Grain shape is a key factor affecting the mechanical properties of granular materials. However, grain shape quantification techniques to distinguish one granular material from another have not reached a stage of development for inclusion in modeling the behavior of granular materials. Part of the problem is the equipment of choice for grain shape measurement is the scanning electron microscope. This is a relatively expensive and complex device. In this research, a practical approach using light microscopy to quantify grain shape and to identify the key shape parameters that can distinguish grains was investigated. A light microscope was found to produce grain images with sufficient quality for the purpose of observing the grain shape profile. Several grain shape parameters were determined for eight different sands - four sands chosen for this study and four sands from an outside source. Six of these - Circularity, Roundness, Sphericity, Aspect Ratio, Compactness and ModRatio - are shown to be the key shape parameters that differentiate these sand grains.Relationships between the six key grain shape parameters and dilatancy were developed to enable a better understanding of the mechanics of granular materials and for potential use in practice. Data to build the relationships were obtained using a light microscope, digital image processing software (ImageJ), and direct shear tests on four uniform sands composed of grains with varying, somewhat-homogeneous, shape profiles - ranging from very rounded grains in one granular conglomerate to very angular shaped grains in another.A Weighted Single Sand Shape Factor (WSSSF) was derived from all of the six key shape parameters was developed using Weighted Factor Analysis. A good correlation was found to exist between dilatancy and WSSSF. The correlation also incorporates normal effective stress, relative density and the critical state friction angle. Verification was conducted through the introduction of a subangular to subrounded sand that was not used in building the correlation. The correlation proved to provide a good estimate of the dilatancy of sands based on the physical properties of grains and the applied loading.

The stability of rock masses is influenced by the occurrence of rock joints. Therefore, the shear strength of rock joints must be considered in dimensioning of underground constructions. One way to predict the shear strength is through usage of failure criteria, which are validated from results of direct shear tests under controlled laboratory conditions. Consequently, the quality of the results from the tests are crucial to the accuracy with which the criteria will be able to predict the shear strength. Since rock joints are unique by nature usage of replicas (man-made copies of rock joints) is of importance in parameter studies. The overall objective of this work is to facilitate the development of improved criteria for predictions of the shear strength of rock joints. To support this objective, two sources of uncertainty have been investigated, namely the geometry of replicas and the influence of the normal stiffness of test systems. Two quality assurance parameters for evaluation of geometrical differences between replicas and rock joints based on scanning data have been derived. The first parameter describes the morphological deviations. The second parameter describes the deviations in orientation with respect to the shear plane. The effective normal stiffness approach, which compensates for the influence of the normal stiffness of the test system in direct shear testing, has been developed, validated, and applied. With help of the quality assurance parameters it is demonstrated that it is possible to reproduce replicas within narrow tolerances. Application of the effective normal stiffness approach basically eliminates the normal load error. In all, the results support generation of improved quality of test data and consequently, the development of shear strength criteria with improved accuracy will also be facilitated. / <p>Academic Dissertation which, with due permission of the KTH Royal Institute of  Technology, is submitted for public defence for the Degree of Licentiate of Engineering on Wednesday the 9th June 2021, at 9:00 a.m. in M108, Brinellvägen 23, Stockholm.</p><p><strong>Paper A</strong>: Larsson J, Flansbjer M, Portal N W, Johnson E, Johansson F, and Mas Ivars D. (2020) Geometrical Quality Assurance of Rock Joint Replicas in Shear Tests – Introductory Analysis. Paper presented at the ISRM International Symposium - EUROCK 2020, physical event not held. https://onepetro.org/ISRMEUROCK/proceedings-abstract/EUROCK20/All-EUROCK20/ISRM-EUROCK-2020-101/451187  In Diva: http://urn.kb.se/resolve?urn=urn:nbn:se:ri:diva-51987 </p><p><strong>Paper B:</strong> Larsson J, Johansson F, Mas Ivars D, Johnson E, Flansbjer M and Portal N W. (2021) Rock joint replicas in direct shear testing – Part 1: Extraction of geometrical quality assurance parameters. To be submitted to Rock Mechanics and Rock Engineering  In DiVA: http://urn.kb.se/resolve?urn=urn:nbn:se:ri:diva-53111 </p><p><strong>Paper C:</strong> Larsson J and Flansbjer M. (2020) An Approach to Compensate for the Influence of the System Normal Stiffness in CNS Direct Shear Tests. Rock Mechancis and Rock Engineering 53, 2185–2199 https://doi.org/10.1007/s00603-020-02051-0  In DiVA: http://urn.kb.se/resolve?urn=urn:nbn:se:ri:diva-44085  </p><p><strong>Paper D:</strong> Larsson J. (2021) Experimental investigation of the system normal stiffness of a 5 MN direct shear test setup and the compensation of it in CNS direct shear tests. Submitted to ISRM International Symposium - EUROCK 2021  In DiVA: http://urn.kb.se/resolve?urn=urn:nbn:se:ri:diva-53112 </p>

No description available.

