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Land surfaces have changed as a result of human and natural processes, such asdeforestation, urbanization, desertification and natural disasters like wildfires. Land use and landcover change impacts local and regional climates through various bio geophysical processes acrossmany time scales. More realistic representation of land surface parameters within the land surfacemodels are essential to for climate models to accurately simulate the effects of past, current andfuture land surface processes. In this study, we evaluated the sensitivity and accuracy of theWeather Research and Forecasting (WRF) model though the default MODIS land cover data andannually updated land cover data over southeast of United States. Findings of this study indicatedthat the land surface fluxes, and moisture simulations are more sensitive to the surfacecharacteristics over the southeast US. Consequently, we evaluated the WRF temperature andprecipitation simulations with more accurate observations of land surface parameters over thestudy area. We evaluate the model performance for the default and updated land cover simulationsagainst observational datasets. Results of the study showed that updating land cover resulted insubstantial variations in surface heat fluxes and moisture balances. Despite updated land use andland cover data provided more representative land surface characteristics, the WRF simulated 2- m temperature and precipitation did not improved due to use of updated land cover data. Further,we conducted machine learning experiments to post-process the Noah-MP land surface modelsimulations to determine if post processing the model outputs can improve the land surfaceparameters. The results indicate that the Noah-MP simulations using machine learning remarkablyimproved simulation accuracy and gradient boosting, and random forest model had smaller meanerror bias values and larger coefficient of determination over the majority of stations. Moreover,the findings of the current study showed that the accuracy of surface heat flux simulations byNoah-MP are influenced by land cover and vegetation type.

This research investigates soil respiration (Rs) in a boreal jack pine (Pinus banksiana Lamb.) fire scar chronosequence at Sharpsand Creek, Ontario, Canada. During two field campaigns in 2006 and 2007, Rs was measured in a chronosequence of fire scars in the range 0 to 59 years since fire. Mean Rs adjusted for soil temperature (Ts) and soil moisture (Ms) (Rs T,M) ranged from 0.56 μmol CO2/m2/s (32 years post fire) to 8.18 μmol CO2/m2/s (58 years post fire). Coefficient of variation (CV) of Rs adjusted for Ts and Ms ranged from 20% (16 years post fire) to 56% (58 years post fire). Across the field site, there was a significant exponential relationship between Rs adjusted for soil organic carbon (Cs) and Ts (P = 1.24*10-06; Q10 = 2.21) but no effect of Ms on Rs adjusted for Cs and Ts for the range 0.21 to 0.77 volumetric Ms (P = 0.702). Rs T,M significantly (P = 0.030) decreased after burning mature forest, though no significant (P > 0.1) difference could be detected between recently burned and unburned young forest. Rs was measured in recently burned boreal jack pine fire scar age categories that differed in their burn history and there was a significant difference in Rs T,M between previously 32 v 16 year old (P = 0.000) and previously 32 v 59 year old (P = 0.044) scars. There was a strong significant exponential increase in S R T,M with time since fire (r2 = 0.999; P = 0.006) for the chronosequence 0, 16 and 59 years post fire, and for all these age categories, Rs T,M was significantly different from one another (P < 0.05). The Joint UK Land Environment Simulator (JULES) was used to model vegetation re-growth over successional time at Sharpsand Creek, though it appeared to perform poorly in simulating leaf area index and canopy height. JULES probably over estimated heterotrophic Rs at Sharpsand Creek when Ts corrected simulated values were compared with measured Rs T,M. The results of this study contribute to a better quantitative understanding of Rs in boreal jack pine fire scars and will facilitate improvements in C cycle modelling. Further work is needed in quantifying autotrophic and heterotrophic contributions to soil respiration in jack pine systems, monitoring soil respiration for extended time periods after fire and improving the ability of JULES to simulate successional vegetation re-growth.

