Este trabalho tem por objetivo a investigação de atenuação de ondas acústicas superficiais (OAS) em filmes finos granulares supercondutores de PbO e Pb depositados por sputtering reativo em substratos piezoelétricos de LiNbO3 e quartzo (ST). As medidas de atenuação de OAS em função da temperatura foram efetuadas para diferentes potências de radiofreqüência, e em freqüência variando de 550 MHz a aproximadamente 700 MHz. A atenuação de OAS medida em filme granular de chumbo (550&#197), dotada de alta resistividade de filme (de 1000 &#937/&#9001) se manifesta piezoeletricamente induzida e proporcional à resistividade do filme. No estado supercondutor esta medida de atenuação excede esta simples relação. Esta atenuação excedente é atribuída à resistência local produzida pela presença de dipolos de vórtice-antivórtice / The subject of this work is the investigation of surface acoustic waves (SAW) on superconducting Pb and PbO granular thin films deposited by sputtering on piezoelectric substrate (LiNbO3 and quartz ST). The SAW attenuation was measured as a function of the temperature (1,3K to 20K) for different r.f. Power, in frequencies from 550 MHz to 700 MHz. The SAW attenuation, measured on granular lead film (550 &#197) with high sheet resistivity (1000 &#937/&#9001) appears to be piezoelectrically induced and should be proportional to the sheet resistivity. In the superconducting state the measured attenuation exceeds this simple relation. This excess attenuation is ascribed to the local resistance produced by the presence of vortex-antivortex dipoles

Dusty plasmas, defined as plasmas of ions, electrons, neutrals, and charged micron to sub-micron dust particles, support a rich diversity of physical states. These states (ranging from solids to liquids to gas) are determined by the ratio of the Coulomb potential energy between dust particles to the particles kinetic energy and allow for a broad range of phenomena, from crystallization to dust acoustic waves. Due to various dusty plasma interactions, dust acoustic waves can be nonlinear and exhibit various wave phenomena, from topological wave defects to shock waves to structure formations. In this thesis, I investigate a spectrum of plasma and wave interactions in liquid-like dusty plasmas and focus on a range of dust acoustic wave phenomena observed experimentally in a dc discharge dusty plasma. By developing various experimental techniques, dust acoustic wave diffraction and topological wave defects, dust acoustic shock waves, temporal dust acoustic wave growth, and structure forming dust acoustic waves were observed. I begin in Chapter 2 with the diffraction of dust acoustic waves, which I investigated by introducing a glass rod into the dusty plasma. The resulting diffraction pattern was compared to acoustic wave diffraction in a neutral gas. In addition to the diffraction pattern, topological wave defects were observed to form. I continue Chapter 2 with a preliminary investigation into topological wave defects in dust acoustic waves. Chapter 3 follows with three nonlinear dust acoustic wave experiments. I created a shock tube like profile for dust acoustic waves using a single slit. The shock-tube like potential resulted in two sets of nonlinear dust acoustic waves, coalescing high and low amplitude waves and dust acoustic waves that developed into dust acoustic shock waves. The self-excited dust acoustic shock waves were compared to theoretical models. The third nonlinear dust acoustic wave phenomenon that I investigated was a reverse drift mode that appears in high amplitude dust acoustic waves. I propose a wave process based on dust particle dynamics in high amplitude dust acoustic waves to explain the observations. In Chapter 4, I describe an experimental technique that I developed to create a quiescent drifting dusty plasma. The drifting dusty plasma was used to observe dust acoustic wave growth from thermal density fluctuations. The observed growth rate and frequency were compared kinetic and fluid models. In Chapter 5, I describe experimental observations of a structure forming instability in dusty plasmas. By increasing the discharge current, transient and aperiodic dust density striations formed. I characterized the transient and stationary modes and compared the stationary mode to an ionization/ion-drag instability and a polarization instability.

