Le vrillage est un mode de retour élastique particulier, qui se produit suite à la mise en forme par emboutissage de pièces allongées, à savoir dont une des dimensions est grande devant les deux autres. Le vrillage est caractérisé par la torsion de la pièce autour d’un axe parallèle à la plus grande dimension. D’un point de vue expérimental, le vrillage représente un véritable défi, du fait de la grande dimension, de l’ordre du mètre, des pièces industrielles et de la grande dispersion des valeurs caractéristiques de vrillage obtenues pour un même procédé et un même matériau. En conséquence, l’étude du vrillage en utilisant une échelle réduite sur l’ensemble des dimensions outils et pièce est retenue pour ce travail de thèse, avec un intérêt particulier pour l’influence de l’alignement tôle/outils sur l’intensité du vrillage.L’objectif général de ce travail de thèse est l’étude expérimentale et numérique du vrillage de pièces en forme de U, à partir de flans de longueur 100 mm et d’épaisseur 0,15 mm. Une première partie concerne la caractérisation et modélisation du comportement mécanique du matériau, un acier inoxydable. Des essais mécaniques de traction et cisaillement simple ont été réalisés, avec une mesure locale sans contact du champ de déformation. L’écrouissage ainsi que l’évolution de la pente à la décharge ont été caractérisés, et les paramètres d’un modèle élasto-plastique avec écrouissage mixte et dépendance du module d’Young avec la déformation plastique équivalente ont été identifiés à partir de ces essais.Afin de constituer une base expérimentale sur le vrillage, un dispositif spécifique a été conçu et usiné dans le cadre de cette thèse. Des essais d’emboutissage de flans rectangulaires, de dimensions 100 x 28 mm2, pour atteindre une forme de U de profondeur 7 mm, ont été réalisés. L’alignement de l’éprouvette avec le poinçon et la matrice a été particulièrement contrôlé et deux orientations ont été étudiées : l’éprouvette est soit alignée avec le poinçon, soit désalignée de 2° par rapport à son centre. La forme finale des éprouvettes a été mesurée avec un scanner laser. Le vrillage est caractérisé par le rapport de l’angle entre le fond de deux sections extrêmes sur leur distance respective. Un vrillage de 11°.m-1 a été mesuré pour les éprouvettes désalignées, tandis que pour les éprouvettes alignées, aucun vrillage significatif n’a été obtenu. L’étude des sections transversales de l’éprouvette montre une corrélation entre l’asymétrie du retour élastique causée par l’asymétrie de la géométrie de l’éprouvette, dans le cas désaligné, et le vrillage. Le glissement de l’éprouvette sous le poinçon au cours de l’essai affecte également le vrillage quelque soit l’orientation de l’éprouvette.Finalement, la simulation numérique de la mise en forme d’un flan en forme de U a été effectuée avec le code de calcul Abaqus®. Un solveur explicite est utilisé pour l’étape d’emboutissage et un solveur implicite pour le retour élastique. L’influence de la taille de maillage, ainsi que celle de la loi de comportement du matériau ont été étudiées. Les résultats de la simulation numérique sont alors confrontés aux résultats expérimentaux. / Twisting of metallic sheets is one particular mode of springback that occurs after drawing of elongated parts, i.e. with one dimension much larger than the two others. Twisting is usually characterized by the disorientation angle between the two end sections which turn around an axis parallel to the greatest dimension. From experimental point of view, twisting is very challenging because a lot of data were obtained on industrial-type parts, with one dimension of the order of the meter. These data are usually very dispersed and with the same process parameters, material and geometry, very different values for the twisting parameter can be obtained. As a consequence, the study of twisting phenomenon by using a reduced scale for all the dimensions of the tools and blank is retained in this work of. The influence of the blank alignment with the tools on the intensity of the twisting parameter was particular investigated.The objective of the thesis is the experimental and numerical study of the twisting of U-shaped part, obtained from stainless steel blanks with a length of 100 mm and thickness of 0.15 mm. The first part relates to the characterization and modeling of the material mechanical behavior. Conventional tests such as tension and simple shear were performed. The kinematic contribution to the hardening and the evolution of the loading-unloading slope with the plastic deformation were carried out. The parameters of an elastic-plastic model based on a mixed hardening and degradation of Young’s modulus with the equivalent plastic strain have been identified from these tests.In order to establish an experimental database for twisting, a dedicated device for drawing U-shaped elongated parts was designed and manufactured. Deep-drawing of rectangular blanks, of dimensions 100 x 28 mm2, to achieve a U-shape rail of 7 mm of depth was performed. Two different orientations of the part with respect to the tools were chosen: either aligned with the tools, or purposefully misaligned by 2°. The geometry of the part after springback was laser scanned. Twisting is characterized by the disorientation angle in-between the two end sections of the part over the distance. Several samples were drawn for each configuration, leading to the conclusion that almost no twisting occurs in the first case whereas a twisting parameter of 11°.m-1 corresponded to the second one. The analysis of the geometry of cross sections has shown a correlation between twisting and asymmetry of springback, like the opening of the U-shaped rail, caused by the asymmetry of the blank in the misaligned case. The sliding of the blank beneath the punch during the process also affects twisting whatever its orientation. Finally, finite element simulation of the drawing process, for the two configurations of the blank, within the explicit framework for drawing and implicit one for springback, were carried out using Abaqus® software. The influences of the mesh size as well as the material behavior law on the intensity of twisting parameter were studied. Numerical predictions were compared with experiments.