No description available.

The use of composites materials in aerospace applications can provide significant weight reduction. However, in airframe designs composites are frequently required to be joined to metal components, which is a challenging issue owing to the very different thermo-physical properties of the two classes of materials. In many cases adhesive bonding has insufficient durability and the requirement for large lapped areas and mechanical fasteners adds considerable weight, reducing the mass savings associated with the introduction of composite structures. A promising approach for improving joint performance is to surface engineer locking features on to the metal part which then integrate with the composite laminate to increase shear load transfer, both via better adhesion and also by mechanical "fit" throughout the thickness of the composite. Such hybrid joints are known as "hyper-joints". For this work, three main techniques are currently being investigated for generating the required surface features. These are; (i) sculpting surfaces using power beam local surface melting techniques (Surfi-Sculpt), (ii) building surface protrusions by additive layer manufacturing (AM) and (iii) arc percussive welding process. The present work aims to provide understanding of the critical metallurgical interactions during the growth/production of the surface engineered features and how some build parameters might affect the eventual joint integrity, durability and performance. To enable the use of the arc-percussive welding process as a viable manufacturing route for these hyper-joints, optimisation of its process parameters were studied in the course of this work. Further work on the effect of process parameters such as voltage, travel velocity, gap setting and time delay on the quality of the weld were also investigated in this study. Of the above mentioned process parameters, the voltage across the capacitor and travel velocity of the actuator have been found to have far greater effect on the weld quality. More importantly, the travel velocity of the actuator was also found to help determine the shape, size and distribution of the melt pool. Based on the systematic study and analysis of all of the process parameters involved, an optimised process window has now been proposed. Microstructural characterisations of hyper-joint samples made via the three manufacturing routes were performed in the course of the work. The observed microstructures were related to the process history and the process parameters. Most importantly it was for found that in common with most welding and AM processes, columnar prior β grains developed in all the samples studied by epitaxial-regrowth either along the build or weld directions. It was also found that the fusion zone of the similar titanium alloy (Ti-6Al-4V to Ti-6Al-4V) arc-percussive welded samples were characterised by extremely fine acicular alpha' martensitic platelets formed as a result of the high cooling rate associated with the process. On the other hand, the fusion zone of the dissimilar titanium alloy (Ti-6Al-4V to β21S) arc-percussive welded samples was characterised by an extremely fine cellular structure prompted by constitutional supercooling. Finally the microstructures observed in the Surfi-Sculpt samples were found to be dependant on the swipe pattern and duration. In order to assess the performance of hyper-joints made via two of the candidate manufacturing routes, tensile testing of standard and modified tensile samples was performed. The result indicated that on average the strength of these hyper-joint pins were within nominal values expected of the Ti-6Al-4V and β21S alloys. It was also found that with optimum weld conditions, failure occurred only along the gauge length for the arc-percussive welded samples whilst the strength of the AM samples degrade as the gauge diameter decreases as the effect of surface defects became prominent. Results are also reported on a novel method for testing the shear strength and properties of individual hyper-pins manufactured via this process. Interpretation of the shear test was assisted by finite element modelling. The shear test results indicated that the arc-percussive welded samples outperformed the SLM-AM samples thereby giving credence to the process as a viable means for making the pins.

