Orientador: Luiz Carlos Barbosa / Tese (doutorado) - Universidade Estadual de Campinas, Instituto de Fisica Gleb Wataghin / Made available in DSpace on 2018-08-08T19:58:45Z (GMT). No. of bitstreams: 1 Osorio_SergioPauloAmaral_D.pdf: 8946065 bytes, checksum: 9771cf8636d67bee8eb1b92d030d0d13 (MD5) Previous issue date: 2007 / Resumo: Neste trabalho três tipos de vidro telurito são estudados, fabricados e caracterizados, tendo em vista a fabricação de fibras ópticas de cristal fotônico. Basicamente, dois processos de fabricação de fibras de cristal fotônico foram considerados: 1) Empilhamento e puxamento, e 2) Extrusão. Os vidros teluritos fabricados são: 0,77TeO2¿0,23WO3; 0,75TeO2¿0,20Li2O¿0,05TiO2 e 0,68TeO2¿0,155ZnO¿0,05Li2CO3¿0,015Bi2O3¿0,095CsCl (mol%), dos tipos binário, ternário e quinqüenário, respectivamente, os quais foram dopados com Er2O3. As caracterizações efetuadas foram: a) Medida do índice de refração, 2) Fotoluminescência, 3) Absorbância, 4) Tempo de vida dos íons de Érbio, 5) Análise Térmica Diferencial, 6) Análise termogravimétrica e, 7) Viscosidade. Como dito anteriormente, pode-se fabricar fibras microestruturadas de telurito por extrusão, ou pelo método de empilhamento e puxamento. A extrusora disponível no laboratório de materiais vítreos foi feita para extrudar materiais polímeros. Nossa tentativa de utilizá-la para vidros telurito não foi bem sucedida. Porém, pudemos tirar algum proveito desta experiência para futuros projetos. Os tubos de vidro telurito utilizados no método de empilhamento e puxamento foram fabricados tanto por sucção vertical do vidro fundido, quanto por rotação horizontal dos tubos em chama. No primeiro método, o diâmetro interno dos tubos de revestimento diminuiu de baixo para cima, devido ao efeito da gravidade, fazendo com que o preenchimento dos mesmos com tubos capilares fosse inadequado, ou seja, a secção transversal da fibra apresentou espaços vazios não preenchidos pelos capilares. No segundo método, o diâmetro interno dos tubos de revestimento não apresentou variação significativa ao longo de seu comprimento, possibilitando, assim, um melhor preenchimento dos mesmos por tubos capilares. Embora as fibras fabricadas com tubos feitos por rotação horizontal em chama apresentem boa geometria de secção transversal, a contaminação do vidro pela chama acarreta um aumento nas perdas de potência óptica dos modos guiados. Este efeito foi eliminado pela utilização de centrifugação em um forno radiante. Verificamos, também, que as fibras microestruturadas com somente um anel de capilares ao redor do núcleo apresentam grandes perdas por confinamento. / Abstract: In this work, three types of tellurite glasses are synthesized and characterized, aiming the manufacturing of photonic crystal fibers or microstructured fibers. Basically, two types of manufacturing processes are considered: 1) Stacking and draw, and 2) Extrusion. The tellurite glasses are: 0,77TeO 2¿0,23WO3; 0,75TeO2¿0,20Li2O¿0,05TiO2 e 0,68TeO2¿ 0,155ZnO¿0,05Li2C3¿0,015Bi2O3¿0,095CsCl (mol%), composed by two, three and five types of oxides, respectively, and Erbium oxide. The glasses were characterized by: a) index of refraction, 2) photoluminescence, 3) absorbance, 4) Erbium ions lifetime, 5) Differential Thermal Analysis, 6) Thermo gravimetric Analysis, and 7) Viscosity. The extrusion machine of the laboratory was devised for polymers. Nevertheless, we tried with telluride glass but without success. The tellurite glass tubes used for the stack and draw process were manufactured by vertical suction of the melted glass as well as by horizontal rotation of the tubes in flame. For the vertical suction method, the tellurite tube inner diameter shows a taper feature from the bottom to the top of the tube, due to the gravity effect, that makes the jacket tube unsuitable for capillary filling, that is, the