Benzothiazole dibenzoic acid derivative (BTDB) is well-known organic linkers utilized for the syntheses of various metal organic frameworks, and demonstrates interesting photophysical properties upon concentration variations in solution. The presence of two carboxylic acid functional groups at each side of the rod-like molecule, facilitates dimerization and oligomerization equilibria. Interestingly, dimers and oligomers have completely different emission behaviors from the monomer of the same species. At a low range of concentration, 0.1 – 64 μM, dimerization process is dominant, and that the equilibrium constant of dimer formation found to be 18,000 M-1. On the other hand, in the 64 – 1000 μM concentration range, oligomerization takes over, and that it results in the formation of a small linear chain of 8 molecules, or 4 dimers, with a high equilibrium constant of 1.2 × 1013 M-3. Various experimental measurements and theoretical calculations have suggested hydrogen-bond formation is the main driving force for the dimerization and oligomerization in the nano- and micro- molar regime, and that structure rigidity of a species is a key factor in controlling its photophysical properties, such as emission quantum yield and excited state lifetime.

Nous proposons dans cette thèse d’étudier l’asservissement de systèmes complexes par des commandes à mode glissant à paramètres fixes. L’objectif est de montrer qu’il est possible d’utiliser des commandes robustes tout en gardant une approche de modélisation du système et de synthèse des lois de commande simples.Le système physique considéré est essentiellement un robot manipulateur anthropomorphique flexible à muscles artificiels pneumatiques à sept degrés de liberté.Nous nous intéressons aux commandes robustes et particulièrement aux commandes à régime glissant d’ordre 2, Twisting et Super–twisting, et à la commande équivalente qui leur est généralement associée pour réduire les discontinuées éventuelles de ce type de commandes. Ces commandes sont évaluées à travers des expériences sur un robot flexible. Grâce à ces expériences nous montrons la robustesse de ces commandes, l’influence des incertitudes de la modélisation sur leurs performances et la difficulté de synthétiser leurs paramètres pour un système incertain. Un accélérateur de convergence est proposé afin d’améliorer l’asservissement en régulation et suivi de consigne et la stabilité des systèmes incertains. Ces résultats théoriques sont confirmés expérimentalement grâce au robot flexible.Compte tenu de la difficulté de synthèse des lois de commande Twisting et Super–twisting, une nouvelle approche à base de retours d’états commutés est présentée, l’objectif est de proposer une commande à mode glissant dont la synthèse des paramètres est systématique, et ce, grâce à l’utilisation de conditions de stabilité au sens de Lyapunov. Cette approche baptisée Puma : Polytopic Uncertain Model Approach utilise un modèle polytopique du système, ce qui per- met de garder une modélisation simple en considérant le système, quelque soit sa complexité, comme une boite noire. Cette approche est appliquée au robot flexible en simulation, elle est comparée à une approche similaire pour montrer son intérêt.Afin d’évaluer la pertinence de ces commandes du point de vue performance et simplicité de mise en œuvre, elles sont comparées à l’une des commandes la plus utilisée en industrie : le PID. / This thesis addresses the control of complex systems through fixed parameters sliding modes. The objective being to show that it is possible to use robust control laws while keeping the system model and control law synthesis simple.The considered physical system is a seven d.o.f flexible anthropomorphic manipulator robot driven by pneumatic artificial muscles.We address robust control laws, particularly second order sliding modes, Twisting and Super–twisting together with the equivalent control which is associated to them in order to reduce the discontinuities of these type of controls. These laws are applied onto a flexible robot. Through experiment we show their robustness, the influence of modelling uncertainties on performance and the difficulty in synthesizing their parameters for an uncertain system. A convergence accelerator is proposed for enhancing control quality both in regulation and tracking. These theoretical results are experimentally verified through the flexible robot.Due to the difficulty in synthetizing Twisting and Super–twisting control laws, a new approach based on commuted state feedback is presented. The objective being a sliding mode control law with a systematic parameters synthesis using Lyapunov stability condition. This approach named Puma: Polytopic Uncertain Model Approach uses the system’s polytopic model, which allows keeping modelling simple by considering the system, whatever its complexity may be, as a black box. This approach is applied to a flexible robot in simulation ; it is compared to a similar approach to show its interest.In order to evaluate the relevance of these laws from the point of view of performance and implementation simplicity, they are compared to one of the most popular control law: The PID.