The stability of rock masses is influenced by the occurrence of rock joints. Therefore, the shear strength of rock joints must be considered in dimensioning of underground constructions. One way to predict the shear strength is through usage of failure criteria, which are validated from results of direct shear tests under controlled laboratory conditions. Consequently, the quality of the results from the tests are crucial to the accuracy with which the criteria will be able to predict the shear strength. Since rock joints are unique by nature usage of replicas (man-made copies of rock joints) is of importance in parameter studies. The overall objective of this work is to facilitate the development of improved criteria for predictions of the shear strength of rock joints. To support this objective, two sources of uncertainty have been investigated, namely the geometry of replicas and the influence of the normal stiffness of test systems. Two quality assurance parameters for evaluation of geometrical differences between replicas and rock joints based on scanning data have been derived. The first parameter describes the morphological deviations. The second parameter describes the deviations in orientation with respect to the shear plane. The effective normal stiffness approach, which compensates for the influence of the normal stiffness of the test system indirect shear testing, has been developed, validated, and applied. With help of the quality assurance parameters it is demonstrated that it is possible to reproduce replicas within narrow tolerances. Application of the effective normal stiffness approach basically eliminates the normal load error. In all, the results support generation of improved quality of test data and consequently, the development of shear strength criteria with improved accuracy will also be facilitated. / Bergmassors stabilitet påverkas av bergssprickor. Bergssprickors skjuvhållfasthet behöver därför beaktas vid fastställandet av vilka laster berganläggningar skall dimensioneras mot. Skjuvhållfastheten predikteras bland annat med hjälp av brottkriterier, vilka valideras med hjälp av resultaten från skjuvtester i kontrollerad laboratoriemiljö. Kvaliteten på resultaten från testerna är därför av avgörande betydelse för med vilken noggrannhet kriterierna kommer att kunna prediktera skjuvhållfastheten. Det övergripande målet med detta arbete är att underlätta utvecklingen av förbättrade kriterier för prediktioner av bergssprickors skjuvhållfasthet. Som ett bidrag till att uppnå detta mål har två osäkerhetsfaktorer undersökts, nämligen geometrin av replikor (kopior) av bergssprickor och inverkan av testsystems normalstyvhet. Två kvalitetssäkringsparametrar för utvärdering av de geometriska skillnaderna mellan replikor och bergprov baserade på skanningdata har tagits fram. Den första parametern beskriver de morfologiska avvikelserna. Den andra parametern beskriver avvikelserna i orientering med avseende på skjuvplanet. Ett tillvägagångssätt med en effektiv systemnormalstyvhet, vilken kompenserar för inverkan av testsystemets normalstyvhet, har utvecklats, validerats och tillämpats. Med hjälp av kvalitetssäkringsparametrarna påvisas att det ar möjligt att reproducera replikor inom snäva toleranser. Genom tillämpning av tillvägagångssättet med en effektiv normalstyvhet kan felet i normallast i princip elimineras. Sammantaget stödjer resultaten framtagning av testdata med förbättrad kvalitet och därigenom underlättas även utvecklingen av skjuvhållfasthetskriterier med förbättrad noggrannhet. / <p>QC 210518</p>

Este trabalho apresenta a caracterização in situ de propriedades de interesse geotécnico de maciços de resíduos sólidos urbanos (RSU) e o estudo das propriedades de resistência ao cisalhamento de RSU com diferentes idades. Foram realizadas investigações por sondagens e com métodos geofísicos sísmicos no Aterro Sanitário de São Carlos (ASSC) e ensaios de cisalhamento direto de grandes dimensões (50x50 cm2) com amostras de diferentes idades de aterramento coletadas no ASSC, no Lixão Desativado de São Carlos e em Aterro Experimental construído nas proximidades do Lixão. As investigações realizadas no ASSC revelaram que as diferentes fases de operação do maciço (aterro controlado e aterro sanitário) produziram dois estratos com diferentes propriedades geotécnicas. A umidade, as velocidades de propagação de ondas sísmicas e o peso específico in situ dos dois estratos são distintos, sendo sempre menores e menos dispersos no estrato mais raso (operado como aterro sanitário) e maiores e mais dispersos no estrato mais profundo (operado como aterro controlado). Realizaram-se tentativas de determinação do peso específico in situ dos RSU com medição dos volumes escavados por substituição de volume. Notou-se que os furos tendiam a diminuir de diâmetro assim que a composição de sondagem era retirada e que o método adotado para avanço dos furos, com trado helicoidal de haste oca, promovia segregação dos componentes atravessados, realizando uma amostragem parcial dos mesmos. Foram calculados valores médios de peso específico in situ para o maciço investigado (9 a 15 kN/m3) e identificadas as principais limitações da aplicação deste método a aterros sanitários. A aplicação de métodos geofísicos sísmicos foi fundamental para a diferenciação dos dois estratos e permitiu que se calculasse o módulo de cisalhamento máximo (Go) dos resíduos, que variou significativamente de um estrato para outro. Foi possível comparar os resultados obtidos com a aplicação do