Cette thèse présente la conception, la caractérisation et l'utilisation d'un microsystème intégrant des fonctions terahertz (THz) guidées. L'interprétation des mesures conduit à la définition d'une métrologie des liquides aux fréquences THz. Ceci est possible par le développement de systèmes robustes, versatiles et sensibles couplant circuits microfluidiques et guides d'ondes THz intégrés. La création d'un procédé technologique compatible avec les processus microélectroniques de fabrication en "salle blanche", et le choix d'une filière silicium/polymère/verre ont permis d'obtenir une résistance à des pressions de plus de 35bar dans des canaux de 50mm de large. De plus, l'assemblage des substrats en amont de la gravure des canaux permet une conception indépendante des circuits électromagnétique et fluidique avec une définition de motifs inégalée pour ce type de microsystèmes. Les mesures réalisées avec ce dispositif ont permis d'atteindre une sensibilité aux protéines de l'ordre de 5mg/mL, état de l'art des dispositifs THz conventionnels, améliorant notablement les performances des dispositifs microfluidiques THz. Cette sensibilité a permis la caractérisation de l'hydratation de protéines en solution. Les calibrations in-situ, assurant l'obtention de mesures quantitatives, permettent d'atteindre leur nombre d'hydratation. Le couplage des mesures avec des techniques de chimiométrie conduit à l'analyse plus fondamentale de la structure et la dynamique de la couche d'hydratation, confrontée avec succès à des modèles numériques. Nous aboutissons à la définition d'un laboratoire sur puce, couplant modélisation, mesures calibrées et interprétation statistique dans le spectre THz, qui par ses caractéristiques propres, contribue à la compréhension des phénomènes d'hydratation. Le véritable apport de cette technologie réside dans ses perspectives pour le suivi des interactions dynamiques nécessaire à une meilleure compréhension du vivant.

The purpose of this study is to investigate the dielectric properties of fuel oils and their ethanol mixtures in the THz spectral region. We presented frequency dependent absorption coefficients, refractive indices, and dielectric constants calculated from the measurements of pure and mixtures of fuel oils. As the mixing ratio changes, meaningful shifts were observed in refractive index and absorption coefficient of the mixtures. For pure liquids, we used Debye model which provides a good estimate for the dielectric parameters of pure liquids in microwave region and also in the THz region. Bruggeman model, which is used for describing the interaction between liquids in binary mixtures, did not work for ethanol mixtures of gasoline within our assumptions. However, these mixtures were modeled successfully with a modified Debye model in which the mixture behavior was described with a basic contribution approach. The results suggest that there is no strong interaction between the ethanol and the molecules in the gasoline. We concluded that this new approach offers a simple and useful method to determine the concentration of ethanol in gasoline with 3% (by volume) maximum error.

A terahertz photoconductive source structure with nano-grating electrodes is proposed. The resonance modes of the one-dimensional nano-grating and their affect the optical power absorption are studied. In addition, an approach for optimal design of the grating to maximize the photocurrent for different proposed DC biases, is presented. The dependence of the photocurrent on physical parameters of photomixer are analyzed. A fast analysis method for a new terahertz waveguide for photo-mixing is proposed. The wave-guiding mixer structure is a modified parallel plate waveguide (PPWG) in which the top plate is replaced by a periodic array of sub-wavelength nano-slits. The substrate of the PPWG is made of a fast photoconductive material in which laser photomixing/absorption occurs. The characteristic equation of the modified PPWG when used as a THz waveguide is derived analytically, and its guided modes are studied in details over THz range of frequencies. The accuracy of the analytical results are verified by comparison with full-wave numerical simulations. The criteria for choosing the suitable mode for photomixing application are also discussed. Finally, based on dyadic Green’s function representation, a systematic approach is provided for calculating the amplitude of the guided modes that are excited by an arbitrary photocurrent.

