Ce travail thèse a pour objet une méthode expérimentale combinant un essai de traction indirect par écaillage et une mesure de champs à partir d’images obtenues par caméra ultra rapide, ceci à des fins d’identification des propriétés de rupture du béton sous chargement de traction dynamique. Cette méthode, proposée dans la littérature peu de temps avant le démarrage de ces travaux, fait ici l’objet d’une étude approfondi ainsi que d’une série de développements et d’amélioration. Les images obtenues sont traités par une technique de grille et la méthode des champs virtuels est appliquée pour identifier le comportement local des matériaux quasi-fragiles soumis à de hautes vitesses de déformation (plusieurs 100 1/s}). Dans un premier temps, afin de valider la technique de traitement maus aussi d’étudier l’incertitude de mesure associée, un simulateur de la chaîne de mesure complète a été mis au point. Il a été ainsi possible d’étudier l’influence de différentes sources potentielles d’erreurs qui peuvent être rencontrées dans le protocole expérimental. Cette étude a permis de retenir des recommandations sur les conditions de réalisations réelles de l’essai afin d’améliorer la fiabilité des mesures obtenues. D’un point de vue expérimental, différents capteurs ultra haute vitesse ont été utilisés afin d’étudier leur performances vis-à-vis des mesures réalisées. Ainsi, les campagnes d’essais ont été réalisées sur un matériau aux caractéristiques bien identifiées permettant l’étude des performances métrologiques de toute la chaine d’identification, pour chaque modèle de capteur. Enfin, le protocole expérimentale a été mis en place pour étudier le comportement de plusieurs types de béton soumis en traction dynamique. L’objectif, ici, est d’identifier leur comportements mécaniques ainsi que leur caractéristiques de rupture et fragmentation sous traction dynamique. En ce qui concerne la résistance à la traction, les valeurs identifiées dans cette étude sont inférieures, pour chaque cas, à celles rapportées dans la littérature et obtenues, pour la plupart, à partir du traitement de la vitesse matérielle mesurée en face arrière de l’échantillon. Pour ce qui est de l’énergie spécifique de rupture, les valeurs obtenues dans ces travaux sont égalements inférieures à celles publiées dans les revues scientifiques. / In this thesis a recently proposed photomechanical spalling experiment has been used in light of identifying concrete failure properties under dynamic tension.The experimental technique uses ultra-high speed imaging, the grid method and the virtual fields method.First, in order to investigate the accuracy and validate the processing technique, a methodology of using simulated experiments has been developed by numerically simulating the entire identification process.In this way, several potential sources of errors have been investigated allowing to place guidelines on how to perform the experiment in a more reliable manner.Second, several latest ultra-high speed acquisition systems have been used in order to investigate their contribution to a possible measurement refinement.In this case, the trial experiments have been conducted on a material of known characteristics which allowed investigating the metrological performance of the acquisition system on the entire identification chain.Finally, the experimental methodology has been applied to testing several grades of concrete in light of identifying the material constitutive response as well as their fracturing characteristics under dynamic tension.The identified tensile strengths in this work were found to be consistently lower than those obtained from the standard processing of the rear-face velocity profile.Moreover, the values of the identified specific fracture energy were also found to be markedly lower than the ones often reported in the literature.

京都大学 / 0048 / 新制・課程博士 / 博士(エネルギー科学) / 甲第22089号 / エネ博第397号 / 新制||エネ||76(附属図書館) / 京都大学大学院エネルギー科学研究科エネルギー応用科学専攻 / (主査)教授 宅田 裕彦, 教授 馬渕 守, 教授 藤本 仁 / 学位規則第4条第1項該当 / Doctor of Energy Science / Kyoto University / DFAM

This master’s thesis studies the influence of dispersed reinforcement on the behaviour of cement composites at thermal loading. In the theoretical part of the research was performed knowledge of the behaviour of concrete at high temperatures. The paper describes the on-going happening in the individual components of concrete and benefits of using dispersed reinforcement. In the practical part were designed concrete mixtures with different types and quantities of fibers. The object of the research was to determine how different types and amounts of fibers affect the physical - mechanical properties of concrete and their suitability for use in high temperatures.

