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L’intégration culture – élevage à l’échelle territoire représente une voie pour améliorer le fonctionnement métabolique et les services écosystémiques fournis par les systèmes agricoles, malgré les contraintes de spécialisation des exploitations. Cette thèse propose une méthodologie de conception de systèmes culture – élevage au niveau du territoire, dans une démarche participative structurée en trois grandes étapes : diagnostic des enjeux, conception d’options techniques et organisationnelles, évaluation multicritère. Chaque étape est outillée par un cadre conceptuel et une grille d’évaluation multicritère adaptée aux dispositifs de terrain menés sur le bassin versant de l’Aveyron. Les scénarios construits présentent deux modèles de l’intégration culture – élevage : une « filière territorialisée » pour la production de luzerne dans les systèmes de culture de l’aval du bassin à destination des élevages de l’amont, un « collectif d’agriculteurs bio » échangeant directement de la luzerne, des méteils et du fumier dans des groupes locaux. Chaque scénario présente des performances de durabilité améliorées et pourraient être complémentaires pour le changement de pratiques sur le territoire. La méthodologie développée permet la conception multi-niveaux et multi-domaines de scénarios d’intégration, et pourrait être renforcée par une évaluation quantitative des bénéfices attendus et des coûts de coordination entre acteurs. / Crop-livestock integration at territory level may be a pathway to impove metabolic functions and delivery of ecosystem services in agricultural systems, overcoming the constraints of farm specialization. This thesis builds on a methodology of participatory design of integrated crop-livestock systems at territory level in three steps: diagnosis of issues, design of technical and organizational options for change, multicriteria assessment. Each step is supported with a conceptual framework and a multicriteria grid adapted to the case study in Aveyron river basin. The designed scenarios show two approaches of crop –livestock integration: the introduction of alfalfa in downstream cropping systems sold to upstream livestock systems through a local supply chain and the direct exchanges of alfalfa, cereal-legume mixtures and animal manure in local groups of organic farmers. Both scenario present improved sustainability performances and could be complementary to initiate more sustainable practices in local farming systems. The methodology allows designing multi-level and multi-domain scenarios of crop-livestock integration. It could be improved with models for quantitative assessment of benefits and coordination costs among stakeholders.

Master thesis deals with usage issues of autonomous, self-sufficient and decentralized systems. In the first part convectional and experimental sources for autonomous systems are disclosed. Second chapter deals with accumulation of electrical and thermal energy and possibilities of applications. 3rd part is focused on pilot project realized for autonomous and smart systems, which were built in last years. In the 4th chapter electrical and thermal energy consumption curves are made on daily and monthly basis for 4 type objects. In the fifth part issue of autonomy is explained, and for type buildings solutions are made with additional return on investment. The last chapter is focused on calculation of thermal accumulator and briefly discloses small district heating.

The aim of this master project is to design an off-grid nearly-zero energy mountain guesthouse. First, the building structure is designed. It is a two-storeys building with roof made of lattice trusses. On first floor is dining room, kitchen, playroom and office. On second floor are guest rooms and an owner´s flat. The vertical load-bearing structures are designed from ceramic blocks. Horizontal load-bearing structures are designed from reinforced concrete monolithic slab. The building envelope is insulated with ETICS. Second, HVAC, lighting, photovoltaics and use of rainwater is designed. TZB system controlled remotely with a PC or cellphone are designed. Third, energy study is made. The project is developed using CAD (drawings), DEKsoft (thermal calculations) and Atrea Duplex (air conditioning design).

The rise in population causes serious issues in larger cities since the electrical grid is becoming overloaded. Simultaneously, the demand on more sustainable energy production and the use of renewable energy sources increase. Renewable energy based off-grid electrical systems are a possible solution to decrease the magnitude of these issues. The purpose of this thesis is to compare solar cells, solar thermal collectors and PVT (Photovoltaic thermal hybrid solar collectors) and design the most suitable combination of solar panels for a selfsufficient multi-family house in Jönköping, Sweden. The solar panels were compared from a cost and energy production perspective, then a suitable renewable energy system with all three types of panels was constructed and optimized using Opti-CE, which is a MATLABbased software. During the course of this thesis, an interview was made with Hans-Olof Nilsson who is a co-founder of Nilsson Energy and owner of a self-sufficient off-grid house. The results show that PVT-panels have higher energy production per area and 22% higher LCC (life cycle cost) than regular solar cells in combination with solar thermal collectors. Optimization results indicate that the house cannot be self-sufficient by installing solar panels on the given roof area only, rather the area of installed solar collectors should be increased to a minimum of 1497𝑚2 . With the given roof area of 900𝑚2 the house can only be self-sufficient a maximum of 75% of the time. The results also indicate that the introduction of compact systems with the simultaneous decrease of cost will make renewable off-grid energy systems more attractive in the future.