método crosshole e do método multichannel analysis of surface waves (MASW) no mesmo aterro sanitário. A caracterização das seis amostras utilizadas nos ensaios de cisalhamento direto revelou que, apesar de elas representarem idades distintas de disposição dos resíduos (2 a 25 anos) e condições de aterramento variadas (formas de operação dos depósitos, ambientes de decomposição e condições de confinamento), a maioria delas se encontrava em estágio avançado de degradação (fase metanogênica) e apenas a mais recente (2 anos de aterramento) encontrava-se em estágio um pouco menos avançado de degradação (início da fase metanogênica). Todas elas exibiram curvas tensão-deslocamento semelhantes, sem pico ou valor de máxima resistência bem caracterizados. Os parâmetros de resistência ao cisalhamento foram obtidos a partir de níveis específicos de deslocamento. Avaliou-se a influência da amostragem, dos procedimentos de preparação das amostras e da composição gravimétrica de cada uma delas sobre os valores calculados para coesão e ângulo de atrito. Para deslocamentos de 100 mm o resíduo aterrado há dois anos apresentou coesão de 13,7 kPa e ângulo de atrito de 22º. Os resíduos mais degradados, com idades de disposição entre 5 e 25 anos, apresentaram coesão de 4,4 kPa e ângulo de atrito de 30º. Utilizaram-se tensões normais de 50, 150 e 250 kPa. Realizaram-se ainda ensaios de cisalhamento direto de grandes dimensões em uma das amostras com corpos de prova em duas posições: paralela e perpendicular à direção de compactação. Os resultados confirmaram que os RSU têm comportamento anisotrópico, sendo que os corpos de prova ensaiados com os componentes alinhados preferencialmente na posição vertical (rotacionados) têm comportamento de endurecimento ainda mais pronunciado que aqueles ensaiados com os componentes orientados preferencialmente no plano horizontal. / Field and laboratory tests were combined to characterize some in-place geotechnical properties of the waste body in the São Carlos Sanitary Landfill (SCSL). The investigation was carried out using hollow stem auger soundings and seismic geophysical methods in the field, and large-scale direct shear testing in the laboratory. The field investigation revealed two strata with different geotechnical properties and they could be related to the different operational phases of the landfill (controlled landfill and sanitary landfill). Moisture content, seismic wave velocities and in-place unit weight were systematically lower and less scattered in the upper stratum than in the lower stratum. The upper stratum was operated as a sanitary landfill and the lower stratum was operated as a controlled landfill. The investigations with geophysical seismic methods were essential for identifying the two strata and allowed for the calculation of the Poisson ratio and the small strain shear modulus (Go) of the waste body. The Poisson ratio showed no sensibility to the waste stratigraphy, but Go values were significantly higher in the lower stratum. Moreover, the results of two different geophysical methods, namely crosshole and multichannel analysis of surface waves (MASW), could be compared. An attempt was made to estimate overboring using a volume substitution method by filling the boreholes with gravel. This aimed at incorporating this aspect in the calculations of the MSW in-place unit weight. Nevertheless, the borings tended to cave in as soon as the augers were removed and this prevented the evaluation of the overboring. Moreover, the hollow stem auger tended to segregate the larger components of the waste and to bring only the smaller ones to the surface. Despite all these difficulties, average values for the MSW inplace unit weight were be calculated (9 to 15 kN/m3). In the laboratory, large-scale direct shear tests (500 x 500 mm2) were performed to provide an insight on the shear strength response of municipal solid waste (MSW) of different landfilling ages. The test samples were collected from the SCSL, a dumpsite and an experimental landfill. Their landfilling ages ranged from 2 to 25 years. Physico-chemical characterization of the samples revealed that most of them were subjected to the metanogenesis degradation phase, in spite of their different landfilling ages and burial conditions (operational characteristics of the deposits, decomposition environment and confining pressures). Only the newest one (2 years old sample) was subjected to an earlier stage of degradation. In the direct shear tests, all samples showed similar stress-strain curves, with continuous strain hardening and no identifiable maximum stress, despite the large displacements. The influence of sampling method, sample preparation and sample gravimetric composition on the calculated shear resistance parameters is discussed. For a 100-mm displacement the shear resistance of the less degraded waste (2 years of landfilling) is best characterized by cohesion = 13.7 kPa and friction angle = 22º. The more degraded wastes (5 to 25 years old samples) are best characterized by cohesion = 4.4 kPa and friction angle = 30º. The tests were performed with initial normal stresses of 50, 150 and 250 kPa. Specific large direct shear tests were performed to evaluate anisotropy in the MSW shear response. The test samples had the fibrous materials oriented perpendicular or parallel to the horizontal shear surface. Results confirmed the expected anisotropy by showing a hardening behaviour that was more pronounced when the fibrous materials were oriented perpendicular to the shear plan.