fiber transversal section shows empty spaces that could not be filled with capillaries. For the second method, the telluride jacket tube inner diameter do not shows a significant variation with length, so it was possible to better fill it with the capillaries. Although the fibers made with tubes manufactured by horizontal rotation in flame shows good transversal geometry, the contamination of the glass by the flame gases brought about great losses for optical guided modes. The burner was replaced by a radiant oven. We verified, also, that micro structured fibers with only one ring of capillaries around the nucleus shows great confinement loss arising from the leaky nature of the modes / Doutorado / Física da Matéria Condensada / Doutor em Física

Made available in DSpace on 2016-03-15T19:37:29Z (GMT). No. of bitstreams: 1 Henrique Guimaraes Rosa.pdf: 986364 bytes, checksum: 89d6b316a537ef2cd3088d9200fd7183 (MD5) Previous issue date: 2010-08-06 / In this work we present a study about ultrashort pulse-train generation in Erbiumdoped fiber lasers, by the passive mode-locking technique, with the use of carbon nanotubes saturable absorbers. Carbon nanotubes were incorporated into laser cavities by two techniques: thermophoresis optically-driven deposition and thin films incorporating carbon nanotubes. The second technique has become more advantageous than the first one, because is possible to control carbon nanotubes concentration and thin films thicknesses. Additionally, we present a study about thin films incorporating carbon nanotubes optimization, in order to maximize generated output bandwidths in passively mode-locked Erbium-doped fiber lasers. We used 0.8 and 1.0 nm diameters carbon nanotubes, fabricated thin films with different transmission values (different αL product values), laser cavities with different features, such as total cavity length, total accumulated dispersion, repetition rate. In this context, best results were achieved with thin films containing 1.0 nm diameter carbon nanotubes, with films transmission about 37% (αL product close to 1.0), in 9 m long laser cavity (0.8 m of highly- Erbium-doped fiber and 8.2 m of SMF) of total accumulated dispersion of 0.153 ps/nm. The largest bandwidth measured, with those characteristics cavity parameters, was 5,7 nm. / Neste trabalho, apresentamos um estudo sobre a geração de trem de pulsos ultracurtos em lasers à fibra dopada com Érbio, utilizando a técnica de acoplamento passivo de modos com o uso de nanotubos de carbono como absorvedores saturáveis. Os nanotubos de carbono foram incorporados à cavidade laser através de duas técnicas: deposição guiada por termoforese e na forma de filmes finos contendo nanotubos de carbono, tendo a segunda técnica se mostrado mais vantajosa, pois por ela podemos ter controle sobre a concentração de nanotubos de carbono no filme e espessura do filme. Adicionalmente, apresentamos um estudo sobre a otimização da produção de filmes finos contendo nanotubos de carbono para maximização da largura de banda gerada em lasers à fibra dopada com Érbio. Utilizamos nanotubos de carbono de diâmetros de 0,8 nm e 1,0 nm, fabricamos filmes finos com transmitâncias diferentes (distintos valores para o produto αL), cavidades laser com diferentes características, tais como comprimento da cavidade, dispersão total acumulada, taxa de repetição. Neste contexto, os melhores resultados foram obtidos com filmes finos contendo nanotubos de carbono com 1,0 nm de diâmetro, em filmes cuja transmissão foi de 37% (produto αL aproximadamente 1,0), numa cavidade laser de aproximadamente 9 m de comprimento (basicamente composta de 80 cm de fibra altamente dopada com Érbio e 8,2 m de SMF), dispersão total acumulada da cavidade de aprox. 0,153 ps/nm. A maior largura de banda obtida, com estes característicos parâmetros da cavidade, foi de 5,7 nm.