Sehzellen von Insekten sind epitheliale Zellen mit einer charakteristischen, hochpolaren Morphologie und Organisation. Die molekularen Komponenten der Sehkaskade befinden sich im Rhabdomer, einem Saum dicht gepackter Mikrovilli entlang der Sehzelle. Bereits in den 70er Jahren des letzten Jahrhunderts wurde beschrieben, dass die Mikrovilli entlang einer Sehzelle eine unterschiedliche Ausrichtung besitzen, oder in anderen Worten, die Rhabdomere entlang der Sehzell-Längsachse verdreht sind. So sind in den Sehzellen R1-R6 bei dipteren Fliegen (Calliphora, Drosophila) die Mikrovilli im distalen und proximalen Bereich eines Rhabdomers etwa rechtwinkelig zueinander angeordnet. Dieses Phänomen wird in der Fachliteratur als rhabdomere twisting bezeichnet und reduziert die Empfindlichkeit für polarisiertes Licht. Es wurde für das Drosophila-Auge gezeigt, dass diese strukturelle Asymmetrie der Sehzellen mit einer molekularen Asymmetrie in der Verteilung phosphotyrosinierter Proteine an die Stielmembran (einem nicht-mikrovillären Bereich der apikalen Plasmamembran) einhergeht. Zudem wurde gezeigt, dass die immuncytochemische Markierung mit anti-Phosphotyrosin (anti-PY) als lichtmikroskopischer Marker für das rhabdomere twisting verwendet werden kann. Bisher wurde hauptsächlich die physiologische Bedeutung der Rhabdomerverdrehung untersucht. Es ist wenig über die entwicklungs- und zellbiologischen Grundlagen bekannt. Ziel der vorliegenden Arbeit war es, die Identität der phosphotyrosinierten Proteine an der Stielmembran zu klären und ihre funktionelle Bedeutung für die Entwicklung des rhabdomere twisting zu analysieren. Zudem sollte untersucht werden, welchen Einfluss die inneren Sehzellen R7 und R8 auf die Verdrehung der Rhabdomere von R1-R6 haben. Für die zwei Proteinkinasen Rolled (ERK) und Basket (JNK) vom Typ der Mitogen-aktivierten Proteinkinasen (MAPK) konnte ich zeigen, dass sie in ihrer aktivierten (= phosphorylierten) Form (pERK bzw. pJNK) eine asymmetrische Verteilung an der Stielmembran aufweisen vergleichbar der Markierung mit anti-PY. Weiterhin wurde diese asymmetrische Verteilung von pERK und pJNK ebenso wie die von PY erst kurz vor Schlupf der Fliegen (bei ca. 90% pupaler Entwicklung) etabliert. Durch Präinkubationsexperimente mit anti-PY wurde die Markierung mit anti-pERK bzw. anti-pJNK unterbunden. Diese Ergebnisse sprechen dafür, dass pERK und pJNK zu den Proteinen gehören, die von anti-PY an der Stielmembran erkannt werden. Da es sich bei ERK und JNK um Kinasen handelt, ist es naheliegend, dass diese an der Entwicklung des rhabdomere twisting beteiligt sein könnten. Diese Hypothese wurde durch die Analyse von hypermorphen (rl SEM)und hypomorphen (rl 1/rl 10a) Rolled-Mutanten überprüft. In der rl SEM-Mutante mit erhöhter Aktivität der Proteinkinase erfolgte die asymmetrische Positionierung von pERK an der Stielmembran sowie die Mikrovillikippung schon zu einem früheren Zeitpunkt in der pupalen Entwicklung. Im adulten Auge war die anti-PY-Markierung im distalen Bereich der Sehzellen intensiver sowie der Kippwinkel vergrößert. In der rl 1/rl 10a-Mutanten mit reduzierter Kinaseaktivität waren die anti-PY-Markierung und der Kippwinkel im proximalen Bereich der Sehzellen verringert. Die Proteinkinase ERK hat somit einen Einfluss auf die zeitliche Etablierung des rhabdomere twisting wie auch auf dessen Ausprägung im Adulttier. Die Rhabdomerverdrehung sowie die Änderung im anti-PY-Markierungsmuster erfolgen an den Sehzellen R1-R6 relativ abrupt auf halber Ommatidienlänge, dort wo das Rhabdomer von R7 endet und das von R8 beginnt. Es stellte sich deshalb die Frage, ob die Rhabdomerverdrehung an R1-R6 durch die Sehzelle R7 und/oder R8 beeinflusst wird. Um dieser Frage nachzugehen wurden Mutanten analysiert, denen die R7- oder die R8-Photorezeptoren bzw. R7 und R8 fehlten. Das wichtigste Ergebnis dieser Untersuchungen war, dass bei Fehlen von R8 die Rhabdomerverdrehung bei R1-R6 nach keinen erkennbaren Regeln erfolgt. R8 ist somit Voraussetzung für die Etablierung der Rhabdomerverdrehung in R1-R6. Folgendes Modell wurde auf Grundlage dieses und weiterer Ergebnisse