Este trabalho apresenta a caracterização in situ de propriedades de interesse geotécnico de maciços de resíduos sólidos urbanos (RSU) e o estudo das propriedades de resistência ao cisalhamento de RSU com diferentes idades. Foram realizadas investigações por sondagens e com métodos geofísicos sísmicos no Aterro Sanitário de São Carlos (ASSC) e ensaios de cisalhamento direto de grandes dimensões (50x50 cm2) com amostras de diferentes idades de aterramento coletadas no ASSC, no Lixão Desativado de São Carlos e em Aterro Experimental construído nas proximidades do Lixão. As investigações realizadas no ASSC revelaram que as diferentes fases de operação do maciço (aterro controlado e aterro sanitário) produziram dois estratos com diferentes propriedades geotécnicas. A umidade, as velocidades de propagação de ondas sísmicas e o peso específico in situ dos dois estratos são distintos, sendo sempre menores e menos dispersos no estrato mais raso (operado como aterro sanitário) e maiores e mais dispersos no estrato mais profundo (operado como aterro controlado). Realizaram-se tentativas de determinação do peso específico in situ dos RSU com medição dos volumes escavados por substituição de volume. Notou-se que os furos tendiam a diminuir de diâmetro assim que a composição de sondagem era retirada e que o método adotado para avanço dos furos, com trado helicoidal de haste oca, promovia segregação dos componentes atravessados, realizando uma amostragem parcial dos mesmos. Foram calculados valores médios de peso específico in situ para o maciço investigado (9 a 15 kN/m3) e identificadas as principais limitações da aplicação deste método a aterros sanitários. A aplicação de métodos geofísicos sísmicos foi fundamental para a diferenciação dos dois estratos e permitiu que se calculasse o módulo de cisalhamento máximo (Go) dos resíduos, que variou significativamente de um estrato para outro. Foi possível comparar os resultados obtidos com a aplicação do método crosshole e do método multichannel analysis of surface waves (MASW) no mesmo aterro sanitário. A caracterização das seis amostras utilizadas nos ensaios de cisalhamento direto revelou que, apesar de elas representarem idades distintas de disposição dos resíduos (2 a 25 anos) e condições de aterramento variadas (formas de operação dos depósitos, ambientes de decomposição e condições de confinamento), a maioria delas se encontrava em estágio avançado de degradação (fase metanogênica) e apenas a mais recente (2 anos de aterramento) encontrava-se em estágio um pouco menos avançado de degradação (início da fase metanogênica). Todas elas exibiram curvas tensão-deslocamento semelhantes, sem pico ou valor de máxima resistência bem caracterizados. Os parâmetros de resistência ao cisalhamento foram obtidos a partir de níveis específicos de deslocamento. Avaliou-se a influência da amostragem, dos procedimentos de preparação das amostras e da composição gravimétrica de cada uma delas sobre os valores calculados para coesão e ângulo de atrito. Para deslocamentos de 100 mm o resíduo aterrado há dois anos apresentou coesão de 13,7 kPa e ângulo de atrito de 22º. Os resíduos mais degradados, com idades de disposição entre 5 e 25 anos, apresentaram coesão de 4,4 kPa e ângulo de atrito de 30º. Utilizaram-se tensões normais de 50, 150 e 250 kPa. Realizaram-se ainda ensaios de cisalhamento direto de grandes dimensões em uma das amostras com corpos de prova em duas posições: paralela e perpendicular à direção de compactação. Os resultados confirmaram que os RSU têm comportamento anisotrópico, sendo que os corpos de prova ensaiados com os componentes alinhados preferencialmente na posição vertical (rotacionados) têm comportamento de endurecimento ainda mais pronunciado que aqueles