As manufacturing is creating welfare and prosperity, it is important for humankind. Nevertheless, manufacturing is causing the depletion of natural resources, environmental burdens affecting the health of animals, humans and eco-systems, and social conflicts. Thus, it is essential to implement sustainability into manufacturing. Paint shops are however known for being liable for a big part of the large energy consumptions within manufacturing. Therefore, it is necessary to investigate what cost-effective solutions can be implemented in paint shops in order to reduce the energy consumption in a sustainable manner. Hence, the aim of this study was to, from a manufacturing perspective identify possible cost-effective solutions for lowering energy consumption within paint shops. The aim was further divided into two research questions: • RQ1: What are the enablers for energy efficient paint shops? • RQ2: What are the challenges for energy efficient paint shops? The research approach used to answer the aim and research questions were a literature review and a case study. The literature review was performed to get a deeper understanding of the subject and was then complimented with the findings from the case study. The case study was performed at the paint shop of a global automotive manufacturing company in Sweden, which currently have a high energy consumption. The enablers identified were (1) implementation of solar photovoltaic, and an energy storage system, which enables an environmentally friendly way of generating energy on-site and store excess energy for later use. The energy storage system can also be used to save money by utilizing the fluctuating electricity market prices, charging the battery when the energy price is at its lowest. (2) Implementation of an UV-curing system and paint, which is an environmentally harmless method of curing paint. (3) Reducing or disabling the heating, ventilation and air conditioning system of a building when it is not a necessity. (4) Workers commitment and motivation towards sustainability, to ensure everyone’s participation. The challenges identified were (1) the expensiveness of sustainability, allocating and prioritizing it in budgets is challenging for a company since profitability is always a major concern that often overshadows sustainability. (2) The risk of modifying the processes within the paint shop, as the consequences are unexplored. (3) In its current state, the energy consumption of the paint shop is very high, it is hence difficult to provide the whole paint shop with solely solar photovoltaic. (4) An energy storage system requires space and freeing up that space is a challenge without reconstructing existing facilities. (5) With implementation of UV- curing, the paint used must be curable with UV-light. Additionally, complex three-dimensional shapes make it challenging to properly cure evenly with UV-curing. (6) It is not guaranteed whether it is possible to completely shut down heating, ventilation and air conditioning since industrial equipment in general is designed to always run. (7) Sustainability is not a focus and even if it is increasingly requested by society, the commitment of companies is experienced as low. It is challenging to motivate all the employees to work towards sustainability and find ways to always keep sustainability in mind and to prioritize it over other alternatives.