<p>QC 20110523</p>

This master’s thesis work is a study of oxidation and degradation of nickel-base alloys at high temperatures. The materials studied are designed for use in critical gas turbine components such as turbine blades and vanes. Some of the alloys are used today, whereas others have not yet entered commercial application. In order to maximize the efficiency of gas turbines, there is an ambition to maximize the operating temperatures. There is therefore a demand for materials which can withstand the damage mechanisms active at high temperatures. Among these damage mechanisms are oxidation and microstructural degradation. To investigate the oxidation resistance of 7 different monocrystalline and polycrystalline alloys, samples have been exposed isothermally in still air at temperatures between 850 and 1000°C, for exposure times of up to 20000h. Two of the alloys were also exposed cyclically at 950°C. Oxidation during the heat treatment resulted in significant weight changes, which were measured after each cycle for cyclically exposed samples and after completed heat treatment for isothermally exposed samples. The weight change data was used to evaluate the relative oxidation resistance of the alloys. The ranking of the alloys with respect to oxidation resistance was generally in agreement with the oxidation resistance predicted by a simple consideration of the Cr and Al contents of the alloys. However, the single-crystal alloy PWA1483 displayed better oxidation resistance than predicted from its chemical composition. Metallographic analysis of the samples indicated that the oxide scales formed consisted of several different types of oxides. The oxide scales were mainly composed of Cr2O3 and Al2O3. Fragments of the oxide scales spalled off, primarily during cooling but also in some cases during the long-term heat treatments. Spalling of the oxide scale accelerated the oxidation process, since the ability of the oxide scale to impede diffusion decreased with its decrease in thickness. Oxidation caused depletion of Al and thereby local dissolution of the aluminum-rich γ′ particles, which are of vital importance to the mechanical properties of the material. A γ′ depleted zone thereby formed underneath the oxide scale. In this zone nitrides and needle-like particles, believed to be topologically close packed μ phase, precipitated during heat treatment. Recrystallization in the depletion zone was observed in some of the monocrystalline materials. MC carbides (M=metal) present in the virgin material decomposed during heat treatment and M23C6 carbides were formed. The γ′ particles coarsened during heat treatment, which resulted in decreased hardness. The hardness decreased with exposure temperature up to 950°C, as expected due to the increased coarsening rate. At 1000°C an unexpected increase in hardness was observed for all sample materials except one. A possible explanation for this hardness increase is redistribution of γ′, by dissolution of γ′ during heat treatment and reprecipitation during cooling as much finer particles. A fine dispersion of γ′ is expected to contribute more to the hardness than a corresponding volume of γ′ in the form of larger particles. For some of the sample series, clear correlations between hardness and γ′ particle size or exposition time were found. These relationships could potentially be used to estimate the exposure temperature of service-exposed material. A numerical model was implemented in Matlab to describe the process of oxide growth and spalling, cycle by cycle. The model was successfully adapted to experimental data from the cyclic oxidation measurements. The general applicability of the model to cyclic oxidation data at different temperatures and cycle frequencies was not investigated. At long times of cyclic exposure, the net weight loss of the samples could be well approximated as a linear function of the number of cycles. However, during the last few cycles the amount of oxide spalled in each cycle suddenly decreased. This change in spallation behavior was mainly observed for the samples cooled in air between every cycle and to a much smaller extent for the samples cooled in water. The proposed explanation is that spalling occurred preferentially at a weak subscale interface and that the spalling propensity decreased with decreasing area of this weak interface. The deviating results of the last few cycles were not included in the modeling of the cyclic oxidation process.