Made available in DSpace on 2016-03-15T19:37:36Z (GMT). No. of bitstreams: 1 Paulo Guilherme Komninos.pdf: 1970255 bytes, checksum: df0cedf278c145259aed73c5d3775f90 (MD5) Previous issue date: 2011-02-21 / This work presents a study based on the numerical analysis of Erbium-doped fiber lasers using the technique of passive mode-locking for the laser working in pulsed regime. The equation describing the dynamics of a laser cavity is known as Ginzburg-Landau Equation, that in this work is solved numerically by the Split-Step Fourier Method. By this method, an algorithm was developed which was incorporated into the MATLAB environment so taht numerical calculations were made. The method was validated by comparing the results generated by the program (temporal pulse width due to the gain of the cavity with and without dispersion and nonlinearity) with the results published in literature. After validation of the method an experimental results were reproduced of an Erbium-doped fiber laser using thin films of carbon nanotubes as saturable absorbers. The laser generates a bandwidth of 5.7 nm for a cavity with a total length of 9 m. This experimental result was used as a calibration parameter in the initial simulations. Just by varying the length of the cavity in the simulation, results very close to the experiment were obtained. These results have helped in understanding some of the experimental variables. / Neste trabalho é apresentado um estudo baseado em análise numérica de lasers à fibra dopada com Érbio utilizando a técnica de acoplamento passivo de modos para que o mesmo opere em regime pulsado. A equação que descreve a dinâmica de uma cavidade laser é conhecida como Equação de Ginzburg-Landau, que neste trabalho é resolvida numericamente pelo Método Split-Step Fourier. Por este método, foi desenvolvido um algoritmo que foi incorporado ao ambiente MATLAB para serem feitos os cálculos numéricos. O método foi validado comparando os resultados gerados pelo programa (largura temporal do pulso devido ao ganho da cavidade com e sem dispersão e não-linearidade) com os resultados publicados na literatura. Após a validação do método, foram reproduzidos resultados experimentais de um laser a fibra dopada com Érbio usando como absorvedor saturável filmes finos de nanotubos de carbono. O laser gera uma largura de banda de 5,7 nm para uma cavidade de comprimento total de 9 m. Este resultado experimental foi utilizado como parâmetro de calibração inicial nas simulações. Apenas variando o comprimento da cavidade na simulação, foram obtidos resultados bem próximos ao do experimento. Esses resultados ajudaram na compreensão de algumas variáveis do experimento.

Made available in DSpace on 2016-03-15T19:37:45Z (GMT). No. of bitstreams: 1 Heidi Kaori Sato Pertile.pdf: 2322047 bytes, checksum: aaee9a054b94e9557394faaf3251bec9 (MD5) Previous issue date: 2013-01-24 / In this work we present a study on the generation of pulse train in an Erbium doped fiber laser in the hybrid mode-locking regime operating with short pulses at high repetition rates. The short pulses are generated by passive mode-locking technique using carbon nanotubes as saturable absorbers. High repetition rates are generated by active mode-locking technique using a phase modulator. We built cavities with three different mode-locking regimes: active, passive and, finally, hybrid, to compare results. In active and hybrid cavities we used an electro-optical modulator. In passive and hybrid cavities we used a homemade film of a polymer containing carbon nanotubes with diameter of 1 nm. With the cavity operating in the hybrid regime we obtained pulse durations of 1.77 ps with repetition rate of 10 GHz. / Neste trabalho apresentamos um estudo sobre a geração de trem de pulsos em laser à fibra dopada com Érbio operando em regime de acoplamento híbrido de modos, com pulsos curtos a altas taxas de repetição. Os pulsos curtos são obtidos pela técnica de acoplamento passivo de modos utilizando absorvedores saturáveis de carbono. As altas taxas de repetição são obtidas pela técnica de acoplamento ativo de modos através de um modulador. Construímos três cavidades distintas: ativa, passiva e finalmente a híbrida para comparação de resultados. Nas cavidades ativa e híbrida foi utilizado um modulador eletro-óptico de fase e, nas cavidades passiva e híbrida foi utilizado um filme de um polímero (NOA 73TM) contendo nanotubos de carbono com diâmetro de 1 nm por nós fabricado. Com a cavidade em regime híbrido de modos, foi obtida uma duração de pulso de 1,77 ps com uma taxa de repetição de 10 GHz.