This work is inspired by the peculiar behavior of the natural systems, namely the ability to produce self-sustained oscillations in the level of tens of Hertz in constant ambient conditions. This feature is one of the key signatures prescribed to living organisms. The firing rate of neuronal cells, a pulsating heart, or the beating of cilia and flagella are among many biological examples that possess amazing functionalities and unprecedented intelligence solely relying on bio-electro-chemical processes. Exploring shapeable polymeric technologies, new self-oscillating artificial microsystems were developed within this thesis. These microsystems rely on the novel nonlinear architecture that exhibits a negative differential resistance (NDR) within the parametric response that enables periodic oscillations. These systems are made of polymers and metals and were microfabricated in a planar fashion. The electrochemically deposited ionic electroactive polymers act as actuators of the system. Upon the self-assembly process, due to the interlayer strains, the planar device transforms into a three-dimensional soft nonlinear system that is able to perform self-sustained relaxation oscillations when subjected to a constant electric field while consuming extremely low powers (as low as several microwatts). The parameters of these systems were tuned for a high oscillation amplitude and frequency. This electro-mechanical parametric relaxation oscillator (EMPRO) can generate a rhythmic motion at stroke frequencies that are biologically relevant reaching up to ~95 Hz. The EMPRO oscillations at high frequencies generate a flow in the surrounding liquid, which was observed in the form of vortices around the micro actuators. This flow was further studied in ex-vivo conditions by measuring Doppler shifts of ultrasound waves. The EMPRO was made autonomous by integrating an electrochemical voltaic cell. Four different electrochemical batteries were tested to match the power consumption of the EMPRO system and electrochemical compatibility of the surrounding media. An Ag-Mg primary cell was then integrated with the EMPRO for autonomous operation without the need for external power sources, cables or controllers. This biomimicking self-powered self-sustaining oscillating microsystem is envisioned to be useful in novel application scenarios operating at low Reynolds numbers in biologically relevant conditions. Furthermore, as the system is electromechanical in nature, it could be integrated with electronic components such as sensors and communication devices in the next generation of autonomous microsystems.:  Table of contents Acronyms 7 1 Introduction 8 1.1 Motivation 9 1.2 Objectives 9 1.3 Thesis organization 10 2 Background 12 2.1 A brief review on nonlinear self-oscillation 12 2.2 Self-oscillating biological systems 13 2.3 Stimuli responsive materials 15 2.3.1 Electroactive polymers in electrochemical cells 16 2.3.2 Sources of electrical field for electroactive polymers 24 2.4 Self-oscillating synthetic systems 27 2.5 Movement in low Reynolds number regime 33 3 Materials and methods 38 3.1 Deposition methods 38 3.1.1 Photolithography 38 3.1.2 Plasma sputtering 41 3.1.3 Atomic layer deposition 42 3.1.4 Electrochemical polymerization 44 3.2 Shapeable polymeric platform technology 46 3.2.1 Sacrificial layer 46 3.2.2 Hydrogel swelling layer 47 3.2.3 Polyimide reinforcing layer 48 3.3 Characterization methods 49 3.3.1 Profilometry 49 3.3.2 Scanning electron and focused ion beam microscopy 50 3.3.3 Cyclic Voltammetry 52 3.3.4 Ultrasound and Doppler shift measurements 53 4 Electromechanical Parametric Relaxation Oscillators (EMPROs) 56 4.1 Relaxation oscillation in EMPROs 56 4.2 Theory of EMPRO relaxation oscillations 61 4.3 Realization of EMPROs 67 4.3.1 Design parameters of EMPROs 67 4.3.2 EMPRO on-chip battery integration 71 4.4 Fabrication of autonomous EMPROs 76 5 EMPRO performances 84 5.1 Externally biased EMPROs 84 5.2 Autonomous EMPROs 95 6 Conclusions and outlook 98 6.1 Outlook 99 Bibliography i List of Figures and Tables xi Versicherung xiii Acknowledgements xiv Scientific publications and contributions xvi Theses xvii Curriculum Vitae xix

Der 2. Präsenz- Workshop des Forschungsprojektes „EVERSOL-MFH“ fand diesmal unter besonderen Voraussetzungen bei der eG Wohnen 1902 in Cottbus statt. In direkter Nachbarschaft zu den im Projekt untersuchten Sonnenhäusern kamen ca. 50 Teilnehmer aus Forschung, Wohnungswirtschaft und Planungsbüros mit gebührendem Abstand zusammen. Zusätzlich konnten an zwei Tagen jeweils weitere fast 20 Interessierte der Onlineübertragung aller Vorträge folgen und sich so auch an den anschließenden Diskussionen über den Chat beteiligen. Diese besondere Herausforderung gelang nach anfänglichen Startschwierigkeiten und wird für folgende Workshops als interessante Zusatzoption geplant. Dank vieler Gastbeiträge wurde insgesamt eine reiche Vortragsvielfalt rund um den Themenschwerpunkt “Bauen der Zukunft“ vorgestellt: • Mietmodelle und rechtliche Hürden • Neue Geschäftsfelder für die Wohnungswirtschaft • Mieterbefragungen mit Blick auf zukünftige Herausforderungen • Vorstellung von Messdaten und Nutzereinfluss bei Pauschalmiete • Sinnvolle Energieversorgungssysteme für das Mehrfamilienhaus, Status quo bei der Solarthermie und Praxisbeispielen • Alternative Sanierungsstrategien und PV-Fassaden mit Eigennutzung Im vorliegenden Tagungsband sind freigegebene Vorträge sowie einzelne Inhalte des Workshops noch einmal tiefergehend dargestellt. Weitere Informationen zum Workshop sowie zum EVERSOL-Projekt sind auf der Projekthomepage unter https://eversol.iwtt.tu-freiberg.de/workshop-2020.html zu finden.:Liste der Herausgeber .......................................................................................... 5 Danksagung ......................................................................................................... 7 Zusammenfassung ............................................................................................... 9 1. Mit Low Tech zu High Savings – warum reduzierte Gebäudetechnik mit autarkem Energiekonzept im Wohnungsbau die Zukunft ist ............................................... 10 2. Pauschalmieten in der WoWi – ein ökonomisches Anreizmodell? ................... 12 3. Energiekennwerte und Nutzereinfluss zweier teilautarker Mehrfamilienhäuser über 1 ½ Jahre Monitoring .................................................................................. 16 4. Neue Geschäftsfelder für die Wohnungswirtschaft- Möglichkeiten und Chancen am Projektbeispiel Winner .................................................................................. 26 5. Wärmepumpe & PV = sinnvolle Energieversorgung im Mehrfamilienhaus? .... 30 6. Energiesprong – Serielles Sanieren von Mehrfamilienhäusern....................... 42 7. Ergebnisse der Mieterbefragungen der Sonnenhäuser vor dem Hintergrund zukünftiger Smart-Home Gebäude ..................................................................... 46 8. Status quo Solarthermie – Ertragskontrolle und neueste Entwicklungen ....... 52 9. WINNER – Projekt .......................................................................................... 60 10. Solarenergie auf Wohnungsebene – heute die Stadt von morgen bauen ... 64 Fazit und Ausblick Eversol Workshop ................................................................ 66