In this thesis, the author proposes and presents a novel simulation technique for the analysis of multilayered Flexural Plate Wave (FPW) devices based on the convergence of the Finite Element method (FEM) with classical Surface Acoustic Wave (SAW) analysis techniques and related procedures. Excellent agreement has been obtained between the author's approach and other more conventional modelling techniques. Utilisation of the FEM allows the performance characteristics of a FPW structure to be critically investigated and refined before undertaking the costly task of fabrication. Based on a series of guidelines developed by the author, it is believed the proposed technique can also be applied to other acoustic wave devices. The modelling process developed is quite unique as it is independent of the problem geometry as verified by both two and three dimensional simulations. A critical review of FEM simulation parameters is presented and their effect on the frequency domain response of a FPW transducer given. The technique is also capable of simultaneously modelling various second-order effects, such as triple transit, diffraction and electromagnetic feedthrough, which often requires the application of several different analysis methodologies. To verify the results obtained by the author's novel approach, several commonly used numerical techniques are discussed and their limitations investigated. The author initially considers the Transmission Matrix method, where it is shown that an inherent numerical instability prevents solution convergence when applied to large frequency-thickness products and complex material properties which are characteristic of liquids. In addition the Stiffness Matrix method is investigated, which is shown to be unconditionally stable. Based on this technique, particle displacement profiles and mass sensitivity are presented for multilayered FPW structures and compared against simpler single layer devices commonly quoted in literature. Significant differences are found in mass sensitivity between single layer and multilayered structures. Frequency response characteristics of a FPW device are then explored via a spectral domain Green's function, which serves as a further verification technique of the author's novel analysi s procedure. Modifications to the spectral domain Green's function are discussed and implemented due to the change in solution geometry from SAW to FPW structures. Using the developed techniques, an analysis is undertaken on the applicability of FPW devices for sensing applications in liquid media. Additions are made to both the Stiffness Matrix method and FEM to allow these techniques to accurately incorporate the influence of a liquid layer. The FEM based approach is then applied to obtain the frequency domain characteristics of a liquid loaded FPW structure, where promising results have been obtained. Displacement profiles are considered in liquid media, where it is shown that a tightly coupled Scholte wave exists that is deemed responsible for most reported liquid sensing results. The author concludes the theoretical analysis with an in-depth analysis of a FPW device when applied to density, viscosity and mass sensing applications in liquid media. It is shown that a single FPW device is potentially capable of discriminating between density and viscosity effects, which is typically a task that requires a complex and costly sensor array.

Bubbles are often present in the natural ocean. Bubbly liquid will have the significant influence the sound propagation, and creates a significant disturbance to under water target's detection. Therefore, it is an important research subject of bubble influence to the sound wave propagation. This study used the sonar training system which developed by British's iTP corporation, through suitable additional design discuss the attenuation of sound propagating through a bubble screen. At first this study collects and infers the formula by the literature review. Secondly, the experimental design of measuring the attenuation of sound wave. The experiment process by using two parallel iron boards to carry on the measurement of gas-volume fraction. Then correlate with the sound pressure from the measurement of hydrophone. After curve fitting, we can clearly know the each other correlation. Finally taking the result compare with the attenuation coefficient formula. The experimental consists of two parts. The first part is to measure the gas-volume fraction of the bubbly liquid contained in the screen; while the second part is to measure the sound attenuation of the bubble screen. The result display that the bubble screen can attenuate about 8 dB per centimeter as the gas-volume fraction stay at 1 percent. At high gas-volume fraction the coefficient of attenuation has increased, and is different from theoretical value. This is because the bubble's correlation has not been considered. In addition, the low frequency sound wave is close to theoretical value, but the high frequency sound wave has big different to theoretical value. Because the high frequency sound wave's wavelength is too small to satisfy the condition. At experiment I suggest to use more appropriate transducers and precise bubble's tube. Thus the experimental result will be better.