Modelling solar radiation data at a high spatiotemporal resolution for an urban environment can inform many different applications related to climate action, such as urban agriculture, forest, building, and renewable energy studies. However, the complexity of urban form, vastness of city-wide coverage, and general dearth of climatological information pose unique challenges doing so. To address some climate action goals related to reducing building emissions in the City of Victoria, British Columbia, Canada, applied geomatics and climatology were used to model solar radiation data suitable for informing renewable energy feasibility studies, including photovoltaic system sizing, costing, carbon offsets, and financial payback. The research presents a comprehensive review of solar radiation attenuates, as well as methods of accounting for them, specifically in urban environments. A novel methodology is derived from the review and integrates existing models, data, and tools – those typically available to a local government. Using Light Detection and Ranging (LiDAR), a solar climatology, Esri’s ArcGIS Solar Analyst tool, and Python scripting, daily insolation (kWh/m2) maps are produced for the city of Victoria. Particular attention is paid to the derivation of daily diffuse fraction from atmospheric clearness indices, as well as LiDAR classification and generation of a Digital Surface Model (DSM). Novel and significant improvements in computation time are realized through parallel processing. Model results exhibit strong correlation with empirical data and support the use of Solar Analyst for urban solar assessments when great care is taken to accurately and consistently represent model inputs and outputs integrated in a methodological approach. / Graduate

Liquid chromatography (LC) coupled to mass spectrometry (MS) offers highly selective and sensitive analysis of a wide variety of compounds. However, the use of hyphenated experimental set-ups implies that many parameters may have an effect on the studied response. Therefore, in order to determine optimized experimental conditions it is of vital importance to incorporate systematic procedures during method development. In this thesis, a generic stepwise optimization strategy is proposed that aims at high chromatographic quality, as well as high mass spectrometric response. The procedure comprises (i) screening experiments to identify the most important parameters, (ii) LC studies to ensure sufficient chromatographic separation, (iii) extended infusion experiments in order to maximize precursor signal(s), and in the case of tandem MS (iv) extended infusion experiments to determine optimal conditions for collision induced dissociation and when applicable also ion trap settings. Experimental design and response surface methodology is used throughout the procedure. Further, the general applicability of LC-MS is demonstrated in this thesis. Specifically, a novel quantitative column-switched LC-MS method for ferrichrome, ferrichrysin and ferricrocin determination is presented. Using the method it was shown how the siderophore content varies with depth in podzolic soil profiles in the north and south of Sweden. The parallel approach using LC coupled to both inductively coupled plasma (ICP) mass spectrometry, and electrospray ionization (ESI) tandem MS is also evaluated as a tool to identify unknown siderophores in a sample. Additionally, different trypsin digestion schemes used for LC-ESI-MS peptide mapping were compared. By multivariate data analysis, it was clearly shown that the procedures tested induce differences that are detectable using LC-ESI-MS. Finally, the glutathione S-transferase catalyzed bioactivation of the prodrug azathioprine was verified using LC-MS.

This thesis addresses the problem of constructing 3D CAD models from 2D engineering drawings of the object. Procedures for each step in the popular bottom-up approach are described. In each of the steps in this approach, the capability is extended to handle classes of parts not handled by present art. These include auxiliary views, parts with curved entities that are inclined to all viewing directions, and views that result in non-manifold edges in the surface model. In addition this thesis also presents procedures to extract features from the solid model constructed so that the 3D model can be manipulated and modified within current CAD systems. In order to enable extracting the construction history, detecting symmetry in the part is essential. This thesis presents an algorithm to detect symmetry (both global and partial) in the part given the solid model of the part. Working of the procedures is illustrated using benchmark parts from the literature. The thesis concludes with a discussion on scope for further work.