Made available in DSpace on 2016-03-15T19:38:55Z (GMT). No. of bitstreams: 1 CLAUDIA BARROS DOS SANTOS DEMORI.pdf: 3640553 bytes, checksum: 13700107293ec12ced27c0e70d6fb334 (MD5) Previous issue date: 2015-08-25 / This work shows an Erbium doped-fiber Laser with many frequencies and many operation regimes based on integration of two paired arrayed waveguide gratings (AWGs) into a ring cavity. The AWGs are highlighted, since 2000, as key technology for multifrequencies lasers for optical communications, spectroscopy, image, astronomy and others applications. Fundamentally, gratings work splitting waveguide signal and since insertion in the cavity they allow simultaneous operating of tens of wavelength. We explore each one of these wavelength withing Erbium gain region, doing channels in different regimes of operation. These regimes may be continuous or pulsed. The advantage is that each channel may be modulated independently. Simultaneous operation with high repetition rates at 10 and 40 GHz were demonstrated, as continuous wave. The laser is stable, versatile and multifunctional. It is possible that more operating regimes, as passive mode-locking, be explored. We showed by this work efficient way to passive mode-locking by carbon nanotubes as saturable absorbers. Soon, the passive mode-locking is a potential regime for the demonstrated laser. As the new bi-dimensional materials, that look efficient for passive mode-locking and in the future, hybrid mode-locking, as graphene and black phosphor. / Esta tese trata de demonstrar um Laser de fibra dopada com Érbio com múltiplas frequências e múltiplos regimes de operação simultâneos baseados na integração de duas grades de difração pareadas (Arrayed Waveguide Gratings, AWGs) dentro de uma cavidade de laser de fibra. As AWGs são apontadas, desde o ano 2000, como tecnologia fundamental em lasers de múltiplas frequencias para as comunicações ópticas, para espectroscopia, imageamento, astronomia, e outras aplicações. Fundamentalmente, as grades funcionam como divisores do sinal óptico e quando inseridas dentro da cavidade de um laser de fibra permitem a operação simultânea de dezenas de comprimentos de onda. Neste trabalho, exploramos cada comprimento de onda, dentro da região de ganho do Érbio, com um regime de operação diferente. Esse regime pode ser pulsado ou contínuo. A vantagem do laser apresentado é que cada comprimento de onda é um canal que pode ser modulado de forma independente. Pôde-se demonstrar operação simultânea com regimes a altas taxas de repetição como 10 GHz e 40 GHz, assim como CW. O laser é estável, versátil e multifuncional. É possível que mais regimes de operação, como o regime de acoplamento de modos passivo sejam explorados. Mostramos ao longo deste trabalho maneiras eficientes de acoplar modos passivamente, utilizando nanotubos de carbono como absorvedores saturáveis, logo a técnica de acoplamento de modos passivo é um dos regimes em potencial para este laser. Assim como, o uso de novos materiais bidimensionais, que se mostram eficientes para o acoplamento de modos passivo e futuramente híbrido, como o grafeno e o fósforo negro.

The aim of this thesis is to introduce to reader the application and use of optical EDFA amplifiers in optical transmission and to show wiring and practical test, including measurements on amplifier. The aim of this thesis is to propose the use of optical amplifier in laboratory practice for subject Optical networks. The thesis briefly introduces the problems of data transmissions through optical fibers with a focus on the use of optical amplifiers. The basic characteristic of optical transmission paths and the reasons for the use of optical amplifiers are described here. One entire chapter is devoted to distinction of optical amplifiers. Amplifiers can be divided according to location in the transmission path to the booster, in-line and pre-amplifiers and according to the used of amplifying technology to optical amplifiers with subsidies, semiconductor optical amplifiers and Raman optical amplifiers. The factors affecting the efficiency of optical amplifiers, such as noise and the level of saturated power are mentioned here too. The different types of optical amplifiers from the two producers are also described. From these amplifiers was chosen EDFA CzechLight Amplifier from Optokon to be used for the laboratory exercise in the subject of Optical networks. The use of EDFA optical amplifiers in optical transmission lines is mentioned here too. These amplifiers can be used in telecommunications transmission systems and for data transmission over long distances. They will find use in WDM transmission systems and cable TV distribution through the optical fiber to the end users. Practical measurements were performed on optical amplifier CLA-PB01F. In the transmission route was located attenuator and the dependence of output power to input signal power was measured. The amplification course was linear in the range of input values provided by the manufacturer. Laboratory exercise for the subject of Optical networks is aimed at preacquaintance of students with problems EDFA optical amplifiers and practical measurements with the optical amplifier CLA-PB01F. Students acquire basic theoretical knowledge of the issue and verify the functionality of optical amplifiers on a specific exercise. This work is destined for all who wish to get basic knowledge of optical amplifiers, their characteristics and possibilities of their use in optical transmission lines.