ensaiados com os componentes orientados preferencialmente no plano horizontal. / Field and laboratory tests were combined to characterize some in-place geotechnical properties of the waste body in the São Carlos Sanitary Landfill (SCSL). The investigation was carried out using hollow stem auger soundings and seismic geophysical methods in the field, and large-scale direct shear testing in the laboratory. The field investigation revealed two strata with different geotechnical properties and they could be related to the different operational phases of the landfill (controlled landfill and sanitary landfill). Moisture content, seismic wave velocities and in-place unit weight were systematically lower and less scattered in the upper stratum than in the lower stratum. The upper stratum was operated as a sanitary landfill and the lower stratum was operated as a controlled landfill. The investigations with geophysical seismic methods were essential for identifying the two strata and allowed for the calculation of the Poisson ratio and the small strain shear modulus (Go) of the waste body. The Poisson ratio showed no sensibility to the waste stratigraphy, but Go values were significantly higher in the lower stratum. Moreover, the results of two different geophysical methods, namely crosshole and multichannel analysis of surface waves (MASW), could be compared. An attempt was made to estimate overboring using a volume substitution method by filling the boreholes with gravel. This aimed at incorporating this aspect in the calculations of the MSW in-place unit weight. Nevertheless, the borings tended to cave in as soon as the augers were removed and this prevented the evaluation of the overboring. Moreover, the hollow stem auger tended to segregate the larger components of the waste and to bring only the smaller ones to the surface. Despite all these difficulties, average values for the MSW inplace unit weight were be calculated (9 to 15 kN/m3). In the laboratory, large-scale direct shear tests (500 x 500 mm2) were performed to provide an insight on the shear strength response of municipal solid waste (MSW) of different landfilling ages. The test samples were collected from the SCSL, a dumpsite and an experimental landfill. Their landfilling ages ranged from 2 to 25 years. Physico-chemical characterization of the samples revealed that most of them were subjected to the metanogenesis degradation phase, in spite of their different landfilling ages and burial conditions (operational characteristics of the deposits, decomposition environment and confining pressures). Only the newest one (2 years old sample) was subjected to an earlier stage of degradation. In the direct shear tests, all samples showed similar stress-strain curves, with continuous strain hardening and no identifiable maximum stress, despite the large displacements. The influence of sampling method, sample preparation and sample gravimetric composition on the calculated shear resistance parameters is discussed. For a 100-mm displacement the shear resistance of the less degraded waste (2 years of landfilling) is best characterized by cohesion = 13.7 kPa and friction angle = 22º. The more degraded wastes (5 to 25 years old samples) are best characterized by cohesion = 4.4 kPa and friction angle = 30º. The tests were performed with initial normal stresses of 50, 150 and 250 kPa. Specific large direct shear tests were performed to evaluate anisotropy in the MSW shear response. The test samples had the fibrous materials oriented perpendicular or parallel to the horizontal shear surface. Results confirmed the expected anisotropy by showing a hardening behaviour that was more pronounced when the fibrous materials were oriented perpendicular to the shear plan.

