High-Frame-Rate Oil Film Interferometry Jonathan Charles White This thesis presents the design and implementation of a high-frame-rate oil film interferometry technique (HOFI) used to directly measure skin friction in time dependent flows. Experiments were performed to determine the ability of a high-speed camera to capture oil film interferometry images. HOFI was found to be able to capture these interferometry images at frequencies up to 105 Hz. Steady laminar and turbulent flows were tested. Transient flows tested consisted of a wind tunnel ramping up in velocity and a laminar boundary layer which was intermittently tripped to turbulence by puffing air out of a pressure tap. Flow speeds ranged from 0 to 108 ft/sec and 10 and 50 cSt Dow Corning 200 dimethylpolysiloxane silicone oil was used. The skin friction was determined from the rate of change of the height of the oil film using lubrication theory. The height of the oil film was determined from the high speed camera interferogram images using a MATLAB script which determined fringe spacing by fitting a four-parameter sine wave to the intensity levels in each image. The MATLAB script was able to determine the height of the oil film for thousands of interferogram images in only a few minutes with sub-pixel error in fringe spacing. The skin friction was calculated using the oil film height history allowing for the direct measurement of skin friction in time dependent flows.

Embora o ressalto hidráulico seja um assunto já muito estudado, é igualmente um assunto de grande interesse, acerca do qual ainda existem diversos questionamentos a respeito de suas características. Por essa razão, buscou-se neste projeto o desenvolvimento de estudos experimentais e a proposição de um modelo teórico. Os trabalhos experimentais foram desenvolvidos com o uso de um sensor ultrassônico, para aquisição de dados instantâneos da superfície livre, sendo estudados ressaltos com número de Froude na seção supercrítica entre 1,94 e 5,26 e duas condições de controle a montante: comporta plana e vertedor de soleira espessa. As seguintes variáveis foram avaliadas a partir dos experimentos: comprimento do rolo, comprimento do ressalto, intensidade turbulenta vertical, perfil da superfície livre e frequências dos sinais de saída do sensor. Os perfis da superfície livre, considerando-se separadamente os dados de comporta e vertedor, foram ajustados a partir de uma equação heurística e as frequências características foram comparadas com os comprimentos característicos do ressalto. Além disso, foram efetuados registros fotográficos do escoamento com uma câmera de alta velocidade e luz laser para uma condição experimental (com baixo número de Froude supercrítico), sendo a superfície livre detectada por meio de técnicas usuais de processamento de imagens. O perfil médio obtido com o sensor foi semelhante ao perfil das imagens. Em relação ao modelo teórico proposto, este foi desenvolvido a partir de dois volumes de controle (VC) fixos, sendo obtidas duas equações para a relação entre o comprimento do rolo e a altura supercrítica. Verificou-se uma variação de quarenta porcento entre os valores previstos com as equações e os dados experimentais, em função da própria divergência dos dados de comprimento do rolo indicados pelos autores. De forma geral, o estudo mostrou-se relevante por possibilitar a avaliação da estrutura externa do ressalto hidráulico por meio de diferentes abordagens metodológicas. / Althought hydraulic jump has been studied for a long time, it is equally a theme of large interest, which many aspects related to its characteristics remain unanswered. Therefore, the development of experimental studies and the proposal of a theoretical model was sought in this project. The experimental works were carried out using an ultrassonic sensor, in order to acquire instantaneous data of the free surface, being studied hydraulic jumps with inflow Froude number ranging between 1.94 and 5.26 and two upstream control structures: plane gate and broad-crested weir. The following variables were evaluated: roller length, hydraulic jump length, vertical turbulent intensity, free surface profile, frequencies of the output data sensor. The free surface profiles, considering individually the plane gate and broad-crested weir, were adjested using a heuristic equation and characteristic frequencies were compared to the characteristic jump lengths. Furthermore, the flow was photographed using a high speed camera and a laser light for one experimental condition (for low inflow Froude number). The free surface in images were detected trought usual image processing techniques. The mean profile obtained from the sensor was very similar to the images profile. Regarding the theoretical model, it was developed considering two fixed control volumes (VC), obtaining two equations for the roller length and supercritical depth ratio. A variation of forty percent was observed between the predicted and experimental values, due to the own divergence among the roller length data suggested by the authors. Overall, the study was relevant, because it allowed the evaluation of the external structure of hydraulic jumps by means of different methodological approaches.