erarbeitet: Im dritten Larvenstadium rekrutiert R8 die Sehzellpaare R2/R5, R3/R4 und R1/R6. Dabei werden R1-R6 durch den Kontakt zu R8 „polarisiert“. Abschließend wird R7 durch R8 rekrutiert. Dies führt zu einer Fixierung der Polarität von R1-R6 durch R7. Die Ausführung der Mikrovillikippung anhand der festgelegten Polarität erfolgt in der späten Puppenphase. Die Proteinkinase ERK ist an diesem letzten Morphogeneseprozess beteiligt. / Visual cells of insects are epithelial cells with a characteristic morphology and organization. The molecular components of the signalling cascade are arranged in the rhabdomere, an array of densely packed microvilli along the side of the cell body. Already in the 70s of the last century it was described that microvilli point in different directions in various segments of the rhabdomere. Thus, in Dipteran flies (Calliphora, Drosophila) microvilli in the distal part of visual cells R1-R6 are nearly perpendicular to the microvilli in the proximal portion. This phenomenon is termed rhabdomere twisting and decreases the sensitivity of visual cells to polarized light. For Drosophila, structural asymmetry was shown to correlate with molecular asymmetry in the distribution of phosphotyrosinated proteins to the stalk (a non-microvillar region of the apical plasma membrane). Furthermore, this asymmetric distribution of antiphosphotyrosine (anti-PY) provides a light microscopic marker for rhabdomere twisting. So far little is known about the developmental and cell biological basis of rhabdomere twisting. Purpose of the present study was to identify the phosphotyrosinated proteins at the stalk und to analyse their functional relevance for the development of rhabdomere twisting. Moreover, influence of the inner visual cells R7 and R8 on rhabdomere twisting should be examined. Two protein kinases of the MAPK-type, Rolled (ERK) and Basket (JNK), show for their activated (= phosphorylated) forms (pERK and pJNK respectively) an asymmetric distribution to the stalk comparable to labelling with anti-PY. In addition, this asymmetric distribution of pERK, pJNK and also PY is established shortly before eclosion of the fly. Preincubation experiments with anti-PY abolished labelling with anti-pERK and anti-pJNK respectively. These results indicate that pERK and pJNK belong to the proteins on the stalk recognized by anti-PY. ERK and JNK are kinases and therefore are likely to be involved in the development of rhabdomere twisting. To test this hypothesis I analysed hypermorph (rl SEM) and hypomorph (rl 1/rl 10a) rolled mutants. In rl SEM mutants with increased kinase activity asymmetric positioning of pERK to the stalk and tilting of microvilli occurred earlier during pupal development. In the adult eye anti-PY labelling was more intensive in the distal part of the visual cells, and congruently the microvillar tilt angle was increased. In rl 1/rl 10a mutants with reduced kinase activity anti-PY labelling and microvillar tilt angle were reduced in the proximal part of visual cells. Hence, protein kinase ERK has an influence on developmental establishment of rhabdomere twisting and its specification in the adult eye. In R1-R6 rhabdomere twisting as well as changes in anti-PY labelling pattern take place within a narrow range halfway along the rhabdomere where the rhabdomere of R7 ceases and that of R8 begins. So the question arises whether rhabdomere twisting of R1-R6 is influenced by R7 and/or R8. To answer that question I analysed mutants that lack R7 or R8 or both visual cells. Most importantly absence of R8 leads to a disorganized rhabdomere twisting in R1-R6. Consequently R8 seems to be required for the establishment of rhabdomere twisting in R1-R6. Following working model was developed: in the third larval instar R8 recruits pairs of visual cells R2/R5, R3/R4 and R1/R6. In that process R1-R6 become „polarised“ by the contact to R8. Finally R7 is recruited by R8. That fixes polarity of R1-R6 by R7. The active tilting of the microvilli on the basis of the given polarity is carried out in late pupal development with the help of protein kinase ERK.