Une technologie prometteuse pour répondre à la demande croissante en énergie renouvelable est la gazéification de biomasse lignocellulosique pour la production de biocarburants de deuxième génération. Ce procédé nécessite une alimentation en biomasse sous forme de poudre. Les problèmes de convoyage et de manipulation liés à la faible coulabilité de la biomasse broyée sont un verrou pour l’industrialisation des procédés BtL. La torréfaction comme procédé de prétraitement, en plus d'augmenter densité énergétique de la biomasse, peut influencer également les propriétés des particules obtenues après broyage, et en conséquence, l’écoulement des poudres. L'évaluation de l'écoulement des poudres de biomasse sous différentes conditions de consolidation est essentielle pour concevoir des technologies de manipulation et de convoyage efficaces.L'objectif de ce travail est d'évaluer l'effet des conditions de torréfaction et de broyage sur l’écoulement de poudres de biomasse. Une première partie consiste en une étude expérimentale dans laquelle la coulabilité d'échantillons torréfiés sous différentes intensités a été évaluée à l'aide d'un appareil de cisaillement annulaire. La coulabilité est corrélée à l'intensité de la torréfaction (mesurée par la perte de masse globale) pour deux essences différentes. La forme des particules semble être le paramètre qui influence de manière prédominante la coulabilité des poudres à l'état consolidé. La caractérisation de la coulabilité à l’état non consolidée a été effectuée à l'aide d'un tambour rotatif par l’analyse des avalanches des poudres. Des corrélations entre les caractéristiques des particules et la coulabilité sont ainsi établies. La modélisation de l'écoulement de la biomasse à l'aide de la Méthode des Éléments Discrets (DEM) constitue une deuxième partie de cette recherche. La taille submillimétrique des particules de biomasse, ainsi que leur faible densité, leur forme allongée et leur comportement cohésif sont des défis pour l’implémentation d’un modèle de réaliste d’écoulement particulaire en DEM. Un modèle DEM des particules de biomasse est mis en œuvre à l'aide d'une représentation simplifiée (assemblement de sphères) à gros grains de la forme des particules, ainsi que d'un modèle de force cohésif. Une procédure systématique de calibration des paramètres DEM permet d'obtenir un ensemble de paramètres ajustés. L'évolution expérimentale des contraintes de cisaillement d’une poudre dans un état consolidé peut alors être reproduite de façon réaliste. De même, le comportement d’avalanche des poudres dans un tambour tournant est également bien reproduit par les simulations, de façon qualitative et quantitative. Ces résultats mettent en évidence le potentiel des simulations DEM pour étudier l'effet des caractéristiques des particules, qui sont influencées par la torréfaction et les conditions de broyage, sur le comportement d'écoulement de la biomasse en poudre. / Gasification of lignocellulosic biomass for production of second-generation biofuels is a promising technology to meet renewable energy needs. However, feeding and handling problems related to the poor flowability of milled biomass considerably hinder the industrial implementation of Biomass-to-Liquid processes. Torrefaction as pretreatment step, in addition to improving energy density of biomass, also affects the properties of the milled particles (namely size and shape) that significantly influence flow behavior. The evaluation of biomass flow characteristics under different flow conditions is essential to design efficient and trouble-free handling solutions.The aim of this work is to assess the effect of the torrefaction and grinding conditions on the biomass flow behavior. A first part consists of an experimental study in which the flow properties of samples torrefied under different intensities were obtained using a ring shear tester. Flowability is correlated to the intensity of torrefaction, as measured by the global mass loss, for two different wood species. Particle shape seems to be the predominant parameter influencing flowability of powders in a consolidated state. Characterization of non-consolidated flowability through avalanching analysis using an in-house rotating drum was also conducted. Correlations between particle characteristics and flow behavior are thus established.The modelling of biomass flow using the Discrete Element Method (DEM) constitutes a second major part of this research. Challenging aspects of biomass particle modeling are their submillimetric size, low density, elongated shape and cohesive behavior. A material DEM model is implemented using a simplified (multisphere) upscaled representation of particle shape, along with a cohesive contact model. A systematic calibration procedure results in an optimal set of DEM parameters. The experimental shear stress evolution and yield locus can then be realistically reproduced. The avalanching behavior of the powders is also well captured by simulations, both qualitatively and quantitatively. These results highlight the potential of DEM simulations to investigate the effect of particle characteristics, which are driven by torrefaction and grinding conditions, on the flow behavior of powdered biomass.

A mechanical testing device was developed for testing the behavior of mineral-bonded composites under impact shear loading. The device is based on the well-known double shear specimen configuration and was designed to be used in a gravity split-Hopkinson tension bar (SHTB), enabling shear testing at high loading rates. In this work, results from impact shear testing performed on a normal cementitious matrix (NSM) and strain-hardening cement-based composites (SHCC) tested by means of the new device are presented and discussed. Failure behavior and fracture modes are analyzed using optical measurements and digital image correlation (DIC).