[pt] Objetivando suprimir as instabilidades dinâmicas de ganho em um amplificador à fibra dopada com Érbio (EDFA), uma nova configuração de laser em anel é apresentada e demonstrada. Neste trabalho, analizamos os efeitos da variação do nível de atenuação no laço de re-alimentação sobre a resposta transitória do EDFA. Particularmente, observamos as excursões de ganho experimentadas pelo canal sobrevivente quando sete dentre oito canais da rede são adicionados ou removidos, à exemplo do que ocorre em sistemas WDM reais. Sob esta análise, avaliamos o desempenho do sistema em suprimir as instabilidades dinâmicas de ganho do EDFA. / [en] A new ring laser configuration to eliminate the gain dynamic instabilities of an erbium doped fiber amplifier (EDFA) is proposed and demonstrated. We examine the effect of the attenuation level in the optical feedback path over thetransient response of the EDFA. In particular, we look at the transient gain excursions experienced by surviving channel when seven of eight channels are added or dropped, like in real WDM systems. Using this analysis as a guide, we highlight the robustness of the approach and evaluate its performance to EDFA gain stabilization.

Photonics and Optical techniques have advanced recently by a great extend to play an important role in Microwave and Radar applications. Antenna array of modern active phased array radars consist of multiple low power transmit and receive mod- ules. This demands distribution of the various Local Oscillator(LO) signals for up conversion of transmit signals and down conversion of receive signals during various modes of operation of a radar system. Additionally, these receivers require control and clock signals which are digital and low frequency analog, for the synchronization between receive modules. This is normally achieved through RF cables with complex distribution networks which add significantly higher additional weight to the arrays. During radar operations, radio frequency (RF) transmit signal needs to be distributed through the same modules which will in turn get distributed to all antenna elements of the array using RF cables. This makes the system bulky and these large number of cables are prone to Electromagnetic Interference (EMI) and need additional shielding. Therefore it is very desirable to distribute a combination of these RF, analog and digital signals using a distribution network that is less complex, light in weight and immune to EMI. Advancements in Optical and Microwave photonics area have enabled carrying of higher datarate signals on a single fiber due to its higher bandwidth capability including RF signals. This is achieved by employing Wavelength Division Multi- plexing (WDM) that combine high speed channels at different wavelengths. This work proposes, characterizes and evaluates an optical Wavelength Division Multiplexed(WDM) distribution network that will overcome the above mentioned problems in a phased array radar application. The work carries out a feasibility analysis supported with experimental measurements of various physical parameters like am- plitude, delay, frequency and phase variation for various radar waveforms over WDM links. Different configurations of optical distribution network are analyzed for multipoint distribution of both digital and RF signals. These network configurations are modeled and evaluated against various parameters that include power level, loss, cost and component count. A configuration which optimizes these parameters based on the application requirements is investigated. Considerable attention is paid to choose a configuration which does not provide excess loss, which is economically viable, compact and can be realized with minimum component count. After analysing the link configuration, multiplexing density of the WDM link is considered. In this work, since the number of signals to be distributed in radar systems are small, a coarse WDM(CWDM) scheme is considered for evaluation. A comparative study is also performed between coarse and dense WDM (DWDM) links for selection of a suitable multiplexing scheme. These configurations are modeled and evaluated with power budgeting. Even though CWDM scheme does not permit the utilisation of the available bandwidth to the fullest extent, these links have the advantage of having less hardware complexity and easiness of implementation. As the application requires signal distribution to thousands of transmit-receive modules, amplifiers are necessary to compensate for the reduction of signal level due to the high splitting ratio. Introduction of commonly available optical amplifiers like Erbium Doped Fiber Amplifier (EDFA), affect the CWDM channel output powers adversely due to their non-flat gain spectrum. Unlike DWDM systems, the channel separation of CWDM systems are much larger causing significantly high channel gain differences at the EDFA output. So an analysis is carried out for the selection of a suitable wavelength for CWDM channels to minimize the EDFA output power variation. If the gain difference is still significant, separate techniques needs to be implemented to flatten the output power at the antenna end. A CWDM configuration using C-band and L-band EDFAs is proposed and is supported with a feasibility analysis. As a part of evaluation of these links for radar applications, a mathematical model of the WDM link