Rolling contacts are utilized in many technical applications, both in bearings and in the contact between gear teeth. These components are often highly loaded, which makes them susceptible to suffer from rolling contact fatigue. This work focuses on the rolling contact fatigue mechanism of pitting. In order to attain a better understanding of why pitting initiates and grows, detailed simulations of rolling contacts have been performed. In particular the contact between two gears in a truck retarder was here used as a case study. The investigated contact experienced elastohydrodynamic lubrication conditions since the load was high enough to causes the surfaces in contact to deform and the viscosity of the lubricant to increase significantly. In Paper A it was investigated if surface irregularities in the size of the surface roughness are large enough to cause surface initiated fatigue. The investigation focused on the pitch line since small surface initiated pits were found here even though there was no slip present. Since there were pits present at the pitch line, it is important that the theories of pitting can explain the development of pits also in the absence of slip. The conclusion of the work was that surface irregularities of the size of normal surface roughness are enough to cause surface initiated fatigue at the pitch line. In Paper B it was investigated why pits are more likely to initiate in the dedendum of pinion gears than in the addendum. In both areas slip is present but in different directions. In the dedendum the friction from slip is against the rolling direction which enhances the risk for pitting. The investigation was performed by studying the effect of the temperature rise in the contact caused by the slip. The conclusion drawn was that the temperature rise in the contact explained why pitting was more common in the dedendum than in the addendum. / Rullande kontakter förekommer i många applikationer, till exempel i lager och mellan kugghjulständer. Både lager och kugghjul utsätts ofta för höga laster vilket gör att dess ytor löper stor risk att utmattas, vilket kallas rullande kontaktutmattning. Denna studie fokuserar på pitting, även kallat spalling, vilket är en typ av rullande kontaktutmattning där en utmattninsspricka växer fram som får delar av ytan att ramla av. För att få en bättre förståelse varför pittingskador uppkommer har noggranna simuleringar utförts av rullande kontakter. Kontakten mellan två tänder på kugghjul i en lastbilsretarder har används som underlag då många pittingskador påträffats på dem.  För att minska friktionen och nötningen i kontakten mellan kuggtänderna användes smörjmedel. De höga lasterna lastbilsretardern utsattes för deformerade kuggarnas ytor elastiskt samtidigt de kraftigt ökade viskositeten hos smörjmedlet. Dessa förhållanden gör att kontakten kallas för elastohydrodynamiskt smord, vilket på engelska förkortas till EHL. I Artikel A undersöktes om små ytojämnheter kan orsaka ytinitierade pittingskador. Eftersom skadan påträffats i friktionslösa kontakter, så som vid rullcirkeln på de undersökta kugghjulen, är det viktigt att teorierna som förklarar uppkomsten inte är beroende av friktion. Undersökningen fokuserade därför på förhållandena vid rullcirkeln.  Slutsatsen från arbetet var att små ytojämnheter, av samma storleksordning som ytojämnheterna på de undersökta kugghjulen, är tillräckligt stora för att orsaka utmattningsskador. I Artikel B undersöktes varför det är vanligare att pitts initieras i dedendum än addendum på drivande kugghjul. Kontakten på båda sidorna om rullcirkeln slirar svagt åt olika håll. Att kontakten slirar skapar friktion som är motriktad rullriktningen i dedendum vilket ökar risken för pittingskador. För att undersöka varför dessa förhållanden ökar risken för skador fördjupades analysen av kontakten genom att inkludera temperaturfältet. Simuleringarna visade att temperaturen ökar genom kontakten vilket orsakar en asymmetrisk spänningsfördelning. Denna asymmetriska spänningsfördelning gör att ytojämnheter i dedendum är troligare att orsaka skador än ytojämnheter i addendum. / <p>QC 20180213</p>

An experimental program was conducted at the Ferguson Structural Engineering Laboratory of The University of Texas at Austin, under the auspices of Texas Department of Transportation (TxDOT) Research Project 5831, to investigate the tensile stresses that develop in the end regions of pretensioned concrete U-beams at transfer of prestress. Understanding the effect of these “bursting” and “spalling” stresses is essential in order to design standard details that might lead to reliably-serviceable end regions. Two full-scale beam specimens, designed to be worst-case scenarios for bursting and spalling, were fabricated. Each beam had one square and one highly skewed end. Extensive instrumentation, including strain gages on transverse and lateral reinforcing bars, was employed in the end regions of these U-beams. Experimentally determined bursting and spalling stresses in these bars were compared to results of past projects (from the literature) investigating I-beams and inverted T-beams. Preliminary recommendations are made for changes in the standard reinforcing details for U-beam end regions. Such recommended details will be tested in the upcoming phase of Research Project 5831. / text