La finalité de cette thèse est d’étudier la pertinence et les limites des méthodes de vision 3D couplées à une caméra ultra-rapide pour la mesure de champs vibratoires, sans contact et de manière synchrone, dans le domaine des fréquences associées à la vibro-acoustique. Un premier montage pseudo stéréoscopique, issu de la robotique, mobilisant un jeu de quatre miroirs afin de générer deux vues virtuelles à partir d’une seule caméra réelle, a été testé sur une plaque et un haut-parleur. Les résultats, validés par comparaison avec ceux obtenus avec un vibromètre laser, attestent de la pertinence de l’approche en dépit des contraintes liées aux éléments optiques. Dans une logique de simplification, trois autres montages ont alors été proposés et testés, permettant de concevoir deux techniques de mesure de vibration plein champ et une méthode itérative de rectification d’images (IRIs), adaptées au contexte. La méthode sans miroir utilise une ligne mathématique pour la triangulation et est fondamentalement adaptée à la mesure de vibrations mono-axiales d'objets globalement plans, affichant des déplacements non-répétables selon la normale de la surface ou selon un axe connu. La méthode à caméras asynchrones, quant à elle, utilise une caméra ultra-rapide et une caméra rapide, et permet la mesure de vibrations multi-axiales de phénomènes vibratoires 3D. Les résultats obtenus sur le capot d’une voiture et sur un haut-parleur attestent de son potentiel pour la caractérisation de panneaux ou le test qualité de fin de chaine d’assemblage de haut-parleurs par exemple. En conclusion, les trois protocoles de mesure et les résultats associés sont comparés afin de cibler leurs potentialités et limites respectives dans le contexte de la mesure de vibrations. / The objective of this Ph.D is to study the relevance and limits of 3D vision methods coupled to high-speed cameras and applied to non-contact synchronous vibration measurement, in the vibro-acoustic range of frequencies. A first pseudo stereoscopic set-up, taken from robotics, using a four-mirror adapter in order to generate two virtual viewpoints from a single real camera, has been tested on a plate and a loudspeaker. The results, validated by comparison with those obtained with a laser vibrometre, prove the relevance of the approach, despite some constraints related to the optical elements. In a logic of simplification, three other set-ups have then been proposed and tested, allowing designing two full-field vibration measurement techniques and a method for the Iterative Rectification of Images (IRIs), adapted to the context. The no-mirror method uses a mathematical line to triangulate positions and is basically suited to measure the single-axis vibrations of globally plane objects, displaying non-repeatable displacements along the normal of the surface or along a known axis. The asynchronous cameras technique requires a high-speed and an industrial camera used simultaneously to measure the multi-axis displacements of 3D vibratory phenomena. The results obtained on a car bonnet and a loudspeaker prove its potential to characterise large panels or to carry out end-of-line testing of loud-speakers for example. In conclusion, the three measurement protocols and the associated results are compared in order to assess their respective potentialities and limits in the context of vibration measurement.