點雲（point cloud）為以大量三維坐標描述地表實際情形的資料形式，其中包含其三維坐標及相關屬性。通常點雲資料取得方式為光達測量，其以單一波段雷射光束掃描獲取資料，以光達獲取點雲，常面臨掃描時間差、缺乏多波段資訊、可靠邊緣線及角點資訊、大量離散點雲又缺乏語意資訊（semantic information）難以直接判讀及缺乏多餘觀測量等問題。 攝影測量藉由感測反射自太陽光或地物本身放射之能量，可記錄為二維多光譜影像，透過地物在不同光譜範圍表現之特性，可輔助分類，改善分類成果。若匹配多張高重疊率的多波段影像，可以獲取包含多波段資訊且位於明顯特徵點上的點雲，提供光達以外的點雲資料來源。 傳統空中三角測量平差解算地物點坐標及產製數值表面模型（Digital Surface Model, DSM）時，多採用可見光影像為主；而目前常見之高空間解析度數值航照影像，除了記錄可見光波段之外，亦可蒐集近紅外光波段影像。但較少採用近紅外光波段影像，以求解地物點坐標及建立DSM。 因此本研究利用多波段影像所蘊含的豐富光譜資訊，以取像方式簡易及低限制條件的近景攝影測量方式，匹配多張可見光、近紅外光及紅外彩色影像，分別建立可見光、近紅外光及紅外彩色之DSM，其目的在於探討加入近紅外光波段後，所產生的近紅外光及紅外彩色DSM，和可見光DSM之異同；並比較該DSM是否更能突顯植被區。 研究顯示，以可見光點雲為檢核資料，計算近紅外光與紅外彩色點雲的均方根誤差為其距離門檻值之相對檢核方法，可獲得約21%的點雲增加率；然而使用近紅外光或紅外彩色影像，即使能增加點雲資料量，但對於增加可見光影像未能匹配的資料方面，其效果仍屬有限。 / Point cloud represents the surface as mass 3D coordinates and attributes. Generally, these data are usually collected by LIDAR (LIght Detection And Ranging), which acquires data through single band laser scanning. But the data collected by LIDAR could face problems, such as scanning process is not instantaneous, lack of multispectral information, breaklines, corners, semantic information and redundancies. However, photogrammetry record the electromagnetic energy reflected or emitted from the surface as 2D multispectral images, via ground features with different characteristics differ in spectrum, it can be classified more efficiently and precisely. By matching multiple high overlapping multispectral images, point cloud including multispectral information and locating on obvious feature points can be acquired. This provides another point cloud source aparting from LIDAR. In most studies, visible light (VIS) images are used primarily, while calculating ground point coordinates and generating digital surface models （DSM） through aerotriangulation. Although nowadays, high spatial resolution digital aerial images can acquire not only VIS channel, but also near infrared (NIR) channel as well. But there is lack of research doing the former procedures by using NIR images. Therefore, this research focuses on the rich spectral information in multispectral images, by using easy image collection and low restriction close range photogrammetry method. It matches several VIS, NIR and color infrared (CIR) images, and generate DSMs respectively. The purpose is to analyze the difference between VIS, NIR and CIR data sets, and whether it can emphasize the vegetation area, after adding NIR channel in DSM generation. The result shows that by using relative check points between NIR, CIR data with VIS one. First, VIS point cloud was set as check point data, then, the RMSE (Root Mean Square Error) of NIR and CIR point cloud was calculated as distance threshold. Its data increment is 21% ca. However, the point cloud data amount can be increased, by matching NIR and CIR images. But the effect of increasing data, which was not being matched from VIS images are limited.

Model-H is used to describe structures found in the phase separation in films of binary liquid mixture that have a surface that is free to deform and also may energetically prefer one of the components. The film rests on a solid smooth substrate that has no preference for any component. On the one hand the study focuses on static aspects by investigating steady states that are characterised by their concentration and film height profiles. A large variety of such states are systematically analysed by numerically constructing bifurcation diagrams in dependence of a number of control parameters. The numerical method used is based on minimising the free energy functional at given constraints within a finite element method for a variable domain shape. The structure of the bifurcation diagrams is related to the symmetry properties of the individual solutions on the various branches. On the other hand the full time dependent model-H is linearised about selected steady states, in particular, the laterally invariant, i.e.\ layered states. The resulting dispersion relations are discussed and related to the corresponding bifurcation points of the steady states. In general, the results do well agree and confirm each other. The described analysis is performed for a number of important cases whose comparison allows us to gain an advanced understanding of the system behaviour: We distinguish the critical and off-critical case that correspond to zero and non-zero mean concentration, respectively. In the critical case the investigation focuses on (i) flat films without surface bias, (ii) flat films with surface bias, (iii) height-modulated films without surface bias, and (iv) height-modulated films with surface bias. Each case is analysed for several mean film heights and (if applicable) energetic bias at the free surface using the lateral domain size as main control parameter. Linear stability analyses of layered films and symmetry considerations are used to understand the structures of the determined bifurcation diagrams. For off-critical mixtures our study is more restricted. There we consider height-modulated films without and with surface bias for several mean film heights and (if applicable) energetic bias employing the mean concentration as main control parameter.

