Magister Scientiae - MSc / This study reports on the changes in the structural properties of a tungsten-filament when exposed to a methane / hydrogen ambient for different durations at various filament-temperatures. / South Africa

Philosophiae Doctor - PhD / When the amorphous silicon (a-Si) dangling bonds are bonded to hydrogen the concentration of the dangling bond is decreased. The resulting film is called hydrogenated amorphous silicon (a-Si:H). The reduction in the dangling bonds concentration improves the optoelectrical properties of the film. The improved properties of a-Si:H makes it possible to manufacture electronic devices including a solar cell. A solar cell device based on the hydrogenated amorphous silicon (a-Si:H) was fabricated using the Hot-Wire Chemical Vapour Deposition (HWCVD). When an n-i-p solar cell configuration is grown, the norm is that the p-doped layer is deposited from a mixture of silane (SiH4) gas with diborane (B2H6). The boron atoms from diborane bonds to the silicon atoms and because of the number of the valance electrons, the grown film becomes a p-type film. Aluminium is a group 3B element and has the same valence electrons as boron, hence it will also produce a p-type film when it bonds with silicon. In this study the p-doped layer is grown from the co-deposition of a-Si:H from SiH4 with aluminium evaporation resulting in a crystallized, p-doped thin film. When this thin film is used in the n-i-p cell configuration, the device shows photo-voltaic activity. The intrinsic layer and the n-type layers for the solar cell were grown from SiH4 gas and Phosphine (PH3) gas diluted in SiH4 respectively. The individual layers of the solar cell device were characterized for both their optical and electrical properties. This was done using a variety of experimental techniques. The analyzed results from the characterization techniques showed the films to be of device quality standard. The analysed results of the ptype layer grown from aluminium showed the film to be successfully crystallized and doped. A fully functional solar cell was fabricated from these layers and the cell showed photovoltaic activity. / South Africa

Philosophiae Doctor - PhD / When the amorphous silicon (a-Si) dangling bonds are bonded to hydrogen the concentration of the dangling bond is decreased. The resulting film is called hydrogenated amorphous silicon (a-Si:H). The reduction in the dangling bonds concentration improves the optoelectrical properties of the film. The improved properties of a-Si:H makes it possible to manufacture electronic devices including a solar cell.A solar cell device based on the hydrogenated amorphous silicon (a-Si:H) was fabricated using the Hot-Wire Chemical Vapour Deposition (HWCVD). When an n-i-p solar cell configuration is grown, the norm is that the p-doped layer is deposited from a mixture of silane (SiH4) gas with diborane (B2H6). The boron atoms from diborane bonds to the silicon atoms and because of the number of the valance electrons, the grown film becomes a p-type film. Aluminium is a group 3B element and has the same valence electrons as boron, hence it will also produce a p-type film when it bonds with silicon.In this study the p-doped layer is grown from the co-deposition of a-Si:H from SiH4 with aluminium evaporation resulting in a crystallized, p-doped thin film. When this thin film is used in the n-i-p cell configuration, the device shows photo-voltaic activity.The intrinsic layer and the n-type layers for the solar cell were grown from SiH4 gas and Phosphine (PH3) gas diluted in SiH4 respectively. The individual layers of the solar cell device were characterized for both their optical and electrical properties. This was done using a variety of experimental techniques. The analyzed results from the characterization techniques showed the films to be of device quality standard. The analysed results of the ptype layer grown from aluminium showed the film to be successfully crystallized and doped.A fully functional solar cell was fabricated from these layers and the cell showed photovoltaic activity.

Magister Scientiae - MSc / The overall aim of this project is to study the heat transfer inside the reaction chamber of the Hot-Wire Chemical Vapor Deposition (HWCVD) system with a commercial software package FLUENT6.3; it is one of the most popular Computational Fluid Dynamics solvers for complex flows ranging from incompressible to mildly compressible to even highly compressible flows. The wealth of physical models in FLUENT allows us to accurately predict laminar and turbulent flows, various modes of heat transfer, chemical reactions, multiphase flows and other phenomena with complete mesh flexibility and solution-based mesh adaptation. In this study the 3-D HWCVD geometry was measured and created in GAMBIT which then generates a mesh model of the reaction chamber for the calculation in FLUENT. The gas flow in this study was characterized as the steady and incompressible fluid flow due to the small Mach number and assumptions made to simplify the complexity of the physical geometry. This thesis illustrates the setups and solutions of the 3-D geometry and the chemically reacting laminar and turbulent gas flow, wall surface reaction and heat transfer in the HWCVD deposition chamber. / South Africa

This thesis consists of description of design and construction of device for measuring air velocity created in it´s practical part. In introduction is mentioned basic theoretical information related to given problem, in the next chapters is descripted design and construction of measuring device along with description of calibration proces. At the end is placed chapter about testing the final device.

