Since the invention of Laser (in 1960) and low loss optical fiber (in 1966) [1], extensive research in fiber-optic sensing technology has made it a well-defined and matured field [1]. The measurement of physical parameters (such as temperature and pressure) in extremely harsh environment is one of the most intriguing challenges of this field, and is highly valued in the automobile industry, aerospace research, industrial process monitoring, etc. [2]. Although the semiconductor based sensors can operate at around 500oC, sapphire fiber sensors were demonstrated at even higher temperatures [3]. In this research, a novel sensor structure is proposed that can measure both pressure and temperature simultaneously. This work effort consists of design, fabrication, calibration, and laboratory testing of a novel structured temperature compensated pressure sensor. The aim of this research is to demonstrate an accurate temperature measurement, and pressure measurement using a composite Fabry-Perot interferometer. One interferometer measures the temperature and the other accurately measures pressure after temperature compensation using the temperature data from the first sensor. / Master of Science

This dissertation presents the structure, operational principle and mathematical model of a novel high speed fiber optic spectrometer (HSFOS). In addition, the performance analysis is conducted and preliminary experimental results are listed and discussed. Such a spectrometer is highly desired by the ever-increasing applications of fiber optic sensors. In the recent decades, a variety of fiber optic sensors have been proposed, built and tested. Compared to their electronic counterparts, fiber optic sensors although still under development, are preferred more by certain industrial and medical applications which benefit from their unique properties such as immunity to electromagnetic interference, ability to withstand harsh environments and composition of purely dielectric materials. In recent years, new fiber optic sensors have been designed for applications where high response frequency up to a few hundred KHz is required while advantages of high accuracy and large dynamic range must be maintained. The bottle neck then emerged in the signal demodulation part of the sensor system. The quadrature phase detection could achieve high demodulation speed but with small dynamic range, medium accuracy and measurement ambiguity. The white light interferometry could provide a solution for high accuracy and large dynamic range measurement without ambiguity because of its absolute measurement nature. However the signal demodulation speed is limited due to the low spectrum acquisition rate of the existing spectrometers. The new HSFOS utilizes time domain dispersion of the sampled incoming light by dispersive fiber rather than the spatial dispersion employed by traditional spectrometers. In addition the signal that represents the spectrum of the light is naturally a serial signal which can be detected by a single detector and recorded by a high speed data acquisition device. Theoretical study of the operation principle is made and a mathematical model for the spectrometer is developed based on Marcuse's previous work. One major difference of the new derivation is that the propagation constant is expanded about the center circular frequency of each monochromatic light pulse instead of the center frequency of the chromatic light pulse which makes the physical picture of the chromatic light pulse evolution in a dispersive fiber clearer and facilitates both the analytical and numerical analysis. The profile of the dispersed chromatic light pulse could be treated as the superposition of all the dispersed monochromatic light pulses. Another major difference is the Taylor's series of the propagation constant is not truncated as it is in those previous work, which improves the accuracy of the model. Moreover, an approximate model is made which could further reduce the computation tasks in numerical simulations. Performance analysis for accuracy, resolution, speed and noise are conducted through numerical simulations based on the model and the experimental results. The sources of two different errors and their effects on accuracy are discussed respectively. The effects on spectral resolution by the properties of the modulation pulse and the fiber dispersion are studied. The results indicate that by using a rectangle modulation pulse under certain conditions, the resolution can be improved. The speed analysis gives that the spectrum acquisition rate can reach 1 million frames per second when the spectral width is less than 100 nm. In the noise analysis, the erbium-doped fiber amplifier (EDFA) is determined to be the dominant noise source. But by using two EDFAs, the overall signal to noise ratio is improved by 9.2 dB. The preliminary experimental results for FP sensor and FBG sensor signal demodulation are presented. The HSFOS for FP sensor signal demodulation achieves 15 nm resolution. By using the oversampling method, the HSFOS for FBG sensor signal demodulation achieves 0.05 nm spectral positioning resolution. / Ph. D.