Mild Traumatic Brain Injuries (mTBIs) are non-penetrating brain injuries that do not result in gross pathological lesions, yet they may cause a spectrum of cognitive and behavioral deficits. mTBI has been placed in the spotlight because of increased awareness of blast induced and sports-related concussions, but the underlying pathophysiological mechanisms are poorly understood. Several studies have implicated neuronal membrane poration and ion channel dysfunction as the primary mechanism of injury. We hypothesized that injury forces utilize mechanically-sensitive, transmembrane integrin proteins, which are coupled to the neuronal cytoskeleton (CSK) and distribute injury forces within the intracellular space, disrupting CSK organization and reducing intercellular neuronal functionality. To test this, magnetic beads were coated with adhesive protein, allowing them to bind to integrins in the neuronal membrane in vitro. To apply forces to the neurons via the bound beads, we built custom magnetic tweezers and demonstrated that focal adhesions (FACs) formed at the site of bead binding. We showed that the beads were coupled to the CSK via integrins by measuring the disparate adhesion of the soma and neurite to their underlying substrate. The soma also required more force to detach than neurites, correlating with the FAC density between each neuronal microcompartment and substrate. We then utilized the magnetic tweezers to test whether beads bound to integrins injured neurons more than beads that bound to neurons nonspecifically. Integrin-bound beads injured neurons more often and the injury was characterized by the formation of focal swellings along axons, reminiscent of Diffuse Axonal Injury. While integrin-bound beads initiated swellings throughout neurons, beads bound nonspecifically only caused local injury where beads were attached to neurons. To demonstrate the electrical dysfunction of integrin-mediated injury forces, we adapted Magnetic Twisting Cytometry to simultaneously apply injury forces to beads bound to multiple cells within neuronal networks in vitro. The formation of focal swellings resulted in reduced axonal electrical activity and decreased coordinated network activity. These data demonstrate that the mechanical insult associated with mTBI is propagated into neurons via integrins, initiating maladaptive CSK remodeling that is linked to impaired electrical function, providing novel insight into the underlying mechanisms of mTBI. / Engineering and Applied Sciences

Micro Air Vehicles (MAVs) are defined as a class of vehicles with their larger dimension not exceeding 15 cm and weighing 100 gm. The three main approaches for providing lift for such vehicles are through fixed, rotating and flapping wings. The flapping wing MAVs are more efficient in the low Reynolds-number regime than conventional wings and rotors. Natural flapping flyers, such as birds and insects, serve as a natural source of inspiration for the development of MAV. Flapping wing design is one of the major challenges to develop an MAV because it is not only responsible for the lift, but also propulsion and maneuvers. Two important issues are addressed in this thesis: (1) an equivalent beam-type modeling of actual insect wing is proposed based on the experimental data and (2) development of the numerical framework for design and analysis of insect scale smart flapping wing. The experimental data is used for structural modeling of the blowfly Calliphora wing as a stepped cantilever beam with nine spanwise sections of varying mass per unit lengths, flexural rigidity (EI) and torsional rigidity (GJ) values. Natural frequencies, both in bending and torsion, are obtained by solving the homogeneous part of the respective governing differential equations using the finite element method. It is found that natural frequency in bending and torsion are 3.17 and 1.57 times higher than flapping frequency of Calliphora wing, respectively. The results provide guidelines for the biomimetic structural design of insect-scale flapping wings. In addition to the structural modeling of the insect wing, development of the biomimetic mechanisms played a very important role to achieve a deeper insight of the flapping flight. Current biomimetic flapping wing mechanisms are either dynamically scaled or rely on pneumatic and motor-driven flapping actuators. Unfortunately, these mechanisms become bulky and flap at very low frequency. Moreover, mechanisms designed with conventional actuators lead to high weight and system-complexity which makes it difficult to mimic the complex wingbeat kinematics of the natural flyers. The usage of the actuator made of smart materials such as ionic polymer metal composites (IPMCs) and piezoceramics to design flapping wings is a potential alternative. IPMCs are a relatively new type of smart material that belongs to the family of Electroactive Polymers (EAP) which is also known as “artificial muscles”. In this work, structural modeling and aerodynamic analysis of a dragonfly inspired IPMC flapping wing are performed using numerical