is developed by considering both the RF and digital sig- nals. A generic CWDM system consisting of transmitters, receivers, amplifiers, multiplexers/ demultiplexers and detectors are considered for the modeling. For RF signal transmission, the transmitters with external modulators are considered. Mod- eling is done based on a bottom-top approach where individual component models are initially modeled as a function of input current/power and later cascaded to obtain the link model. These models are then extended to obtain the wavelength dependent model ( spectral response) of the hybrid signal distribution link Further mathematical analysis of the developed link model revealed its variable separable nature in terms of the input power and wavelength. This led to significant reduction in the link equation complexity and development of some approximation techniques to easily represent the link behavior. The reduced form of the link spectral model was very essential as the initially developed wavelength model had a lot of parametric dependency on the component models. This mathematical reduction process led to simplification of the spectral model into a product of two independent functions, the input current and wavelength. It is also noticed that the total link power within specific wavelength range can be obtained by the integrating these functions over a specific link input power. After the mathematical modelling, an experimental prototype physical link is set up and characterized using various radar signals like continuous wave (CW) RF, pulsed RF, non linear frequency modulated signal (NLFM) etc. Additionally a proof of concept Radio-Over-Fiber (RoF) link is established to prove the superior transmission of microwave signal through an optical link. The analysis is supported with measurements on amplitude, delay, frequency and phase variations. The NLFM waveforms transmissions are further analysed using a matched _ltering process to confirm the side lobe requirement. Further a prototype WDM link is built to study the performance when digitally modulated channels are also multiplexed into the link. The link is again validated for signal levels, delay, frequency and phase parameters. Since amplitude and delay are deterministic, it is proposed that these parameter variations can be compensated by using suitable components either in the electrical or the optical domain. Radar systems use low frequency digital signals of different duty-cycles for synchronization and control across various transmit-receive modules. In the proposed link, these digital signals also modulate a WDM channel and hence the link is called a hybrid system. As the proposed link has EDFA to compensate for the splitting losses, there are chances of transient effects at the EDFA output for these low bitrate channels. Owing to the long carrier lifetime, low bitrate digital channels are prone to EDFA transient effects under specific signal and pump power conditions. Additionally, the synchronization signals used in radar application vary the duty-cycle over time, which is found to introduce variations in transient output. This practical challenge is further studied and the thesis for the first time, includes an analysis of EDFA transient e_ects for variable duty-cycle pulsed signals. The analysis is carried out for various parameters like bitrate, input power, pump power and duty-cycle. Investigations on EDFA transients on variable duty-cycle signals help in proposing a viable method to predict the lower duty-cycle transients from higher duty-cycle transients. The predicted transients were again validated against simulated transients and experimental results. As these transient effects are not desirable for radar signals, we propose a novel transient suppression techniques in optical and electrical domain which are validated with simulation and experimental measures. One suppression technique tries to avoid transient effect by keeping the optical input to EDFA always constant by feeding an inverted version of the original pulse into the EDFA along with the actual pulse. It is observed that as the wavelength of the inverted pulse is closer to the original input pulse, the transient effect settles faster. These EDFA transients are evaluated with WDM link configurations, where both high and low bitrate signals are co-propagated. Another challenging aspect of the link operation is the non-at gain spectrum of EDFA. i.e., EDFA provides unequal power level for various signals at WDM link output. This is especially true in the case of local oscillator signals, where it is preferable to have the same amplitude signals before feeding it to the mixer stages. But in the radar applications, this will require additional hardware circuits to equalize the signal level within a phased array antenna. This work also proposes some of the power equalization methods that can be used along with the WDM links. This part of the work is also supported with simulation model and experimental results. The analytical and experimental study of this thesis aids the evaluation process of a suitable optical Wavelength Division Multiplexed(WDM) distribution network that can be used for the distribution of both RF and digital signals. The optical WDM links being superior with its light weight, less loss and EMI/ EMC immunity provides a better solution to future class of radars.