The health monitoring of smart structures in civil engineering is becoming more and more important as in-situ structural monitoring would greatly reduce structure life-cycle costs and improve reliability. The distributed strain and temperature sensing is highly desired in large structures where strain and temperature at over thousand points need to be measured simultaneously. It is difficult to carry out this task using conventional electrical strain sensors. Fiber optic sensors provide an excellent opportunity to fulfill this need due to their capability to multiplex many sensors along a single fiber cable. Numerous research studies have been conducted in past decades to increase the number of sensors to be multiplexed in a distributed sensor network. This dissertation presents detailed research work on the analysis, design, fabrication, testing, and evaluation of an intrinsic Fabry-Perot fiber optic sensor for quasi-distributed strain and temperature measurements. The sensor is based on two ultra-short and broadband reflection fiber Bragg gratings. One distinct feature of this sensor is its ultra low optical insertion loss, which allows a significant increase in the sensor multiplexing capability. Using a simple integrated sensor interrogation unit and an optical spectrum based signal processing algorithm, many sensors can be interrogated along a single optical fiber with high accuracy, high resolution and large dynamic range. Based on the experimental results and theoretical analysis, it is expected that more than 500 sensors can be multiplexed with little crosstalk using a frequency-division multiplexing technology. With this research, it is possible to build an easy fabrication, robust, high sensitivity and quasi-distributed fiber optic sensor network that can be operated reliably even in harsh environments or extended structures. This research was supported in part by U.S. National Science Foundation under grant CMS-0427951. / Ph. D.

Measurement of physical parameters in harsh environments (high pressure, high temperature, highly corrosive, high electromagnetic interference) is often desired in a variety of areas, such as aerospace, automobile, energy, military systems, and industrial processes. Pressure and temperature are among the most important of these parameters. A typical example is pressure monitoring in jet engine compressors to help detect and control undesirable air flow instabilities, namely rotating stall and surge. However, the temperatures inside a compressor could reach beyond 600°C for today's large engines. Current fiber-optic sensor can operate up to about 300°C and even the most widely employed semiconductor sensors are limited below 500°C. The objective of this research is to push the limit of fiber-optic sensing technology in harsh environment applications for both pressure and temperature measurements by developing novel sensing structures, fabrication techniques, and signal processing algorithms. An all-fused-silica pressure sensor has been demonstrated which is fabricated on the tip of a fiber with a diameter no larger than 125μm. The sensor was able to function beyond the current limit and operate into the 600~700°C range. Also a temperature sensor has been developed using sapphire fibers and wafers for ultra-high temperature measurement as high as 1600°C. This effort will generate more understanding regarding sapphire fiber's high temperature properties and could possibly lead to novel designs of pressure sensor for beyond 1000°C. Both sensors have been field tested in real-world harsh environments and demonstrated to be reliably and robust. In this dissertation, the design, fabrication, and testing of the sensors are discussed in detail. The system and signal processing techniques are presented. The plan and direction for future work are also suggested with an aim of further pushing the operating limit of fiber-optic sensors. / Ph. D.

In this work, we first analyze the behavior of the acoustic wave from the theoretical point of view using a simplified 1-dimensional model. The model was developed based on the conservation of mass, the conservation of momentum, and the state equation; in addition, the fluid medium obeys Stokes assumption and it is homogeneous, adiabatic and isentropic. Experiment and simulation results show consistency to theoretical calculation. The second part of this thesis focuses on the PD signal analysis from an on-site PD measurement of the in-house design fiber optic sensors (by Virginia Tech, Center for Photonics Technology). Several commercial piezoelectric transducers (PZTs) were also used to compare the measurement results. The signal analysis employs the application of wavelet-based denoising technique to remove the noises, which mainly came from vibration, EMI, and light sources, embedded in the PD signal. The denoising technique includes the discrete wavelet transform (DWT) decomposition, thresh-holding of wavelet coefficients, and signal recovery by inverse discrete wavelet transform. Several approaches were compared to determine the optimal mother wavelet. The threshold limits are selected to remove the maximum Gaussian noises for each level of wavelet coefficients. The results indicate that this method could extract the PD spike from the noisy measurement effectively. The frequency of the PD pulse is also analyzed; it is shown that the frequencies lie in the range of 70 kHz to 250 kHz. In addition, with the assumed acoustic wave propagation delay between PD source and sensors, it was found that all PD activities occur in the first and third quadrant in reference to the applied sinusoidal transformer voltage. / Master of Science