simulations. An optimization study is performed to obtain improved flapping actuation of the IPMC wing. Later, a comparative study of the performances of three IPMC flapping wings having the same size as the actual wings of three different dragonfly species Aeshna Multicolor, Anax Parthenope Julius and Sympetrum Frequens is conducted. It is found that the IPMC wing generates sufficient lift to support its own weight and carry a small payload. In addition to the IPMC, piezoelectric materials are also considered to design a dragonfly inspired flapping wing because they have several attractive features such as high bandwidth, high output force, compact size and high power density. The wings of birds and insects move through a large angle which may be obtained using piezofan through large deflection. Piezofan which is one of the simple motion amplifying mechanisms couples a piezoelectric unimorph to an attached flexible wing and is competent to produce large deflection especially at resonance. Non-linear dynamic model for the piezoelectrically actuated flapping wing is done using energy method. It is shown that flapping angle variations of the smart flapping wing are similar to the actual dragonfly wing for a specific feasible voltage. Subsequently, a comparative study of the performances of three piezoelectrically actuated flapping wings is performed. Numerical results show that the flapping wing based on geometry of dragonfly Sympetrum Frequens wing is suitable for low speed flight and it represents a potential candidate for use in insect scale micro air vehicles. In this study, single crystal piezoceramic is also considered for the flapping wing design because they are the potential new generation materials and have attracted considerable attention due to superior electromechanical properties. It is found that the use of single crystal piezoceramic can lead to considerable amount of wing weight reduction and increase of aerodynamic forces compared to conventional piezoelectric materials such as PZT-5H. It can also be noted that natural fliers flap their wings in a vertical plane with a change in the pitch of the wings during a flapping cycle. In order to capture this particular feature of the wingbeat kinematics, coupled flapping-twisting non-linear dynamic modeling of piezoelectrically actuated flapping wing is done using energy method. Excitation by the piezoelectric harmonic force generates only the flap bending motion, which in turn, induces the elastic twist motion due to interaction between flexural and torsional vibrations modes. It is found that the value of average lift reaches to its maximum when the smart flapping wing is excited at a frequency closer to the natural frequency in torsion. Moreover, consideration of the elastic twisting of flapping wing leads to an increase in the lift force.

L’objectif de cette thèse est de proposer des stratégies de diagnostic dans le cas d'une commande en vitesse sans capteur mécanique (vitesse/position) d’une machine asynchrone triphasée en présence de défaut d'ouverture des transistors IGBT (Insulated Gate Bipolar Transistor) de l’onduleur. Une étude de l’impact de ces défauts sur les performances de ces structures sans capteur mécanique en termes de stabilité et de robustesse des observateurs en mode dégradé est présentée. Un observateur par mode glissant (Sliding Mode Observer) à base de modèle est développé et validé expérimentalement en vue de la commande sans capteur mécanique de la machine asynchrone triphasée. Les signaux issus de l’observateur (approche modèle) sont utilisés conjointement avec ceux mesurés (approche signale) pour former une approche hybride de diagnostic de défauts des transistors IGBT de l’onduleur. Un observateur par mode glissant d’ordre 2 à base d’un algorithme Super-Twisting est ensuite développé en vue d’améliorer la stabilité et d’assurer la continuité de fonctionnement du système en présence d'un défaut afin de pouvoir appliquer une stratégie de commande tolérante aux défauts dans les meilleures délais et conditions de fonctionnement. / The main goal of this thesis is to propose diagnostic strategies in the case of a sensorless speed control of a three-phase induction motor under an opened-switch or opened-phase fault. A qualitative analysis of the performances, in terms of stability and robustness, of sensorless control applied to the electrical drive in pre-fault and post-fault operation modes is presented. A model-based sliding mode observer is developed and experimentally validated for sensorless speed control of three-phase induction motor. The signals issued from the observer (model approach) as well as the measured ones (signal approach) are simultaneously used to form a hybrid approach for inverter open-switch fault detection and identification. A second-order sliding mode observer based on Super-Twisting algorithm (STA) is also developed to improve the stability and to ensure the continuity of operation of the electrical drive especially during transient states induced by the fault, permitting thus to apply the reconfiguration step without losing the control

