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This investigation was undertaken to determine the effectiveness of ultrasonic energy in removing spray residue from collards, to determine its effect on the content of ascorbic acid and carotene levels in the treated tissues, and to investigate the influence of ultrasonic energy on the respiratory activity and the histological changes of the tissues involved. / Ph. D.

Ultrasonic techniques were investigated for non-invasive quality evaluation of selected fruits and vegetables. An ultrasonic non-destructive evaluation system was developed and used to investigate physical and acoustical property changes for the selected fruits and vegetables non-invasively. The system included a high power burst pulser, a broadband receiver, a digital storage oscilloscope, two pairs of transducers of 250 kHz and 1 MHz, and a microcomputer system, which was interfaced with the ultrasonic equipment through a General Purpose Interface Board (GPIB), for data acquisition and analysis. Using potatoes and apples, several forms of the acoustic indices were investigated using the system. Investigation of “Yukon-Gold’ potatoes concentrated on the physical and acoustical property changes during the storage period of approximately five months. The tests were conducted at regular intervals. Ultrasonic velocity, attenuation coefficient, modulus of elasticity, and tissue density were determined for each potato along two different orientations — longitudinal and transverse. Three varieties of apples, ‘Golden Delicious’, ‘Red Delicious’, and ‘Granny Smith’, were tested to detect their physiological changes with ripeness. The tests were conducted at two different stages of ripeness. In each test, ultrasonic velocity, attenuation coefficient, modulus of elasticity, and tissue density were determined along longitudinal and radial directions of the apples. Frequency analysis of the transmitted ultrasonic signals through potato and apple samples was also conducted using Fast Fourier Transform (FFT) techniques. The experimental results for the potatoes and apples indicated the measured acoustical and physical properties differed along different orientations; i.e., potato and apple tissues are anisotropic materials. Apple tissues transmitted much lower frequency components than potato tissues and the transmitted frequency range was much narrower due to the much higher percentage of intercellular void space in apple tissues (24%) than in potato tissues (2%). The ultrasonic measurements were able to detect physiological changes and physical heterogeneities in fruit and vegetable tissues. Therefore, the ultrasonic technique can be a useful and quick method for evaluating firmness as well as textural and rheological property changes during storage of fruits and vegetables. Hollow hearts in ‘Atlantic’ potatoes were successfully detected using the ultrasonic nondestructive evaluation system at 250 kHz. A objective this work was to develop a quantitative, non-invasive method for hollow heart detection in potatoes, and to provide information for designing evaluation equipment which could serve as an automatic quality control step in the production process. The analysis of the transmitted ultrasonic signals through the potatoes was carried out in both time and frequency domains. The results of the investigation of ‘Atlantic’ potatoes showed that the waveform of transmitted ultrasonic signals through a hollow heart potato differed significantly from that of a normal potato. Further, the defective potatoes could be separated on the basis of the amount of ultrasonic power transmitted through a potato. By means of digital Fourier analysis, the 0^th spectral moment, M₀, was determined from the power spectral density curve of a transmitted ultrasonic signal. The spectral moment represents the amount of ultrasonic power transmitted through a tested potato, and was chosen as the basis for quantitative, non-invasive method for hollow heart detection, since power transmission of ultrasonic wave was affected by the presence of hollow heart in potatoes. Potatoes with hollow heart transmitted much less ultrasonic power than normal potatoes — approximately 89% less on average. There was a distinct separation between the normal potatoes and hollow heart potatoes. The reliability of this method was confirmed. Among 41 ‘Atlantic’ potatoes tested, all 26 hollow-heart potatoes were identified without exception. Therefore, the parameter M₀ could provide an effective method of analyzing the ultrasonic measurements for quantitative, non-invasive evaluation of hollow hearts in potatoes. This non-invasive method could be used to identify internal quality of potatoes that is difficult to evaluate from external appearance. Such a measurement offers promises for the development of equipment that would sort potatoes with hollow heart automatically. / Ph. D.

