been micro-machined using wet chemical etching in order to form extrinsic Fabry-Perot (FP) interferometric cavities. Sol-gel is used as an intermediate-layer for both fiber-ferrule bonding and ferrule-diaphragm bonding at relatively low temperature (250 °C). The pressure sensors fabricated in the manner can operate at temperatures as high as 600 °C. The self-calibrated interferometric-intensity-based (SCIIB) technology, which combines fiber interferometry and intensity-based sensing method into a single sensor system, is used to test and monitor the pressure sensor signal. The light returned from the FP cavity is split into two channels. One channel with longer coherence length can test the effective interference generated by the FP cavity, while the other channel with shorter coherence length can get signal proportional only to the source power, fiber attenuation, and other optical losses. The ratio of the signals from the two channels can compensate for all unwanted factors, including source power variations and fiber bending losses. [11] / Master of Science

The FP interferometer was found to be feasible for detecting changes in machining forces. The fiber optic sensor was able to detect increases in strain corresponding to force increases detected by a dynamometer. The FP interferometer system must progress in several ways. A better data acquisition and data analysis system must be developed. A robust sensor must be made to withstand the harsh environment of machining. Also a method for eliminating the affects of thermal strain must be created. Finally, the placement of the FP sensor must also be determined. The FP has the potential to effectively monitor machining forces without affecting the rigidity of a turning operation setup. / Master of Science

Interferometric optical fiber sensors have proved many orders of magnitude more sensitive than their electrical counterparts, but they suffer from limitations in signal demodulation caused by phase ambiguity and complex fringe counting when the output phase difference exceeds one fringe period. Various signal demodulation methods have been developed to overcome some of the these drawbacks with limited success. This thesis proposes a new measurement system for the extrinsic Fabry-Perot interferometer (EFPI) sensor. Using a wavelength modulated source and a novel extended-gap EFPI, some of the limitations of interferometric signal demodulation are overcome. By scanning the output wavelength of a multilongitudinal mode laser diode through current modulation, the EFPI sensor signal is scanned through multiple fringes. Gap movement is then unambiguously determined by monitoring the phase of the multiple fringe pattern. / Master of Science

An adaptation of an extrinsic Fabry-Perot interferometer (EFPI) strain sensor is described, which permits the state of cure of an epoxy matrix to be monitored, when the sensor is embedded in a polymeric matrix composite. By using a glass rod with a retroreflecting end for the target fiber in the EFPI sensor, the intensity of the light reflected depends on the refractive index of the host matrix, if a low coherence source is used. As the epoxy cross-links during cure, the refractive index of the epoxy will increase to a value exceeding that of the target fiber. The resulting increased loss in the fiber can be detected at the sensor output and correlated to the state of cure of the epoxy. After cure, the sensor may be operated as a conventional extrinsic Fabry-Perot interferometric strain sensor if a coherent source is used. Using the modified extrinsic Fabry-Perot sensor, we monitor the cure of Devcon® 5-Minute® Epoxy, and show that it cures in approximately 60 minutes. / Master of Science