Cette thèse porte sur le développement de nouvelles stratégies de commande et d’observation adaptatives par Modes Glissants (MG) et par Modes Glissants d’Ordres Supérieurs (MGOS). En effet, la mise en œuvre des commandes par MG et MGOS classiques nécessite la connaissance des limites supérieures des perturbations ou de leurs dérivées, souvent inconnues. Le premier apport de cette thèse est la synthèse d’une stratégie d’adaptation permettant d'assurer la convergence de la variable de glissement vers un voisinage prédéfini de zéro sans nécessiter d'informations sur les perturbations ou leurs dérivées et sans surestimation du gain. Cette stratégie est ensuite déclinée pour concevoir : deux commandes par MG d’ordre 1 et 2, une commande par mode glissant intégral, ainsi qu’une version du différenciateur de Levant. La deuxième contribution de la thèse est la mise au point de deux commandes adaptatives par MGOS discontinues. Ces deux algorithmes assurent un mode glissant d'ordre n en s’affranchissant de la connaissance de la limite supérieure de la perturbation et de sa dérivée. Enfin, afin de montrer l’efficacité des algorithmes proposés, ils sont appliqués avec succès à travers des simulations pour la commande d’un système de conversion de l’énergie éolienne et la commande d’un moteur à induction linéaire pour la cogénération. / This thesis deals with the development of novel strategies to adapt higher order sliding mode controllers and observers. The implementation of classics first order and higher order sliding mode controllers requires the knowledge of the upper bound of the disturbance or its derivative, which are often not known. The first contribution of this thesis is the design of an adaptive strategy that can ensure the convergence of the sliding variable to a predefined neighborhood of zero without requiring any information of the disturbance or its derivative and without overestimating the adaptive gain. This adaptive strategy is then declined for the design of the first order, second order and integral sliding mode controllers, and for the Levant's differentiator. The second contribution of the thesis is the development of two adaptive strategies for discontinuous higher order sliding mode control. The proposed two algorithms can provide the achievement of n-order sliding mode despite disturbances with unknown upper bounds or with unknown upper bounds of their derivatives. Finally, in order to show the effectiveness of the proposed algorithms, they are successfully applied through simulations to control the wind energy conversion system and the linear induction motor system for cogeneration.

L'hyperdéformation est une technique efficace pour transformer la microstructure des métaux en une structure de grain de taille inférieure au micron ou même en nanostructure (<100 nm). Cette très petite taille de grain confère d'excellentes propriétés mécaniques au matériau. Dans ce travail de thèse, deux techniques d'hyperdéformation récemment développées, appelées High Pressure Tube Twisting (HPTT) and Cyclic Expansion and Extrusion (CEE) ont été appliquées à température ambiante sur différents matériaux métalliques. La fragmentation de la microstructure ainsi que le développement de la texture cristallographique ont été analysés en détails par la diffraction d'électrons rétrodiffusés (EBSD), par microscopie électronique en transmission (TEM), par transmission Kikuchi diffraction (TKD) ainsi que par diffraction des rayons X (XRD). Le gradient de déformation de cisaillement dans l'épaisseur des tubes d'aluminium déformés par HPTT a été déterminé par une méthode de mesure locale du cisaillement. Ce gradient de cisaillement induit une hétérogénéité aussi bien de microstructure que de texture dans les échantillons d'aluminium et de magnésium purs ainsi que dans l'alliage Al-4%Mg en solution solide. La micro-dureté et la taille de grain dans différentes zones ont été mesurées et analysées en fonction du taux cisaillement local. Les tailles de grain limites atteintes de façon stationnaire pour ces différents matériaux produit par HPTT sont respectivement de 700 nm, 900 nm et 100 nm. L'évolution de texture du magnésium pur après HPTT jusqu'à un cisaillement de 16 a été simulée par cisaillement simple par le model auto-cohérent (VPSC), le résultat de simulation a montré de bons accords avec les mesures de texture obtenues par XRD. Sur la base des mesures de distribution de désorientation dans l'aluminium déformé par HPTT, une nouvelle technique de détermination du taux de cisaillement local dans les procédés d'hyper déformation a été proposée. Cette nouvelle technique a été appliquée sur deux échantillons d'aluminium produit par twist extrusion (TE) et par torsion à extrémités libres. Les échantillons d'aluminium et de cuivre ont été déformés intensément par CEE. Les évolutions de texture et de microstructures ont été mesurées par EBSD, montrant un gradient du centre à la périphérie des échantillons cylindriques. L'évolution de texture dans le cuivre déformé par CEE a été simulée par le modèle