Stratified two-phase flows were investigated at different test facilities with horizontal test sections in order to provide an experimental database for the development and validation of computational fluid dynamics (CFD) codes. These channels were designed with rectangular cross-sections to enable optimal observation conditions for the application of optical measurement techniques. Consequently, the local flow structure was visualised with a high-speed video camera, delivering data with high-resolution in space and time as needed for CFD code validation. Generic investigations were performed at atmospheric pressure and room temperature in two air/water channels made of acrylic glass. Divers preliminary experiments were conducted with various measuring systems in a test section mounted between two separators. The second test facility, the Horizontal Air/Water Channel (HAWAC), is dedicated to co-current flow investigations. The hydraulic jump as the quasi-stationary discontinuous transition between super- and subcritical flow was studied in this closed channel. Moreover, the instable wave growth leading to slug flow was investigated from the test section inlet. For quantitative analysis of the optical measurements, an algorithm was developed to recognise the stratified interface in the camera frames, allowing statistical treatments for comparison with CFD calculation results. The third test apparatus was installed in the pressure chamber of the TOPFLOW test facility in order to be operated at reactor typical conditions under pressure equilibrium with the vessel atmosphere. The test section representing a flat model of the hot leg of the German Konvoi pressurised water reactor (PWR) scaled at 1:3 is equipped with large glass side walls in the region of the elbow and of the steam generator inlet chamber to allow visual observations. The experiments were conducted with air and water at room temperature and maximum pressures of 3 bar as well as with steam and water at boundary conditions of up to 50 bar and 264°C. Four types of experiments were performed, including generic test cases as well as transient validation cases of typical nuclear reactor safety issues. As an example, the co-current flow experiments simulate the two-phase natural circulation in the primary circuit of a PWR. The probability distribution of the water level measured in the reactor pressure vessel simulator was used to characterise the flow in the hot leg. Moreover, the flooding behaviour in this conduit was investigated with dedicated counter-current flow limitation experiments. A comparison of the flooding characteristics with similar experimental data and correlations available in the literature shows that the channel height is the characteristic length to be used in the Wallis parameter for channels with rectangular cross-sections. Furthermore, for the analysis of steam/water experiments, condensation effects had to be taken into account. Finally, the experimental results confirm that the Wallis similarity is appropriate to scale flooding in the hot leg of a PWR over a large range of pressure and temperature conditions. Not least, different examples of comparison between experiment and simulation demonstrate the possibilities offered by the data to support the development and validation of CFD codes. Besides the comparison of qualitative aspects, it is shown exemplarily how to treat the CFD results in order to enable quantitative comparisons with the experiments.

Für die Menschen zählen Gewitter mit Donner und Blitz zu den ältesten bekannten Phänomenen der Natur. Die Tatsache, dass Blitze dennoch bis heute nicht abschließend erforscht sind, liegt in dem äußerst komplexen, schnellen und stochastischen Verhalten der Blitzentladung begründet. Der Autor befasste sich in Rahmen dieser Arbeit u.a. mit der Entwicklung eines modernen Messsystems, durch das die Erfassung von sowohl elektrischen als auch optischen Parametern der im Nanosekundenbereich ablaufenden Prozesse der Entladungen möglich wurde. Es handelt sich um technisch anspruchsvolle Messungen von hohen Stoßspannungen und schwachen Vorentladungsströmen in einem großen Frequenzbereich. Außerdem gelang es durch eine geschickte Synchronisation, die Entladungsprozesse präzise und erstmalig in einer Fotosequenz aufzunehmen. Auf Grundlage der Messergebnisse konnte der Entladungsprozess in mehrere Phasen der Vorentladung unterteilt und beschrieben werden. Vor allem beweisen die Messergebnisse die Existenz einer kanalartigen Vorentladung, die nicht zwingend zu einem Durchschlag führt. Dieser Mechanismus, der bei langsam ansteigenden Spannungen als stabile Leaderentladung benannt und mit Thermoionisation gekennzeichnet ist, war bei Blitzstoßspannungen bisher umstritten. / The breakdown behavior of long air gaps by Lightning Voltages has been investigated and the results of a new measurement system are reported. A series of up to eight photos (made by a high-speed camera) have recorded the expansion of discharge activities during the breakdown process. The pre-discharge current and voltage have been measured as well. The modern measurement techniques have made possible the synchronization of the photos with the current and voltage measurements in nanosecond-ranges. The combination of the measured current, voltage, and photos can precisely explain the breakdown process. The experiments have been carried out with the lightning impulses up to 2.4 MV and the air gaps up to 4 m. Despite of such high voltages, the experimental system has been verified to be appropriate for measuring the pre-discharge current in mA-ranges.