El hormigón armado compuesto de cemento Portland fue inventado hace algo más de un siglo aproximadamente y se ha convertido en el material más utilizado en la construcción. La durabilidad de este hormigón es una de las consideraciones más importantes a ser tenidas en cuenta en el diseño de nuevas estructuras y en la evaluación estructural de las ya existentes. Cuando un hormigón sujeto a un ambientes o cargas que puede degradarlo, como puede ser su uso en puentes y ambientes marinos o si contiene grandes cantidades de alúmina o áridos reciclados, el conocimiento o predicción de su durabilidad es una aspecto crítico para su comportamiento en servicio. Los ensayos no destructivos se han mostrado como unos de los ensayos preceptivos con una importancia económica y social más relevante desde que se han aplicado para la auscultación de la durabilidad de las estructuras de hormigón pertenecientes a la ingeniería civil, donde estos materiales son ampliamente utilizados. En cualquier caso, el uso de las técnicas no destructivas en estos materiales no está suficientemente implementado, hecho este motivado por las características heterogéneas de su microestructura. De todos los métodos no destructivos aplicables para el hormigón, el uso de pulsos ultrasónicos es de gran interés para la caracterización de la microestructura y las propiedades de materiales heterogéneos. El objetivo del presente trabajo es obtener un procedimiento de evaluación del ciclo de vida del hormigón preparado y puesto en servicio para ambientes marinos. Además, será estudiado y analizado la incorporación de varias metodologías (destructivas y non destructivas) para caracterizar el proceso de degradación de morteros y hormigones expuestos a disolución de sulfato de sodio y a exposición en disolución de nitrato amónico. Con esta finalidad, una integración adecuada de diferentes técnicas será usada para la caracterización de propiedades y el seguimiento del proceso de degradación que afectan al hormigón. Como objetivos adicionales, destaca que fueron estudiadas las relaciones entre los parámetros destructivos y no destructivos, así como la relación entre los distintos parámetros no destructivos entre sí. Muchos de los estudios anteriores que han usado la inspección ultrasónica las cuáles fueron utilizadas para determinar la relación agua/cemento del mortero, de la pasta de cemento y del hormigón, o para monitorizar los cambios estructurales, para diferentes relaciones a/c, en el proceso de curado. En este trabajo de investigación fue analizado el efecto que tiene para diferentes relaciones a/c en los parámetros ultrasónicos durante el proceso de degradación. Para este objetivo, se utilizaron un Cemento Portland tipo II A L 42.5 (LPC), y otro sulforresistente tipo I 42.5R/SR (SRPC) que fueron usados en la fabricación de dos marcos de hormigón, los cuales fueron utilizados como hormigón en servicio (caso real). Para el estudio del efecto de la variación de a/c en los parámetros ultrasónicos durante la degradación se utilizaron muestras de mortero con deferentes relaciones agua cemento 0.525- 0.45- 0.375 and 0.30 a partir de LPC para obtener diferentes niveles de degradación. Para monitorizar el proceso de degradación se utilizó la inspección por pulso/eco (1 y 3.5 MHz) para la obtención del parámetro del área del perfil de atenuaciones (APA) el cual fue estimado por L Vergara et al., 2003 y usado por Fuente et al, 2004. Para seguir el proceso de curado de pasta de cemento y morteros, este parámetro ha demostrado una alta sensibilidad para caracterizar los cambios microestructurales de materiales derivados del cemento a lo largo de su curado. El método de transmisión se ha utilizado para la determinación de las velocidades de ondas longitudinales con la frecuencia de 1MHz y transversales con la frecuencia de 500 kHz. La velocidad ultrasónica también ha demostrado la capacidad para seguir los cambios microestructurales de un modo sencillo porque dicho parámetro está relacionado con la variación de las propiedades mecánicas, y bajo ciertas premisas, con la variación de la porosidad. El análisis con la imagen ultrasónica con 2 MHz fue también usada para la consecución de los mismos objetivos. Como métodos destructivos, los ensayos de resistencia a la compresión y flexión fueron los utilizados para determinar la pérdida de actividad resistente de morteros y hormigones, y la porosidad conectada al agua para analizar los cambios en la matriz porosa por el efecto de la difusión de elementos agresivos que penetran en el material provocando su degradación. La porosimetría de mercurio (MIP) fue usada para observar las variaciones del volumen y tamaño de poro y, por último, la microscopía electrónica de barrido (MEB) que fue utilizada para cuantificar y detectar los cambios en la microestructura por el ataque de elementos agresivos. Los resultados obtenidos muestran que, la degradación producida por exposición a sulfato de sodio, tiene dos etapas, en la primera etapa se forma la etringita que llena los poros pero que no produce microfisuración. En esta etapa se observó una variación en los parámetros obtenidos por ejemplo, incremento de la velocidad de la onda ultrasónica, de las resistencias a compresión y a la flexión o la disminución de la porosidad. Esta variación en los parámetros podría indicar una mejora en las prestaciones mecánicas del material objeto de la investigación, pero en realidad esto no es cierto porque los poros están llenos de etringita, provocando una expansión, que es la causa de la degradación en la segunda etapa. En dicha segunda etapa, se produce una microfisuración generalizada por la expansión de la etringita e incrementando su volumen dentro de los poros. Este hecho produjo un cambio en los parámetros medidos que contrastan con la evolución en la primera etapa, disminución de la velocidad de las ondas ultrasónicas, y de las resistencias mecánicas y consecuentemente un aumento de la porosidad. Por otro lado, la degradación por ataque de nitrato amonio tiene una única etapa debida al proceso de descalificación que comienza desde el principio del proceso de exposición y es lineal durante todo el periodo de exposición. Para ambos casos, la integración de las diversas técnicas se revela como satisfactoria para el seguimiento del proceso de degradación, encontrando buenas correlaciones entre los parámetros no destructivos y los parámetros destructivos de técnicas de análisis físico-químico. / Mahmoud, TI. (2013). Evaluation of the degradation process of cement-based materials exposed to aggressive environment by using ultrasonic techniques and physical characterisation [Tesis doctoral]. Universitat Politècnica de València. https://doi.org/10.4995/Thesis/10251/27550