VPSC en utilisant un modèle de ligne de courant pour décrire la déformation dans le procédé. Les résultats de simulation confirment les caractéristiques de la texture expérimentale observées après CEE. Le comportement en traction du cuivre pré-déformé par grande déformation en torsion a ensuite été testé. En dépit du gradient de cisaillement existant dans la barre, une technique a été proposée pour obtenir la courbe contrainte-déformation pour ce type de matériau. / Severe plastic deformation (SPD) is an efficient technique to transform the microstructure of bulk metals into ultra fine grained structure with grain sizes less than 1 µm or even into nanostructure with nano-grains of less than 100 nm in diameter. The very small grain size attributes excellent mechanical properties to the material. In present thesis work, two recently developed SPD techniques, namely, High Pressure Tube Twisting (HPTT) and Cyclic Expansion and Extrusion (CEE) were performed on different metallic materials at room temperature. Details of fragmentation of microstructure and metallographic texture evolution were investigated by electron backscattered diffraction (EBSD), transmission electron microscopy (TEM), transmission kikuchi diffraction (TKD) and X-ray diffraction (XRD). Shear strain gradient across the thickness of the HPTT deformed Al tube sample was found by a local shear measurement method. This shear strain gradient induced the inhomogeneity of microstructure and texture in HPTT deformed pure Al, solid solution alloy Al-4%Mg and pure Mg. The microhardness and average grain size in different zones as a function of shear strain were measured. The limiting steady grain sizes in the steady state for these different materials produced by HPTT were 700 nm, 100 nm and 900 nm, respectively. The texture evolution of pure Mg in HPTT up to a shear strain of 16 was simulated in simple shear using the self-consistent (VPSC) polycrystal model and showed good agreements with the experimental results measured by XRD. Based on the measured disorientation distribution function in HPTT deformed Al, a new technique for the magnitude of local shear strain in SPD was proposed. This new technique was applied to a protrusion produced in twist extrusion (TE) and to an Al sample deformed in free-end torsion. Cu and pure Al samples were intensively deformed by the CEE SPD technique. The microstructure and texture evolutions were measured by EBSD, showing a gradient from the center-zone to the edge part of the rod sample. The texture evolution of CEE deformed Cu was simulated by the VPSC polycrystal model using a flow line function. The simulation results confirmed the experimental texture features observed in the CEE process. The tensile testing behavior of large strain torsion pre-processed Cu was examined. In spite of the shear strain gradient existing in the bar, a technique was proposed to obtain the tensile stress-strain curve of such gradient material.

Grätzel cells or Dye-Sensitized Solar Cells (DSSCs) are considered one of the most promising methods to convert the sun's energy into electricity due to their low cost and simple technology of production. The Grätzel cell is based on a photosensitizer adsorbed on a low band gap semiconductor. The photosensitizer can be a metal complex or an organic dye. Organic dyes can be produced on a large scale resulting in cheaper dyes than complexes based on rare elements. However, the performance of Grätzel cells based on metal-free, organic dyes is not high enough yet. The dye's performance depends primarily on the electron dynamics. The electron dynamics in Grätzel cells includes electron injection, recombination, and regeneration. Different deactivation processes affect the electron dynamics and the cells’ performance. In this thesis, the electron dynamics was explored by various time-resolved spectroscopic techniques, namely time-correlated single photon counting, streak camera, and femtosecond transient absorption. Using these techniques, new deactivation processes for organic dyes used in DSSCs were uncovered. These processes include photoisomerization, and quenching through complexation with the electrolyte. These deactivation processes affect the performance of organic dyes in Grätzel cells, and should be avoided. For instance, the photoisomerization can compete with the electron injection and produce isomers with unknown performance. Photoisomerization as a general phenomenon in DSSC dyes has not been shown before, but is shown to occur in several organic dyes, among them D149, D102, L0 and L0Br. In addition, D149 forms ground state complexes with the standard iodide/triiodide electrolyte, which directly affect the electron dynamics on TiO2. Also, new dyes were designed with the aim of using ferrocene(s) as intramolecular regenerators, and their dynamics was studied by transient absorption. This thesis provides deeper insights into some deactivation processes of organic dyes used in DSSCs. New rules for the design of organic dyes, based on these insights, can further improve the efficiency of DSSCs.