This thesis deals with the use of the video as a didactic tool in the education of the physics. Introductory part is theoretic and focuses on classification of didactic tools which can be used for physics teaching. Second part analyses the possibility of capturing physical effects, especially effects with very long or very short duration which cannot be captured by conventional devices. This part is focused on the right selection of physical effects, selecting and setting of suitable devices for capturing and further processing of the recorded video. The next section is based on the previous analysis of physical effects, which are recorded and processed into the form of educational movie. The main result of this thesis is the collection of educational movies of fast and very slow physical effects useful as the didactic tool for the teaching of physics.

Embora o ressalto hidráulico seja um assunto já muito estudado, é igualmente um assunto de grande interesse, acerca do qual ainda existem diversos questionamentos a respeito de suas características. Por essa razão, buscou-se neste projeto o desenvolvimento de estudos experimentais e a proposição de um modelo teórico. Os trabalhos experimentais foram desenvolvidos com o uso de um sensor ultrassônico, para aquisição de dados instantâneos da superfície livre, sendo estudados ressaltos com número de Froude na seção supercrítica entre 1,94 e 5,26 e duas condições de controle a montante: comporta plana e vertedor de soleira espessa. As seguintes variáveis foram avaliadas a partir dos experimentos: comprimento do rolo, comprimento do ressalto, intensidade turbulenta vertical, perfil da superfície livre e frequências dos sinais de saída do sensor. Os perfis da superfície livre, considerando-se separadamente os dados de comporta e vertedor, foram ajustados a partir de uma equação heurística e as frequências características foram comparadas com os comprimentos característicos do ressalto. Além disso, foram efetuados registros fotográficos do escoamento com uma câmera de alta velocidade e luz laser para uma condição experimental (com baixo número de Froude supercrítico), sendo a superfície livre detectada por meio de técnicas usuais de processamento de imagens. O perfil médio obtido com o sensor foi semelhante ao perfil das imagens. Em relação ao modelo teórico proposto, este foi desenvolvido a partir de dois volumes de controle (VC) fixos, sendo obtidas duas equações para a relação entre o comprimento do rolo e a altura supercrítica. Verificou-se uma variação de quarenta porcento entre os valores previstos com as equações e os dados experimentais, em função da própria divergência dos dados de comprimento do rolo indicados pelos autores. De forma geral, o estudo mostrou-se relevante por possibilitar a avaliação da estrutura externa do ressalto hidráulico por meio de diferentes abordagens metodológicas. / Althought hydraulic jump has been studied for a long time, it is equally a theme of large interest, which many aspects related to its characteristics remain unanswered. Therefore, the development of experimental studies and the proposal of a theoretical model was sought in this project. The experimental works were carried out using an ultrassonic sensor, in order to acquire instantaneous data of the free surface, being studied hydraulic jumps with inflow Froude number ranging between 1.94 and 5.26 and two upstream control structures: plane gate and broad-crested weir. The following variables were evaluated: roller length, hydraulic jump length, vertical turbulent intensity, free surface profile, frequencies of the output data sensor. The free surface profiles, considering individually the plane gate and broad-crested weir, were adjested using a heuristic equation and characteristic frequencies were compared to the characteristic jump lengths. Furthermore, the flow was photographed using a high speed camera and a laser light for one experimental condition (for low inflow Froude number). The free surface in images were detected trought usual image processing techniques. The mean profile obtained from the sensor was very similar to the images profile. Regarding the theoretical model, it was developed considering two fixed control volumes (VC), obtaining two equations for the roller length and supercritical depth ratio. A variation of forty percent was observed between the predicted and experimental values, due to the own divergence among the roller length data suggested by the authors. Overall, the study was relevant, because it allowed the evaluation of the external structure of hydraulic jumps by means of different methodological approaches.