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Submitted by Luciana Ferreira (lucgeral@gmail.com) on 2016-12-27T11:27:00Z No. of bitstreams: 2 Dissertação - Avilmar Antonio Rodrigues - 2016.pdf: 13580117 bytes, checksum: 2b78a395b4bd955f8d72e83399bcc578 (MD5) license_rdf: 0 bytes, checksum: d41d8cd98f00b204e9800998ecf8427e (MD5) / Approved for entry into archive by Luciana Ferreira (lucgeral@gmail.com) on 2016-12-27T11:27:20Z (GMT) No. of bitstreams: 2 Dissertação - Avilmar Antonio Rodrigues - 2016.pdf: 13580117 bytes, checksum: 2b78a395b4bd955f8d72e83399bcc578 (MD5) license_rdf: 0 bytes, checksum: d41d8cd98f00b204e9800998ecf8427e (MD5) / Made available in DSpace on 2016-12-27T11:27:20Z (GMT). No. of bitstreams: 2 Dissertação - Avilmar Antonio Rodrigues - 2016.pdf: 13580117 bytes, checksum: 2b78a395b4bd955f8d72e83399bcc578 (MD5) license_rdf: 0 bytes, checksum: d41d8cd98f00b204e9800998ecf8427e (MD5) Previous issue date: 2016-11-25 / This research aimed to evaluate the use of Unmanned Aerial Vehicle (UAV) as a platform for taking aerial photographs for mapping erosion planialtimetric located in urban areas. In addition, we evaluated the need to use or not to field control points for the generation of Digital Surface Model (DSM) and ortomosaico as tools to evaluate the erosive process. Despite the wide variation in attitude of aerial photographs that make up the aerophotogrammetric block arising from the instability of the UAV, it was possible to generate the MDS and ortomosaico with or without control points. This research was conducted in two urban erosions located in Goiania in Sector Fonte Nova in the stream of grass and the other in Silvânia called foot-washing. Whole generation of MDS, Digital Surface Model (MDT) and ortomosaico were performed in Agisoft PhotoScan program in semi-automatic processing, if used control points, or automatic without control points. The ortomosaicos generated without control points presented rotation, translation and scale of different generated with support. In addition, MDS generated without control points showed elevation or lowering of the reference surface with respect to the generated control, it is emphasized that these discrepancies are not constant. When performing automatic conversion of MDS to MDT, it was realized that the program was not able to eliminate the shrub vegetation located within the erosion. The vegetation or tree, shrub or undergrowth (grass) prevents proper limitation of erosion to the volume calculation. But unlike the MDS generated between two distinct epochs identifies the changes in the interval of time in areas without vegetation. The use of control points was essential to ensure the orientation, scale and the reference plane in the products generated from aerial photographs and thus evaluate the changes. Anyway, the UAV can be used as a platform for taking aerial photographs for generating cartographic products that enable the mapping and evaluation of erosions. / Esta pesquisa teve por objetivo avaliar a utilização do Veículo Aéreo Não Tripulado (VANT) como plataforma para a tomada de fotografias aéreas para o mapeamento planialtimétrico de erosão situada em zona urbana. Além disso, analisou-se a necessidade de utilização ou não de pontos de controle de campo para a geração de Modelo Digital de Superfície (MDS) e ortomosaico como instrumentos para examinar o processo erosivo. Apesar da grande variação da atitude da aeronave durante a obtenção das fotografias aéreas que compõem o bloco aerofotogramétrico, foi possível gerar o MDS e o ortomosaico com ou sem pontos de controle. Este estudo foi realizado em duas erosões urbanas, uma situada em Goiânia-GO, no Setor Fonte Nova/Córrego do Capim, e a outra em Silvânia-GO, denominada de Lava-Pés. Toda a geração dos MDS, Modelo Digital de Terreno (MDT) e ortomosaico foram realizados no programa Agisoft PhotoScan, em processamento semiautomático (i.e., com pontos de controle) e automático (i.e., sem pontos de controle). Os ortomosaicos gerados sem pontos de controle apresentaram rotação, translação e escala diferente dos gerados com apoio. Ademais, os MDS gerados sem pontos de controle apresentaram elevação ou rebaixamento da superfície de referência em relação aos gerados com controle. Ressalta-se, ainda, que essas discrepâncias não foram constantes. Ao realizar a conversão automática do MDS para o MDT, percebeu-se que o programa não foi capaz de eliminar a vegetação arbustiva localizada no interior da erosão. As vegetações arbórea, arbustiva ou rasteira (gramíneas) impedem a correta delimitação da erosão para o cálculo do volume. Porém, a diferença dos MDS gerados entre duas épocas distintas propicia identificar as alterações ocorridas nesse intervalo de tempo nas regiões sem cobertura vegetal. O uso de pontos de controle foi essencial para garantir a orientação, a escala e o plano de referência nos produtos gerados a partir das fotografias aéreas e, assim, avaliar as modificações da erosão. Por fim, o VANT pode ser utilizado como plataforma para a tomada de fotografias aéreas para gerar produtos cartográficos que possibilitem o mapeamento e as avaliações das erosões, sobretudo em áreas urbanas.