The Photonic Crystal (PC) is a potential candidate for a compact optical integrated circuit on a solid state platform. The fabrication process of a PC is compatible with CMOS technology; thus, it could be potentially employed in hybrid optical and electrical integrated circuits. One of the main obstacles in the implementation of an integrated optical circuit is the polarization dependence of wave propagation. Our goal is to overcome this obstacle by implementing PC based polarization controlling devices. One of the crucial elements of polarization controlling devices is the polarization rotator. The polarization rotator is utilized to manipulate and rotate the polarization of light. In this thesis, we have proposed, designed and implemented an ultra-compact passive PC based polarization rotator. Passive polarization rotator structures are mostly composed of geometrically asymmetric structures. The polarization rotator structure consists of a single defect line PC slab waveguide. The geometrical asymmetry has been introduced on top of the defect line as an asymmetric loaded layer. The top loaded layer is asymmetric with respect to the z-axis propagation direction. To synchronize the power conversion and avoid power conversion reversal, the top loaded layer is alternated around the z-axis periodically. The structure is called periodic asymmetric loaded PC slab waveguide. Due to the compactness of the proposed structure, a rigorous numerical method, 3D-FDTD can be employed to analyze and simulate the final designed structure. For the quick preliminary design, an analytical method that provides good approximate values of the structural parameters is preferred. Coupled-mode theory is a robust and well-known method for such analyses of perturbed waveguide structures. Thus, a coupled-mode theory based on semi-vectorial modes was developed for propagation modeling on square hole PC structures. In essence, we wish to develop a simple yet closed form method to carry out the initial design of the device of interest. In the next step, we refined the design by using rigorous but numerically expensive 3D-FDTD simulations. We believe this approach leads to optimization of the device parameters easily, if desired. To extend the design to a more general shape PC based polarization rotator, a design methodology based on hybrid modes of asymmetric loaded PC slab waveguide was introduced. The hybrid modes of the structure were calculated utilizing the 3D-FDTD method combined with the Spatial Fourier Transform (SFT). The propagation constants and profile of the slow and fast modes of an asymmetric loaded PC slab waveguide were extracted from the 3D-FDTD simulation results. The half-beat length, which is the length of each loaded layer, and total number of the loaded layers are calculated using the aforementioned data. This method provides the exact values of the polarization rotator structure’s parameter. The square hole PC based polarization rotator was designed employing both coupled-mode theory and normal modal analysis for THz frequency applications. Both design methods led to the same results. The design was verified by the 3D-FDTD simulation of the polarization rotator structure. For a square hole PC polarization rotator, a polarization conversion efficiency higher than 90% over the propagation distance of 12 λ was achieved within the frequency band of 586.4-604.5 GHz corresponding to the normalized frequency of 0.258-0.267. The design was extended to a circular hole PC based polarization rotator. A polarization conversion efficiency higher than 75% was achieved within the frequency band of 600-604.5 GHz. The circular hole PC polarization rotator is more compact than the square-hole PC structure. On the other hand, the circular hole PC polarization rotator is narrow band in comparison with the square hole PC polarization rotator. In a circular hole PC slab structure, the Bloch modes (fast and slow modes) couple energy to the TM-like PC slab modes. In both square and circular hole PC slab structures with finite number of rows, and the TM-like PC slab modes are extended to the lower edge of the bandgap. In bandgap calculation using PWEM, it is assumed that the PC structure is extended to infinity, however in practice the number of rows is limited, which is the source of discrepancy between the bandgap calculation using PWEM and 3D-FDTD. In an asymmetric loaded circular hole PC slab waveguide, the leaky TM-like PC slab modes are extended deep inside the bandgap and overlapped with both the slow and fast Bloch modes; whereas, in an asymmetric loaded square hole PC slab waveguide, the leaky TM-like PC slab modes are below the frequency band of slow and fast modes. Therefore, TM-like PC slab modes have significantly more adverse effect on the performance of the circular-hole based polarization rotator leading to a narrow band structure. SOI based PC membrane technology for THz application was developed. The device layer is made of highly resistive silicon to maintain low loss propagation for THz wave. The PC slab waveguide and polarization rotators were fabricated employing this technology. Finally, an a-SiON PC slab waveguide structures were also fabricated at low temperature for optical applications. This technology has the potential to be implemented on any substrate or CMOS chips.

No description available.

