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In power generation from solid fuel such as coal-fired power plants, combustion efficiency can be monitored by the loss on ignition (LOI) of the pulverised fuel. It is the role of the pulveriser-classifier combination to ensure pulverised fuel delivered to the burners is within the specified limits of fineness and mass flow deviation required to keep the LOI at an acceptable level. However, government imposed limits on emissions have spurred the conversion of many coal fired power plants to convert to the use of Low NOx Burners. To maintain good LOI or combustion efficiency, the limits of fineness and mass flow deviation or inter-outlet fuel distribution have become narrower. A lot of existing pulveriser units cannot operate efficiently within these limits hence retrofits of short term solutions such as orifice balancing and classifier maintenance has been applied. The work performed in this thesis relates to an investigation into coal classifier devices that function to control fineness and inter pipe balancing upstream of the burner and downstream of the pulverisers. A cold flow model of a static classifier was developed to investigate the flow characteristics so that design optimisations can be made. Dynamic similarity was achieved by designing a 1/3 scale model with air as the continuous phase and glass cenospheres of a similar size distribution as pulverised fuel, to simulate the coal dust. The rig was operated in positive pressure with air at room temperature and discharge to atmosphere. The Stokes number similarity (0.11-prototype vs. 0.08-model) was the most important dimensionless parameter to conserve as Reynolds number becomes independent of separation efficiency and pressure drop at high industrial values such as 2 x 10 4 Hoffman, 2008). Air-fuel ratio was also compromised and an assumption of dilute flow was made to qualify this. However, the effect of air fuel ratio was ascertained by its inclusion as an experimental variable. Experiments were conducted at air flow rates of 1.41-1.71kg/s and air fuel ratios of 4.8-10 with classifier vane angle adjustment (30°- 60°) and inlet swirl umbers (S) of 0.49 – 1. Radial profiles of tangential, axial and radial velocity were obtained at several cross sections to determine the airflow pattern and establish links with the separation performance and outlet flow balance. Results show a proportional relationship between cone vane angle and cut size or particle fineness. Models can be derived from the data so that reliable predictions of fineness and outlet fuel balance can be used in power stations and replace simplistic and process simulator models that fail to correctly predict performance. It was found that swirl intensity is more significant a parameter in obtaining balanced flow at the classifier outlets than uniform air flow distribution in the mill. However the latter is important in obtaining high grade efficiencies and cut size. The study concludes that the static classifier can be further improved and retrofit-able solutions can be applied to problems of outlet flow imbalance and poor fineness at the mill outlets.

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Multiphase flow is the simultaneous flow of two or several phases through a system such as a pipe. This common phenomenon can be found in the petroleum and chemical engineering industrial fields. Transport of sand particles in multiphase production has attracted considerable attention given sand production is a common problem especially to the oil and gas industry. The sand production causes loss of pipe wall thickness which can lead to expensive failures and loss of production time. Build-up of sand in the system can result in blockage and further hamper production. Monitoring of multiphase flow is a process that has been established over several decades. This thesis reports an assessment of the application of Acoustic Emission (AE) technology as an alternative online technique to monitoring of sand particles under multiphase flow conditions in a horizontal pipe. The research was conducted on a purpose built test rig with the purpose of establishing a relation between AE activity and sand concentration under different multiphase flow conditions. The investigation consisted of five experimental tests. The initial experiment was performed to provide a basis for the application of AE technology to detect sand particle impact prior to performing tests in multiphase flow conditions. Further investigations are reported on two phase air-sand, water-sand and air- water-sand three-phase flows in a horizontal pipe for different superficial gas velocities (VSG), superficial liquid velocities (VSL) and sand concentrations (SC). The experimental findings clearly showed a correlation exists between AE energy levels and multiphase flow parameters, such as superficial liquid velocity (VSL), superficial gas velocity (VSG), sand concentration and sand minimum transport condition (MTC).