High voltage power transformer is one of the most important and expensive components in today's power transmission and distribution systems. Any overlooked critical fault generated inside a power transformer may lead to a transformer catastrophic failure which could not only cause a disruption to the power system but also significant equipment damage. Accurate and prompt information on the health state of a transformer is thus the critical prerequisite for an asset manager to make a vital decision on a transformer with suspicious conditions. Partial discharge (PD) is not only a precursor of insulation degradation, but also a primary factor to accelerate the deterioration of the insulation system in a transformer. Monitoring of PD activities and the concentration of PD generated combustible gases dissolved in the transformer oil has been proven to be an effective procedure for transformer health state estimation. However current commercially available sensors can only be installed outside of transformers and offer indirect or delayed information. This research is aimed to investigate and develop several sensor techniques for transformer health monitoring. The first work is an optical fiber extrinsic Fabry-Perot interferometric sensor for PD detection. By filling SF6 into the sensor air cavity of the extrinsic Fabry-Perot interferometer sensor, the last potential obstacle that prevents this kind of sensors from being installed inside transformers has been removed. The proposed acoustic sensor multiplexing system is stable and more economical than the other sensor multiplexing methods that usually require the use of a tunable laser or filters. Two dissolved gas analysis (DGA) methods for dissolved hydrogen or acetylene measurement are also proposed and demonstrated. The dissolved hydrogen detection is based on hydrogen induced fiber loss and the dissolved acetylene detection is by direct oil transmission measurement. / Ph. D.

From the monitoring of deep ocean conditions to the imaging and exploration of the vast universe, optical sensors are playing a unique, critical role in all areas of scientific research. Optical fiber sensors, in particular, are not only widely used in daily life such as for medical inspection, structural health monitoring, and environmental surveillance, but also in high-tech, high-security applications such as missile guidance or monitoring of aircraft engines and structures. Measurements of physical parameters are required in harsh environments including high pressure, high temperature, highly electromagnetically-active and corrosive conditions. A typical example is fossil fuel-based power plants. Unfortunately, current optical fiber sensors for high-temperature monitoring can work only for single point measurement, as traditional fully-distributed temperature sensing techniques are restricted for temperatures below 800°C due to the limitation of the fragile character of silica fiber under high temperature. In this research, a first-of-its-kind technology was developed which pushed the limits of fully distributed temperature sensing (DTS) in harsh environments by exploring the feasibility of DTS in optical sapphire waveguides. An all sapphire fiber-based Raman DTS system was demonstrated in a 3-meters long sapphire fiber up to a temperature of 1400°C with a spatial resolution of 16.4cm and a standard deviation of a few degrees Celsius. In this dissertation, the design, fabrication, and testing of the sapphire fiber-based Raman DTS system are discussed in detail. The plan and direction for future work are also suggested with an aim for commercialization. / Ph. D.

Made available in DSpace on 2014-06-11T19:22:35Z (GMT). No. of bitstreams: 0 Previous issue date: 2006-04-28Bitstream added on 2014-06-13T18:06:43Z : No. of bitstreams: 1 sakamoto_jms_me_ilha.pdf: 6608858 bytes, checksum: 00cb410d8ba756148ea0f5626f2c8f3b (MD5) / Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES) / A interferometria a laser é uma técnica consolidada para a caracterização de atuadores piezoelétricos. No entanto, este método requer um alinhamento óptico preciso e uma operação meticulosa. Há um grande interesse no desenvolvimento de sistemas de medição de deslocamento e vibração usando sensores reflexivos em fibra óptica devido a sua inerente simplicidade, tamanho reduzido, largura de banda ampla, limite de detecção extremamente baixo e capacidade de realizar medições sem contato ou afetar o sistema a ser ensaiado. Neste trabalho apresenta-se um arranjo simples do sensor reflexivo para se atingir resolução sub-micrométrica, utilizando-se fibras e componentes ópticos de baixo custo e circuitos eletrônicos simples. O sistema é constituído por duas fibras ópticas adjacentes (uma transmissora e outra receptora) e com extremidades emparelhadas, posicionadas na frente de uma superfície reflexiva vibratória. A luz proveniente de uma fonte óptica (no caso um laser) é acoplada à fibra transmissora e parte dos raios refletidos pela superfície móvel é capturada pela fibra receptora, que conduz a luz para um fotodetector. A tensão de saída do fotodetector é função da distância entre as extremidades das fibras e a superfície reflexiva. Apresenta-se uma formulação teórica da função de intensidade óptica refletida no plano a uma distância qualquer, juntamente com comparações entre características experimentais e teóricas do sensor reflexivo. Finalmente, atuadores piezoelétricos flextensionais, projetados com o método de otimização topológica, são caracterizados experimentalmente através da medição de seus deslocamentos sub-micrométricos, utilizando o sensor reflexivo. As respostas em freqüência dos piezoatuadores flextensionais são levantadas e o fenômeno de erro de trajetória e linearidade são discutidos. / The laser interferometer method is a well-established technique for the characterization of piezoelectric actuators. However, this method requires precise optical alignment and meticulous operation. There is great interest in developing displacement and vibration measurement systems using reflective fiber optic displacement sensors (RFODS) because of their inherent simplicity, small size, wide frequency range, extremely low displacement detection limit, and ability to perform measurements without contact or affecting the vibrating system. This work presents a simple arrangement of RFODS to achieve sub-micrometer resolution, using low-cost fibers and optical components, and simple electronic circuits. The system is composed of two adjacent transmitting and receiving fibers at one end, located in front of a reflecting vibrating surface. The transmitting fiber is connected to a laser source, and part of the reflected rays by the moving surface is captured by the receiving fiber, which is connected to a light detector. The output voltage is a function of the distance between probe and vibrating surface. A theoretical formulation of the reflected light intensity function at distal end plane is presented, together with comparisons of experimental and ideal RFODS characteristics. Finally, piezoelectric flextensional actuators (PFAs), designed with the topology optimization method, are experimentally characterized by the measurement of their sub micrometric displacements using a RFODS. The frequency responses of the PFAs are evaluated, and the tracking error phenomenon and linearity are discussed.