This thesis focuses on an experimental study of the anode area of the hybrid water- gas DC arc plasma torch that is used in many industrial applications, including plasma spraying, hydrocarbon reforming, pyrolysis, and organic waste gasification. The effects of ambient pressure and plasma generation conditions on the torch's plasma jet were studied, with particular focus on the torch's anode area. Movement of the anode arc attachment is described in detail, including its speed, range of its motion on the anode surface, restrike periods, and the frequency of its many sudden decelerations and re-accelerations. It was found that the anode erosion can be compared relatively simply by quick processing of high-speed camera videos. The anode erosion was also measured directly. Many electric probe measurements were made in the anode area of this plasma torch for the first time. By using these electric probes, shock waves, turbulent vortices, and plasma potential fluctuations were studied directly. It was found that a mean plasma electric field and a mean plasma electrical conductivity in the anode area can be satisfactorily estimated also non-intrusively by quick processing of high-speed camera videos. Moreover, schlieren videos of the plasma jet in the anode area were created. 1

In this present work, the dynamics of deformation mechanisms activated in binary magnesium-gadolinium alloys with respect to amount of Gd were investigated with in-situ experimental methods. Cast alloys are characterized by random texture. Compression test were done at room temperature with simultaneous record of acoustic emission response. The acoustic emission signal was subsequently analysed using advanced clustering method providing information about the dominant deformation mechanisms. High speed camera was used to study the dynamics of twinning, including estimation of the velocity of twin propagation with respect to Gd concentration. The deformation tests were repeated in a chamber of scanning electron microscope (in-situ SEM) with concurrent following the microstructure development using secondary electrons and electron back-scattered diffraction (EBSD) in different stages of the deformation. Main goal of this measurements was to identify active slip systems and the progress of twin volume fraction during deformation. Keywords: magnesium alloy, deformation tests, acoustic emission, high-speed camera, electron microscopy, twinning

La démarche expérimentale menée dans cette thèse CIFRE a eu comme objectif l’étude de la faisabilité de la séparation électrostatique d’une large gamme de mélanges de matériaux granulaires issus de déchets d’équipements électriques et électroniques (conducteur – isolant, conducteur – conducteur et isolant – isolant). Trois mécanismes physiques de charge électriques ont été mis en oeuvre : l’induction électrostatique, la décharge couronne et l’effet triboélectrique. Un dispositif de charge de laboratoire et deux séparateurs électrostatiques industriels ont été conçus et réalisés. Le dispositif de charge à cylindre(s) tournant(s) permet la charge triboélectrique de matériaux plastiques. Le prototype de séparateur industriel a d’abord été réalisé pour le traitement de mélanges granulaires conducteur – isolant puis a été adapté à la séparation isolant – isolant. Les trois mécanismes de charge peuvent y être utilisés. Ce prototype a permis la fabrication du premier séparateur électrostatique de série de la société CITF dédié à la séparation de déchets de câbles électriques. Des mesures de charge et de masse ainsi que des simulations et visualisations des trajectoires des particules par caméra rapide ont facilité l’analyse des phénomènes. La méthode des plans d’expérience a permis d’identifier les facteurs influents sur les processus de séparation et de définir leur point de fonctionnement optimal. L’influence d’une décharge à barrière diélectrique sur la charge triboélectrique et la séparation électrostatique de mélanges plastiques a été étudiée. Les travaux réalisés dans cette thèse ont confirmé la séparabilité électrostatique de mélanges de matériaux granulaires. / The experimental approach used in this thesis was aimed at the study of the feasibility of the electrostatic separation of a wide range of granular mixtures from waste electric and electronic equipment (conductive – insulator, conductive – conductive, insulator – insulator). Three physical mechanisms of electrical charging have been employed: electrostatic induction, corona discharge and triboelectric effect. A tribocharging device and two industrial electrostatic separators have been designed and engineered. The rotating cylinder tribocharging device allows the triboelectric charging of plastics. The industrial separator prototype was firstly built for processing conducting – insulator granular mixtures and then adapted for insulator – insulator separation. This prototype, which enables the use of all three electrical charging mechanisms, served as model for the CITF company first industrial electrostatic separator for the recycling of metals and plastics from electric cable wastes. Charge and mass measurement, as well as modelling and visualization of particle trajectories by a high-speed camera facilitated the investigations. Design of experiments method was used to define the influential factors and find the optimum operating conditions of the separation processes. Dielectric barrier discharge exposure of granular plastics may enhance the efficiency of the triboelectric charging of these materials and hence facilitate their electrostatic separation. These researches have confirmed the feasibility of the electrostatic separation of a wide variety of granular mixtures.