The Photonic Crystal (PC) is a potential candidate for a compact optical integrated circuit on a solid state platform. The fabrication process of a PC is compatible with CMOS technology; thus, it could be potentially employed in hybrid optical and electrical integrated circuits. One of the main obstacles in the implementation of an integrated optical circuit is the polarization dependence of wave propagation. Our goal is to overcome this obstacle by implementing PC based polarization controlling devices. One of the crucial elements of polarization controlling devices is the polarization rotator. The polarization rotator is utilized to manipulate and rotate the polarization of light. In this thesis, we have proposed, designed and implemented an ultra-compact passive PC based polarization rotator. Passive polarization rotator structures are mostly composed of geometrically asymmetric structures. The polarization rotator structure consists of a single defect line PC slab waveguide. The geometrical asymmetry has been introduced on top of the defect line as an asymmetric loaded layer. The top loaded layer is asymmetric with respect to the z-axis propagation direction. To synchronize the power conversion and avoid power conversion reversal, the top loaded layer is alternated around the z-axis periodically. The structure is called periodic asymmetric loaded PC slab waveguide. Due to the compactness of the proposed structure, a rigorous numerical method, 3D-FDTD can be employed to analyze and simulate the final designed structure. For the quick preliminary design, an analytical method that provides good approximate values of the structural parameters is preferred. Coupled-mode theory is a robust and well-known method for such analyses of perturbed waveguide structures. Thus, a coupled-mode theory based on semi-vectorial modes was developed for propagation modeling on square hole PC structures. In essence, we wish to develop a simple yet closed form method to carry out the initial design of the device of interest. In the next step, we refined the design by using rigorous but numerically expensive 3D-FDTD simulations. We believe this approach leads to optimization of the device parameters easily, if desired. To extend the design to a more general shape PC based polarization rotator, a design methodology based on hybrid modes of asymmetric loaded PC slab waveguide was introduced. The hybrid modes of the structure were calculated utilizing the 3D-FDTD method combined with the Spatial Fourier Transform (SFT). The propagation constants and profile of the slow and fast modes of an asymmetric loaded PC slab waveguide were extracted from the 3D-FDTD simulation results. The half-beat length, which is the length of each loaded layer, and total number of the loaded layers are calculated using the aforementioned data. This method provides the exact values of the polarization rotator structure’s parameter. The square hole PC based polarization rotator was designed employing both coupled-mode theory and normal modal analysis for THz frequency applications. Both design methods led to the same results. The design was verified by the 3D-FDTD simulation of the polarization rotator structure. For a square hole PC polarization rotator, a polarization conversion efficiency higher than 90% over the propagation distance of 12 λ was achieved within the frequency band of 586.4-604.5 GHz corresponding to the normalized frequency of 0.258-0.267. The design was extended to a circular hole PC based polarization rotator. A polarization conversion efficiency higher than 75% was achieved within the frequency band of 600-604.5 GHz. The circular hole PC polarization rotator is more compact than the square-hole PC structure. On the other hand, the circular hole PC polarization rotator is narrow band in comparison with the square hole PC polarization rotator. In a circular hole PC slab structure, the Bloch modes (fast and slow modes) couple energy to the TM-like PC slab modes. In both square and circular hole PC slab structures with finite number of rows, and the TM-like PC slab modes are extended to the lower edge of the bandgap. In bandgap calculation using PWEM, it is assumed that the PC structure is extended to infinity, however in practice the number of rows is limited, which is the source of discrepancy between the bandgap calculation using PWEM and 3D-FDTD. In an asymmetric loaded circular hole PC slab waveguide, the leaky TM-like PC slab modes are extended deep inside the bandgap and overlapped with both the slow and fast Bloch modes; whereas, in an asymmetric loaded square hole PC slab waveguide, the leaky TM-like PC slab modes are below the frequency band of slow and fast modes. Therefore, TM-like PC slab modes have significantly more adverse effect on the performance of the circular-hole based polarization rotator leading to a narrow band structure. SOI based PC membrane technology for THz application was developed. The device layer is made of highly resistive silicon to maintain low loss propagation for THz wave. The PC slab waveguide and polarization rotators were fabricated employing this technology. Finally, an a-SiON PC slab waveguide structures were also fabricated at low temperature for optical applications. This technology has the potential to be implemented on any substrate or CMOS chips.