This master's thesis deals with the measurement of soil temperature. In the theoretical part, optical fiber systems were explained, with a focus on DSTS systems and their use. In the practical part, a functional system was created to measure the soil temperature at depths of 0.1-1~m using the Arduino platform. Furthermore, the temperature measurement was demonstrated on the test polygon using the optical fiber of the FTB 2505 instrument in laboratories.

La présence croissante de diverses substances dans notre environnement, conséquencedes activités anthropiques de ces dernières décennies, a entraîné un besoingrandissant et urgent de nouveaux matériaux et dispositifs dans la quête de senseurschimiques efficaces et fiables. D'énormes progrès technologiques ont permis de mettreà disposition toute une gamme d'outils techniques pour leur développement, enprenant en compte les exigences à respecter en terme de sélectivité ou de rapidité deréponse, entre autres. Dans ce contexte, les méthodes de chimie quantique permettentune compréhension fondamentale des processus en jeu dans la détection des espèceschimiques, et par extension, l'élaboration de manière rationnelle de nouveauxmatériaux sensibles. Certaines molécules organiques pouvant être largementfonctionnalisées, elles constituent un point de départ idéal en raison des importantesmodulations possibles de leurs propriétés par des modifications structuralesappropriées.Cette étude vise à développer de manière rationnelle des chromoionophores pour lacomplexation de cations par une approche combinant méthodes de chimiecomputationnelles et caractérisation par spectroscopie optique. Deux pointsprincipaux ont été traités à l'aide de la Théorie de la Fonctionnelle de la Densité(DFT) et son extension dépendante du temps (TD-DFT): d'une part les relationsstructure moléculaire-propriétés optiques de chromophores, d'autre part le phénomènede complexation. En particulier, la détection de l'ion Zn2+, démontrée de manièrethéorique et expérimentale, est finalement réalisée après intégration du senseurmoléculaire dans un dispositif à fibre optique. / The increasing presence of various substances in our environment has brought abouta growing need for rapid emergence of new materials and devices in the quest forefficient and reliable chemical sensors. Massive technological progress have madeavailable an extensive range of technical tools to serve their development, accountingfor the requirements to be fulfilled (selectivity, quick response..). In this context,quantum chemistry methods provide a fundamental understanding of the processes atstake in the detection of chemical species and allow for rational design of sensingmaterials. Certain organic molecules can be extensively functionalised and thusconstitute an evident starting point owing to the tunability of their propertiesprovided by appropriate choice of structural modifications. The versatility of somechromophores associated to the selectivity offered by receptor units constitute theresearch playground for the development of ever better chemosensors.The present research aims at the rational development of chromoionophores for thecomplexation of cations, combining computational chemistry methods with basicspectroscopic characterisation. Using Density Functional Theory (DFT) and its timedependentextension (TD-DFT), two main aspects were treated, namely therelationship between molecular structure and optical properties of organicchromophores featuring valuable characteristics, and the complexation phenomenon.Photophysics of Zn2+ ion detection were more specifically studied, and recognitionwas demonstrated with both quantum-chemical calculations and experiments,accounting for the future integration of the chemical sensor in an optical fibre device.