The geological disposal of nuclear waste, in underground openings and the long-term performance of these openings demand a detailed understanding of fundamental rock mechanics. A full scale field experiment: Äspö Pillar Stability Experiment was conducted at a depth of 450 m in sparsely fractured granitic rock to examine the rock mass response between two deposition holes. An oval shaped tunnel was excavated parallel to the σ3 direction to provide access to the experiment and also provide elevated stress magnitudes in the floor. In the tunnel floor two 1.75-m diameter 6-m deep boreholes were excavated so that a 1-m thick pillar was created between them. In one of the holes a confinement pressure of 700 kPa was applied and in the other displacement transducers were installed. The pillar volume was monitored by an Acoustic Emission System. Spatially distributed thermocouples were used to monitor the temperature development as the pillar was heated by electrical heaters. The excavation-induced stress together with the thermal-induced stress was sufficient to cause the wall of the open borehole to yield. The temperature-induced stress was increased slowly to enable detailed studies of the rock mass yielding process. Once the rock mass loading response was observed, the rock mass was unloaded using a de-stress slotting technique. This thesis focuses on the in-situ study of the rock mass response to coupled mechanical thermal loading and thermal-mechanical unloading. The experiment, its design, monitoring and observations are thoroughly described. An estimate of the yielding strength of the rock mass is presented and compared with laboratory test and results from other rock mass conditions reported elsewhere in the open literature. General conclusions about the effect of the confining pressure and the observations from the unloading of the pillar are also presented. Important findings are that the yielding strength of the rock mass has been successfully determined, low confinement pressures significantly affects the onset of yielding, the primary mode of fracture initiation and propagation is extensional, no significant time dependency of the yielding process was observed. The unloading studies also indicated that what appeared to be shear bands likely was a propagating zone of extensile failure that weakened the rock so that displacements in the shear direction could occur. / <p>QC 20100622</p>

Dans les dernières années, les incendies majeurs dans les tunnels ont causé des dommages importants. Dans ces conditions extrêmes (la température dépasse rapidement 1200 °C), l'augmentation de pression dans les pores, la dilatation thermique empêchée, l'incompatibilité de dilatation thermique entre la pâte du ciment et des granulats, la déshydratation ... sont des principaux mécanismes de dégradation qui peuvent être à l'origine de l'écaillage. L'écaillage progressif pendant l'incendie se manifeste par le détachement de la surface du béton par petits morceaux réduisant ainsi la section résistante et pouvant conduire à une rupture prématurée de la structure. Dans cette thèse, un modèle éléments finis THM est enrichi par un modèle d'écaillage progressif en proposant un critère d'écaillage de type détachement-flambement. La partie thermo-hydrique du modèle THM est basée sur l'approche à trois fluides en milieux partiellement saturés. Le comportement mécanique est développé dans le cadre d'une approche thermo-poro-mécanique couplée à l'endommagement et à la plasticité adoucissante. Cette modélisation de l'écaillage conduit à un problème avec frontière et conditions aux limites évolutives. Une stratégie de résolution numérique sans remaillage a été développée pour transférer les conditions aux limites THM simultanément avec l'occurrence de l'écaillage. L'implémentation du modèle dans le code aux éléments finis CESAR-LCPC a permis de procéder à différentes études paramétriques et à des confrontations avec des essais pour évaluer les capacités opérationnelles du modèle à décrire l'occurrence de l'écaillage et identifier les paramètres majeurs qui la contrôlent / In the recent years, there were major tunnels fires which caused fatalities and severe traffic restrictions. In such extreme conditions (temperatures exceeding 1200 °C for considerable time spans), pore pressure build-up, restrained thermal dilatation, cement paste to aggregate incompatibility, dehydration... are some main degradation mechanisms of concrete that may cause its thermal spalling. Progressive concrete spalling occurring during a fire presents as the breakdown of surface layers which flake into small pebble-like pieces. Then, the resistant section of the structure reduces which may lead to its premature failure.In this thesis, a THM finite element model is enriched with a detachment-buckling type criterion for progressive spalling. The thermo-hygral part of the THM model is based on the three fluid approach for partially saturated porous media. The mechanical part is derived within the framework of thermo-poro-mechanics coupled to damage and softening plasticity.The adopted modeling of spalling leads to a problem with evolving boundary and boundary conditions. A suitable numerical solution strategy without remeshing is then developed in order to transfer properly the THM boundary conditions simultaneously with spalling occurrence.The efficiency of the model THM-Spalling is illustrated by some numerical examples and by parametric studies. These studies identify the influence, on spalling, of size variation of spalling flakes, the average spalling velocity and uncertainties on different material parameters. Confrontation with experimental tests shows satisfactory capacity of the THM-Spalling model in reproducing qualitatively the occurrence of spalling