The present work explores the possibilities of adapting poro-elastic lightweight acoustic materials to specific applications. More explicitly, a design approach is presented where finite element based numerical simulations are combined with optimization techniques to improve the dynamic and acoustic properties of lightweight multilayered panels containing poro-elastic acoustic materials. The numerical models are based on Biot theory which uses equivalent fluid/solid models with macroscopic space averaged material properties to describe the physical behaviour of poro-elastic materials. To systematically identify and compare specific beneficial or unfavourable material properties, the numerical model is connected to a gradient based optimizer. As the macroscopic material parameters used in Biot theory are interrelated, they are not suitable to be used as independent design variables. Instead scaling laws are applied to connect macroscopic material properties to the underlying microscopic geometrical properties that may be altered independently. The design approach is also combined with a structural sandwich panel mass optimization, to examine possible ways to handle the, sometimes contradicting, structural and acoustic demands. By carefully balancing structural and acoustic components, synergetic rather than contradictive effects could be achieved, resulting in multifunctional panels; hopefully making additional acoustic treatment, which may otherwise undo major parts of the weight reduction, redundant. The results indicate a significant potential to improve the dynamic and acoustic properties of multilayered panels with a minimum of added weight and volume. The developed modelling techniques could also be implemented in future computer based design tools for lightweight vehicle panels. This would possibly enable efficient mass reduction while limiting or, perhaps, totally avoiding the negative impact on sound and vibration properties that is, otherwise, a common side effect of reducing weight, thus helping to achieve lighter and more energy efficient vehicles in the future. / <p>QC 20120815</p>

The thickness shear mode acoustic wave (TSM) sensor, operated in a flow-through format, has been widely used in bioanalytical research. My research is mainly focused on the study of surface-attached biomolecules and cells using the TSM sensor, including lesions in DNA, conformational change of calmodulin, as well as the properties and attachment of rat aortic smooth muscle cells. Aldehydic apurinic or apyrimidinic sites (AP sites) that lack a nucleobase moiety are one of the most common forms of toxic lesions in DNA. In this work, synthesized oligodeoxyribonucleotides containing one, two, or three abasic sites were hybridized to complementary sequences immobilized on the gold electrode of the TSM device by affinity binding. The influence of AP sites on local base stacking energy and geometry caused a dramatic destabilization of the DNA duplex structure, which was detected by the TSM sensor. The signals detected by TSM correlated well with the thermostability of DNA duplexes in solution. The results indicate that both the number of sites and their localization in the double-stranded structure influence the stability of a 19 b.p. duplex. TSM was also used to detect the binding of ions or peptides to surface-attached calmodulin. The interaction between calmodulin and ions induced an increase in resonant frequency and a decrease in motional resistance. In addition, these signal changes were reversible upon washing with buffer. The response was interpreted as a decrease in surface coupling induced by exposure of hydrophobic domains on the protein, and an increase in the length of calmodulin by approximately 3 Å. In addition, the interaction of the protein with peptide together with calcium ions was detected successfully, despite the relatively low molecular mass of the 2-kDa peptide. In addition, the attachment of smooth muscle cells to various surfaces has been monitored by TSM. These surfaces include laminin, fibronectin and bare gold. The results of these experiments in terms of changes of frequency (fs) and resistance (Rm) were analyzed. The responses of the surface-bound cells to the introduction of various ions, depolarisation events and damage subsequent to exposure to hydrogen peroxide were also observed. Morphological changes in the cells, as confirmed by atomic force microscopy and scanning electron microscopy, are correlated with results from the TSM sensor.

The thickness shear mode acoustic wave (TSM) sensor, operated in a flow-through format, has been widely used in bioanalytical research. My research is mainly focused on the study of surface-attached biomolecules and cells using the TSM sensor, including lesions in DNA, conformational change of calmodulin, as well as the properties and attachment of rat aortic smooth muscle cells. Aldehydic apurinic or apyrimidinic sites (AP sites) that lack a nucleobase moiety are one of the most common forms of toxic lesions in DNA. In this work, synthesized oligodeoxyribonucleotides containing one, two, or three abasic sites were hybridized to complementary sequences immobilized on the gold electrode of the TSM device by affinity binding. The influence of AP sites on local base stacking energy and geometry caused a dramatic destabilization of the DNA duplex structure, which was detected by the TSM sensor. The signals detected by TSM correlated well with the thermostability of DNA duplexes in solution. The results indicate that both the number of sites and their localization in the double-stranded structure influence the stability of a 19 b.p. duplex. TSM was also used to detect the binding of ions or peptides to surface-attached calmodulin. The interaction between calmodulin and ions induced an increase in resonant frequency and a decrease in motional resistance. In addition, these signal changes were reversible upon washing with buffer. The response was interpreted as a decrease in surface coupling induced by exposure of hydrophobic domains on the protein, and an increase in the length of calmodulin by approximately 3 Å. In addition, the interaction of the protein with peptide together with calcium ions was detected successfully, despite the relatively low molecular mass of the 2-kDa peptide. In addition, the attachment of smooth muscle cells to various surfaces has been monitored by TSM. These surfaces include laminin, fibronectin and bare gold. The results of these experiments in terms of changes of frequency (fs) and resistance (Rm) were analyzed. The responses of the surface-bound cells to the introduction of various ions, depolarisation events and damage subsequent to exposure to hydrogen peroxide were also observed. Morphological changes in the cells, as confirmed by atomic force microscopy and scanning electron microscopy, are correlated with results from the TSM sensor.