Carrier dynamics in GaAs-based photoconductive terahertz (THz) sources is investigated using Monte Carlo techniques to optimize the emitted THz transients. A self-consistent Monte Carlo-Poisson solver is developed for the spatio-temporal carrier transport properties. The screening contributions to the THz radiation associated with the Coulomb and radiation fields are obtained self-consistently by incorporating the three-dimensional Maxwell equations into the solver. In addition, the enhancement of THz emission by a large trap-enhance field (TEF) near the anode in semi-insulating (SI) photoconductors is investigated. The transport properties of the photoexcited carriers in photoconductive THz sources depend markedly on the initial spatial distribution of those carriers. Thus, considerable control of the emitted THz spectrum can be attained by judiciously choosing the optical excitation spot shape on the photoconductor, since the carrier dynamics that provide the source of the THz radiation are strongly affected by the ensuing screenings. The screening contributions due to the Coulomb and radiation parts of the electromagnetic field acting back on the carrier dynamics are distinguished. The dominant component of the screening field crosses over at an excitation aperture size with full width at half maximum (FWHM) of ~100 um for a range of reasonable excitation levels. In addition, the key mechanisms responsible for the TEF near the anode of SI photoconductors are elucidated in detail. For a given optical excitation power, an enhancement of THz radiation power can be obtained using a maximally broadened excitation aperture in the TEF area elongated along the anode due to the reduction in the Coulomb and radiation screening of the TEF.

This thesis utilized pulse shaping and Gerberg-Saxton algorithm to develop high power tunable narrowband terahertz radiation and applications. By the way of using Freezing algorithm and Gerberg-Saxton, pulse width, pulse duration, pulse position and pulse number can be controlled. The pulse train can be pumping source of high power tunable narrowband terahertz radiation, by avoid the saturations and different pulse duration. The simulation shown the result can have 5GHz narrowband width closing to commercial product. Besides, we demonstrated the THz multi-wavelength interference method by using THz-TDS (terahertz time domain spectroscopy) to measure the liquid crystal cell gap. We have also used THz-TDS to investigate the complex optical constants and birefringence of cholesteric liquid crystal mixture BL006. The extraordinary (ne) and ordinary (no) indices of refraction at are 1.784-1.817 and 1.516-1.555 giving rise to a birefringence of 0.25¡V0.29 in 0.2THz~1.6THz.

In this thesis we use pulse shaping system to generate pulse train. Using empirical mode decomposition(EMD) and short-time Fourier transform(STFT) to analyze the signal of terahertz radiation. we use pulse shaping system to modulate the amplitude and phase of light which provide for pulse train generation. Compare with other method, first, our method will improve the stability of time delay control. Second this method is easier to control the time delay and number of pulse in the pulse train. In the past, people find the occur time of high frequency by observed the time domain of terahertz radiation directly, but if the occur time near the time of the peak power of terahertz radiation, we can¡¦t find out the occur time of high frequency. Using STFT can find out the relationship between intensity and time, but if the modes in signal have different width of frequency STFT have to use different time window to get the best frequency resolution and time resolution. However the time window with different width will have different frequency resolution, and the relationship between intensity and time will change with different frequency resolution, therefore using different frequency resolution will get different result, so we need a new signal analysis method. To solve this problem we use EMD to decompose different mode in the signal of terahertz radiation into different intrinsic mode function(IMF), and analyze the signal of terahertz by STFT to find the occur time of high frequency of terahertz radiation. Because the modes are separated in to different IMF, we can use STFT with the same time window. We expect this method applied to narrow-band frequency-tunable THz wave generation will be better.

In this thesis, we propose and demonstrate a simple and precise method for measuring mm scaled cell gap by using terahertz time domain spectroscopy (THz-TDS) system. This method allows us to measure the cell gap from 15mm to 1.5mm. In addition, the accuracy of measured thickness for the proposed method is also discussed and analyzed. Meanwhile, a nematic liquid crystal BL006 with birefringence as high as 0.27 in THz frequency range and its optical properties of cholesteric liquid crystal (CLC) as mixing chiral materials are investigated and reported. The ordinary refractive index and average effective refractive index at 20oC are from 1.52 to 1.56 and from 1.61 to 1.64, respectively, in THz frequency ranging from 0.2 THz to 1.4THz. In addition, we also demonstrate that cell filled with CLC is with polarization independent property for THz radiation. Through the 5mm cell filled CLC with diluted concentration of the dopant chiral material for decreasing the critical voltage, an electric controlled polarization independent phase shifter with the modulation depth exceeding 2pi is demonstrated. Furthermore, we also investigate the driving field dependence of phase retardation and discuss the reliability.