Esta pesquisa foi motivada pela existência de controvérsia na literatura sobre concreto exposto a altas temperaturas, das dúvidas ainda por solucionar acerca da matéria e da lacuna na norma brasileira para a matéria. Este tema reapareceu após os vários acidentes em túneis ao redor do mundo ocorridos nos últimos dez anos, nos quais se verificou a ocorrência de lascamento explosivo de forma intensa, afetando a estabilidade estrutural. O objetivo principal da tese é correlacionar os parâmetros tecnológicos de dosagem (relação água/cimento, teor de argamassa e consumo total de água) às condições de risco de lascamento, associados à umidade ambiente, que indiretamente, influencia no grau de saturação do concreto. O segundo objetivo é otimizar o uso de fibras de polipropileno para minimizar o efeito do lascamento. Adotou-se empregar a curva-padrão H durante 55 minutos em corpos-de-prova cúbicos aquecidos apenas em uma das fases com sua dilatação térmica lateral restringida. O nível de lascamento foi avaliado usando o volume lascado, obtido pela espessura medida diretamente nos corpos-de-prova, multiplicada pela área lascada, calculada pelo AUTOCAD 2000. Os resultados mostraram que o parâmetro tecnológico mais relevante na ocorrência de lascamento foi a relação água/cimento e a umidade ambiente apresentou capacidade de alterar as condições de risco de lascamento. No estudo com as fibras percebeu-se diferentes teores de fibras e diferentes características das fibras para cada grupo de a/c. Conclui-se que a relação água/cimento mais baixa associada a umidade a ambiente mais elevada é a condição mais propícia a ocorrência de lascamento. Conclui-se também que o teor de fibras de 600g/m³ é o teor mínimo para se reduzir o lascamento no grupo a/c=0,50 e 1750g/m³ no grupo a/c=0,25. A fibra L=12mm F=36µm PF=140°C mostrou-se a mais eficaz no grupo a/c=0,50 apenas o comprimento L=6 mm mostrou-se eficiente na redução do lascamento. / The present research was motivated by the going controversy in the literature about concrete exposed to high temperatures, the yet unanswered doubts existent on this subject and in the absence of regulation on the matter in Brazil. The theme gained significance after the occurrence of several accidents in tunnels all over the world in the last ten years, in which were observed a very intense form of explosive spalling that affected structural stability of the sites. The main purpose of this work is set up a correlation between technological parameters of dosage in concrete (water cement rate -w/c, mortar content - a, and total water consumption - H) and risk conditions of spalling, which are related to environment humidity that indirectly effects concrete saturation level. The second goal is to optimize the use of polypropylene fiber in order to minimize spalling. The standard H curve was applied during 55 minutes in cubic samples with only a single surface exposed to heat and with restrained lateral thermo dilatation. The response variable was the observed volume of spalling (with multiplied by area of spalling in the sample). The results showed the rate water/cement as the most relevant technology parameter related to spalling risk conditions. Whereas the use of fiber is concerned, efficiency required different fiber content and characteristic for each water/cement rate combined with higher environment humidity provides proper conditions for the occurrence of spalling were 600g/m³ and 1750g/m³ for water/cement ratios of 0,5 and 0,25 respectively. It was also found that the fiber with L=12mm, F=36µm PF=140°C was the most effective in reducing spalling for a water/cement ratio of 0,50 whilst for a effective in reducing spalling for a water/cement ratio of 0,50 whilst for a water/cement ratio of 0,50 whilst for a water/cement ratio 0,25 only the length (L=6 mm) appeared as a significant factor.