This thesis proposes a new proof of the acoustic transparency theorem for material with a bounded variation. The theorem states that if the material properties (density, bulk modulus) is of bounded variation, the net power transmitted through the point z = 0 over a time interval [−T,T] is greater than some constant times the energy at the time zero over a spatial interval [0,Z], provided that T equals the time of travel of a wave from 0 to Z. This means the reflected energy of an input into the earth will be received. Otherwise, the reflections may not arrive at the surface. A proof gives a lower bound for material properties (density, bulk modulus) with bounded variation using sideways energy estimate. A different lower bound that works only for piecewise constant coefficients is also given. It gives a lower bound by analyzing reflections and transmissions of the waves at the jumps of the material properties. This thesis also gives an example to illustrate that the bounded variation assumption may not be necessary for the medium to be transparent. This thesis also discusses relations between the transparency property and the data of an inverse problem.

In this study, AlN films are deposited using reactive RF magnetron sputter on various bottom metals, such as Mo, Al and Pt. The orientation of piezoelectric AlN thin films on different bottom electrode materials are investigated. Moreover, the acoustic Bragg reflectors deposited by DC magnetron sputter are composed of alternating layers of high and low acoustic impedance materials. To improve the performance of the reflectors, rapid thermal anneal and deposition process control over roughness of the thin film are also investigated. The resonance characteristics are improved obviously by deposition process control over thin films. The roughness control is the key factor of good frequency responses of SMR. In addition, the more layer of the reflectors the better the frequency response we obtained. The frequency responses of SMR are slightly improved by rapid thermal annealing procsess. Although defects in the thin films would be eliminated, nevertheless the thin film roughness became worse after annealing. This phenomenon would limit the improvement of frequency responses.

Recently, there are great demands for RF band pass filters with smaller size/volume, lighter weight, and higher performance for advanced mobile/wireless communication system. However, fabricated RF filters using traditional lumped element, dielectric resonators, or surface acoustic wave¡]SAW¡^filters have difficulties in on-chip integration, power handling capability, and temperature compensation. Alternatively, thin-film bulk acoustic wave resonator¡]FBAR¡^filters are very suitable devices for MMIC¡¦s since they can be fabricated on Si or GaAs substrates at a lower magnitude than lumped elements or dielectric resonators, plus they have a much lower insertion loss and higher power handling capabilities than surface acoustic wave devices and full integration with other CMOS RF IC circuitry for realizing a goal of system on chip¡]SOC¡^. In their simplest form, practical FBARs consist of a sputtered piezoelectric thin film sandwiched between top and bottom electrodes onto which an electric field is then applied. An FBAR must have two acoustically reflecting surfaces in order to trap energy and produce resonating characteristics. For this purpose, the thin film bulk acoustic resonator has to be isolated acoustically from the substrate. In view of this, in order to obtain a high Q factor and reduce spurious responses, this paper proposed the air gap type resonator using the sacrificial layer etching. The thickness of the AlN thin film used for piezoelectric thin film of Air-gap FBAR is 1um. Pt/Ti with 3000&#x00C5;/300&#x00C5; thickness is used as the top and bottom electrode. The device has a resonance frequency of 1.2GHz, and S11-paparameter of -25dB is also obtained.