This thesis deals with flow measuring techniques applied on steady and pulsatingflows. Specifically, it is focused on gas flows where density changes canbe significant, i.e. compressible flows. In such flows only the mass flow ratehas a significance and not the volume flow rate since the latter depends onthe pressure. The motivation for the present study is found in the use of flowmeters for various purposes in the gas exchange system for internal combustionengines. Applications can be found for instance regarding measurements of airflow to the engine, or measurements of the amount of exhaust gas recirculation.However the scope of thesis is wider than this, since the thesis aims toinvestigate the response of flow meters to pulsating flows. The study is mainlyexperimental, but it also includes an introduction and discussion of several inindustry, common flow measuring techniques.The flow meters were studied using a newly developed flow rig, designedfor measurement of steady and pulsating air flow of mass flow rates and pulsefrequencies typically found in the gas exchange system of cars and smallertrucks. Flow rates are up to about 200 g/s and pulsation frequencies from 0 Hz(i.e. steady flow) up to 80 Hz. The study included the following flow meters:hot-film mass flow meter, venturi flowmeter, Pitot tube, vortex flowmeter andturbine flowmeter. The performance of these meters were evaluated at bothsteady and pulsating conditions. Furthermore, the flow under both steady andpulsating conditions were characterized by means of a resistance-wire basedmass flow meter, with the ability to perform time resolved measurements ofboth the mass flux ρu, and the stagnation temperature T0.Experiments shows that, for certain flow meters, a quasi-steady assumptionis fairly well justified at pulsating flow conditions. This means that thefundamental equations describing the steady flow, for each instant of time,is applicable also in the pulsating flow. In the set-up, back-flow occurred atcertain pulse frequencies, which can result in highly inaccurate output fromcertain flow meters, depending on the measurement principle. For the purposeof finding means to determine when back flow prevails, LDV measurementswere also carried out. These measurements were compared with measurementsusing a vortex flow meter together with a new signal processing technique basedon wavelet analysis. The comparison showed that this technique may have apotential to measure pulsating flow rates accurately.Descriptors: Flow measuring, compressible flow, steady flow, pulsating flow,hot-wire anemometry, cold-wire anemometry. / QC 20101208

The compressible turbulent boundary layer developing over atwo-dimensional bump which leads to a supersonic pocket with aterminating shock wave has been studied. The measurements havebeen made with hot-wire anemometry and Particle ImageVelocimetry (PIV). A method to calibrate hot-wire probes in compressible ow hasbeen developed which take into account not only the ow velocitybut also the inuence of the Mach number, stagnation temperatureand uid density. The calibration unit consists of a small jetow facility, where the temperature can be varied. The hot wiresare calibrated in the potential core of the free jet. The jetemanates in a container where the static pressure can becontrolled, and thereby the gas density. The calibration methodwas verfied in the at plate zero pressure gradient turbulentboundary layer in front of the bump at three different Machnumbers, namely 0.3, 0.5 and 0.7. The profiles were alsomeasured at different static pressures in order to see theinuence of varying density. Good agreement between the profilesmeasured at different pressures, as well as with the standardlogarithmic profile was obtained. The PIV measurements of the boundary layer ow in front ofthe 2D bump showed good agreement with the velocity profilesmeasured with hotwire anemometry. The shock wave boundary layerinteraction was investigated for an inlet Mach number of 0.69.A lambda shock wave was seen on the downstream side of thebump. The velocity on both sides of the shock wave as measuredwith the PIV was in good agreement with theory. The shock wavewas found to cause boundary layer separation, which was seen asa rapid growth of the boundary layer thickness downstream theshock. However, no back ow was seen in the PIV-data, probablybecause the seeding did not give enough particles in theseparated region. The PIV data also showed that the shock wavewas oscillating, i.e. it was moving approximately 5 mm back andforth. This distance corresponds to about five boundary layerthicknesses in terms of the boundary layer upstream theshock. <b>Descriptors:</b>Fluid mechanics, compressible ow,turbulence, boundary layer, hot-wire anemometry, PIV, shockwave boundary layer interaction, shape factor. / NR 20140805

Despite its importance in various industrial applications there is still a lack of experimental studies on the dynamic and thermal field of swirling jets in the near-field region. The present study is an attempt to close this lack and provide new insights on the effect of rotation on the turbulent mixing of a passive scalar, on turbulence (joint) statistics as well as the turbulence structure. Swirl is known to increase the spreading of free turbulent jets and hence to entrain more ambient fluid. Contrary to previous experiments, which leave traces of the swirl generating method especially in the near-field, the swirl was imparted by discharging a slightly heated air flow from an axially rotating and thermally insulated pipe (6 m long, diameter 60 mm). This gives well-defined axisymmetric streamwise and azimuthal velocity distributions as well as a well-defined temperature profile at the jet outlet. The experiments were performed at a Reynolds number of 24000 and a swirl number (ratio between the angular velocity of the pipe wall and the bulk velocity in the pipe) of 0.5. By means of a specially designed combined X-wire and cold-wire probe it was possible to simultaneously acquire the instantaneous axial and azimuthal velocity components as well as the temperature and compensate the former against temperature variations. The comparison of the swirling and non-swirling cases clearly indicates a modification of the turbulence structure to that effect that the swirling jet spreads and mixes faster than its non-swirling counterpart. It is also shown that the streamwise velocity and temperature fluctuations are highly correlated and that the addition of swirl drastically increases the streamwise passive scalar flux in the near field. / QC 20101124

No description available.

Flush-mounted cavity hot-wire probes have been around since two decades, but have typically not been applied as often compared to the traditional wall hot-wires mounted several wire diameters above the surface. While the latter suffer from heat conduction from the hot wire to the substrate in particular when used in air flows, the former is belived to significantly enhance the frequency response of the sensor. The recent work using a cavity hotwire by Gubian et al. (2019) came to the surprising conclusion that the magnitute of the fluctuating wall-shear stress τ+w,rms reaches an asymptotic value of 0.44 beyond the friction Reynolds number Re τ ∼ 600. In an effort to explain this result, which is at odds with the majority of the literature, the present work combines direct numerical simulations (DNS) of a turbulent channel flow with a cavity modelled using the immersed boundary method, as well as an experimental replication of the study of Gubian et al. in a turbulent boundary layer to explain how the contradicting results could have been obtained. It is shown that the measurements of the mentioned study can be replicated qualitatively as a result of measurement problems. We will present why cavity hot-wire probes should neither be used for quantitative nor qualitative measurements of wall-bounded flows, and that several experimental short-comings can interact to sometimes falsely yield seemingly correct results.