Gas lift is a means of enhancing oil recovery from hydrocarbon reservoirs. Gas injected at the production riser base reduces the gravity component of the pressure drop and thereby, increases the supply of oil from the reservoir. Also, gas injection at the base of a riser helps to mitigate slugging and thus, improving the performance of the topside facility. In order to improve the efficiency of the gas lifting technique, a good understanding of the characteristics of gas-liquid multiphase flow in vertical pipes is very important. In this study, experiments of gas/liquid (air/water) two-phase flows, liquid/liquid of oil/water two-phase flows and gas/liquid/liquid (air/oil/water) three-phase flows were conducted in a 10.5 m high 52 mm ID vertical riser. These experiments were performed at liquid and gas superficial velocities ranging from 0.25 to 2 m/s and ~0.1 to ~6.30 m/s, respectively. Dielectric oil and tap water were used as test fluids. Instruments such as Coriolis mass flow meter, single beam gamma densitometer and wire-mesh sensor (WMS) were employed for investigating the flow characteristics. For the experiments of gas/liquid (air/water) two-phase flow, flow patterns of Bubbly, slug, churn flow regimes and transition regions were identified under the experimental conditions. Also, for flow pattern identification and void fraction measurements, the capacitance WMS results are consistent with those obtained simultaneously by the gamma densitometer. Generally, the total pressure gradient along the vertical riser has shown a significant decrease as the injected gas superficial velocity increased. In addition, the rate of decrease in total pressure gradient at the lower injected gas superficial velocities was found to be higher than that for higher gas superficial velocities. The frictional pressure gradient was also found to increase as the injected gas superficial velocity increased. For oil-water experiments, mixture density and total pressure gradient across the riser were found to increase with increasing water cut (ranging between 0 - 100%) and/or mixture superficial velocity. Phase slip between the oil and water was calculated and found to be significant at lower throughputs of 0.25 and 0.5 m/s. The phase inversion point always takes place at a point of input water cut of 42% when the experiments started from pure oil to water, and at an input water cut of 45% when the experiment’s route started from water to pure oil. The phase inversion point was accompanied by a peak increase of pressure gradient, particularly at higher oil-water mixture superficial velocities of 1, 1.5 and 2 m/s. The effects of air injection rates on the fluid flow characteristics were studied by emphasizing the total pressure gradient behaviour and identifying the flow pattern by analysing the output signals from gamma and WMS in air/oil/water experiments. Generally, riser base gas injection does not affect the water cut at the phase inversion point. However, a slight shift forward for the identified phase inversion point was found at highest flow rates of injected gas where the flow patterns were indicated as churn to annular flow. In terms of pressure gradient, the gas lifting efficiency (lowering pressure gradient) shows greater improvement after the phase inversion point (higher water cuts) than before and also at the inversion point. Also, it was found that the measured mean void fraction reaches its lowest value at the phase inversion point. These void fraction results were found to be consistent with previously published results.

Current oil production technologies recover only about one‐third to one‐half of the oil originally present in an oil reservoir. Given current oil prices, even a modest increase in oil recovery efficiency is fiscally attractive. One novel approach to increase oil recovery efficiency is a process called microbial enhanced oil recovery (MEOR), where microorganisms are either used as a clogging agent to redirect flow or to produce biosurfactant that reduces interfacial tension. This dissertation aims to understand the MEOR pore‐scale mechanisms relevant to oil recovery by taking a two‐fold approach where transparent 2‐dimensional micromodel experiments imaged with stereo microscopy and 3‐dimensional column experiments imaged with x‐ray computed microtomography (CMT) are utilized. Micromodel experiments allow for direct visualization of the biological phase (i.e. biofilm), however, only 2‐dimensional information is provided. Conversely, CMT experiments provide 3‐dimensional pore‐scale information, but lack the ability to image the biological phase. With this two‐fold approach, it is possible to distinguish multiple fluid interfaces, quantify fluid phase saturations, measure oil blob size distributions, and visualize the biological phase. Furthermore, a method to measure interfacial curvature from 3‐dimensional images is developed, providing researchers a new perspective from which to study multiphase flow experiments. Overall, the presented research utilizes pore‐scale imaging techniques to study the interfacial interactions occurring during MEOR in an effort to better explain the physics, and thus, increase the efficacy of MEOR. / Graduation date: 2012

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