Hydrocracking and hydrotreating are bitumen upgrading technologies designed to enhance fuel quality by decreasing its density, viscosity, boiling point and heteroatom content via hydrogen addition. The aim of this thesis is to model and simulate an upgrading and integrated gasification combined cycle then to evaluate the feasibility of integrating slurry hydrocracking, trickle-bed hydrotreating and residue gasification using the Aspen HYSYS® simulation software. The close-coupling of the bitumen upgrading facilities with gasification should lead to a hydrogen, steam and power self-sufficient upgrading facility with CO2 capture. Hydrocracker residue is first withdrawn from a 100,000 BPD Athabasca bitumen upgrading facility, characterized via ultimate analysis and then fed to a gasification unit where it produces hydrogen that is partially recycled to the hydrocracker and hydrotreaters and partially burned for power production in a high hydrogen combined cycle unit. The integrated design is simulated for a base case of 90% carbon capture utilizing a monoethanolamine (MEA) solvent, and compared to 65% and no carbon capture scenarios. The hydrogen production of the gasification process is evaluated in terms of hydrocracker residue and auxiliary petroleum coke feeds. The power production is determined for various carbon capture cases and for an optimal hydrocracking operation. Hence, the feasibility of the integration of the upgrading process and the IGCC resides in meeting the hydrogen demand of the upgrading facility while producing enough steam and electricity for a power and energy self-sufficient operation, regardless of the extent of carbon capture.

Hydrocracking and hydrotreating are bitumen upgrading technologies designed to enhance fuel quality by decreasing its density, viscosity, boiling point and heteroatom content via hydrogen addition. The aim of this thesis is to model and simulate an upgrading and integrated gasification combined cycle then to evaluate the feasibility of integrating slurry hydrocracking, trickle-bed hydrotreating and residue gasification using the Aspen HYSYS® simulation software. The close-coupling of the bitumen upgrading facilities with gasification should lead to a hydrogen, steam and power self-sufficient upgrading facility with CO2 capture. Hydrocracker residue is first withdrawn from a 100,000 BPD Athabasca bitumen upgrading facility, characterized via ultimate analysis and then fed to a gasification unit where it produces hydrogen that is partially recycled to the hydrocracker and hydrotreaters and partially burned for power production in a high hydrogen combined cycle unit. The integrated design is simulated for a base case of 90% carbon capture utilizing a monoethanolamine (MEA) solvent, and compared to 65% and no carbon capture scenarios. The hydrogen production of the gasification process is evaluated in terms of hydrocracker residue and auxiliary petroleum coke feeds. The power production is determined for various carbon capture cases and for an optimal hydrocracking operation. Hence, the feasibility of the integration of the upgrading process and the IGCC resides in meeting the hydrogen demand of the upgrading facility while producing enough steam and electricity for a power and energy self-sufficient operation, regardless of the extent of carbon capture.