Made available in DSpace on 2016-03-15T19:38:52Z (GMT). No. of bitstreams: 1 Henrique Guimaraes Rosa.pdf: 6486656 bytes, checksum: 6fc9fe7875ed2cceb89c9f5179b9f028 (MD5) Previous issue date: 2015-02-25 / Fundo Mackenzie de Pesquisa / In this thesis, we present results on the fabrication, transfer and characterization of chemical vapor deposition (CVD) graphene and exfoliated graphene over glass and optical fiber substrates, to study optical properties of graphene and its application as a saturable absorber for Erbium-doped fiber laser (EDFL). Monolayer CVD graphene and stacked CVD graphene samples were fabricated and characterized, transferred to the transverse face of optical fibers, and a study on the relation between the optical properties of graphene samples and the properties of ultrashort laser pulses generated in (EDFL) was performed. Furthermore, we have developed a technique for transferring exfoliated nanomaterials which allowed us to transfer exfoliated graphene onto optical fiber s faces and align the graphene flake to the fiber core. With this transfer technique it is possible to fabricate samples with controlled number of graphene layers onto optical fiber faces. As application, we demonstrate ultrashort pulse generation in Erbium-doped fiber laser with exfoliated monolayer graphene samples as saturable absorber. This is the first time that ultrashort laser pulses are generated with a single exfoliated monolayer graphene sample. / Nesta tese, apresentamos resultados sobre a fabricação, transferência e caracterização de grafeno CVD (grafeno fabricado por deposição química de vapor chemical vapour deposition) e de grafeno esfoliado em substratos de vidro e em fibras ópticas, para o estudo das propriedades ópticas do grafeno e sua aplicação como absorvedor saturável em laser à fibra dopada com Érbio (EDFL). Foram fabricadas e caracterizadas amostras de grafeno CVD monocamada e de grafeno CVD empilhado, transferidas para a face transversal de fibras ópticas, e com estas amostras foram feitos estudos sobre a relação entre as propriedades ópticas do grafeno e as propriedades de pulsos ultracurtos gerados em EDFL. Além disto, desenvolvemos uma técnica para a transferência de nanomateriais esfoliados que permitiu a transferência de grafeno esfoliado para fibras ópticas e seu alinhamento com o núcleo da fibra. Com esta técnica de transferência é possível fabricar amostras com controlado número de camadas de grafeno em fibra óptica. Como aplicação, demonstramos a geração de pulsos em EDFL com uma amostra de grafeno esfoliado monocamada como absorvedor saturável. Esta é a primeira vez que pulsos ultracurtos são gerados em lasers à fibra com amostra de grafeno esfoliado de uma única camada sobre a face transversal da fibra óptica.

Chalcogenide glasses are highly nonlinear optical materials which can be used for fabricating active and passive photonic devices. This thesis work deals with the fabrication of buried, three dimensional, channel waveguides in chalcogenide glasses, using ultrafast laser inscription technique. The femtosecond laser pulses are focused into rare earth ions doped and undoped chalcogenide glasses, few hundred microns below from the surface to modify the physical properties such as refractive index, density, etc. These changes are made use in the fabrication of active and passive photonic waveguides which have applications in integrated optics. The first chapter provides an introduction to the fundamental aspects of femtosecond laser inscription, laser interaction with matter and chalcogenide glasses for photonic applications. The advantages and applications of chalcogenide glasses are also described. Motivation and overview of the present thesis work have been discussed at the end. The methods of chalcogenide glass preparation, waveguide fabrication and characterization of the glasses investigated are described in the second chapter. Also, the details of the experiments undertaken, namely, loss (passive insertion loss) and gain measurements (active) and nanoindentation studies are outlined. Chapter three presents a study on the effect of net fluence on waveguide formation. A heat diffusion model has been used to solve the waveguide cross-section. The waveguide formation in GeGaS chalcogenide glasses using the ultrafast laser, has been analyzed in the light of a finite element thermal diffusion model. The relation between the net fluence and waveguide cross section diameter has been verified using the experimentally measured properties and theoretically predicted values. Chapter four presents a study on waveguide fabrication on Er doped Chalcogenide glass. The active and passive characterization is done and the optimal waveguide fabrication parameters are given, along with gain properties for Er doped GeGaS glass. A C-band waveguide amplifier has been demonstrated on Chalcogenide glasses using ultrafast laser inscription technique. A study on the mechanical properties of the waveguide, undertaken using the nanoindentation technique, is presented in the fifth chapter. This work brings out the close relation between the change in mechanical properties such as elastic modulus and hardness of the material under the irradiation of ultrafast laser after the waveguide formation. Also, a threshold value of the modulus and hardness for characterizing the modes of the waveguide is suggested. Finally, the chapter six provides a summary of work undertaken and also discusses the future work to be carried out.