A technique for calculating bulk ultrasonic fields which uses implicit difference equations to evaluate the parabolic approximation to the Helmholtz equation is described. The parabolic approximation assumes that the field varies much faster in the transverse directions than in the direction of propagation and results in a partial differential equation which is formulated as a pure i initial value problem . Finite difference equation descriptions are derived for one-dimensional, cylindrically symmetric problems and for more general two-dimensional problems. A Fourier stability analysis is performed on the simpler numerical scheme to determine acceptable values for parameters such as the grid spacing and increment step sizes. Several example calculations for each geometry are presented to demonstrate the usefulness of this parabolic-difference equation technique in transducer modeling. Included in these examples are gaussian, rectangular, circular, and concentric ring amplitude distributions, as well as uniform and focused phase distributions. In many cases, qualitative agreement between the numerical results and analytic diffraction theory predictions can be observed. An experimental system is developed for the detection of acoustic fields in water using a dual beam differential interferometer which is scanned through a large tank. The output from this system is proportional to the average difference in refractive index sampled by the two beams and is effectively integrated along the path of the beams through the specimen. An algorithm is presented which reconstructs a radial profile of the measured field from the integrated data assuming cylindrical symmetry. Raw, averaged, and reconstructed data is given for scans taken in the far-field of a circular, uniform transducer. / M.S.

The performance of two acoustooptical systems for ultrasonic materials characterization has been investigated. The first system uses an optical fiber interferometric technique to detect directly slowly varying residual stresses and both high frequency continuous and transient ultrasonic waves characteristic of acoustic emission events in composites. The potential for embedding optical fibers inside fiber composites during manufacturing makes this an attractive built-in alternative to conventional contact transducers for the nondestructive evaluation of composite materials. Experimental static and dynamic calibration as well as the frequency domain characterization of acoustic emission as detected by this system are discussed. The second system is a pulse-echo transducer system that generates an electronically focusable ultrasonic field and detects the reflected field optically. The generating transducer consists of concentric ring electrodes etched on a single x-cut quartz crystal substrate with a 1 mm circular aperture at the center. By shaping the amplitude and phase profile of the high voltage pulse applied to each ring, a focused ultrasonic field results at an adjustable distance below the transducer. If the field is focused below the surface of a specimen, energy in the wave reflected from the focal point modulates the normal and parallel components of surface displacement. Furthermore, if the sample arm of an adaptively stabilized interferometer is focused on the free surface at the transducer center aperture, the normal component of surface motion may be detected. This system has potential applications in materials characterization and evaluation as well as biomedical imaging. The design of the system is discussed with particular emphasis on the necessary sub-system interfaces required for operational flexibility. / Master of Science

A presentation is given of an acousto-ultrasonic system for the evaluation of composite materials. First, a brief statement will be made on the acousto-ultrasonic technique and its relative worth compared to other nondestructive testing techniques as applied to composite materials. The following two chapters describe the system instrumentation and system software, respectively. Next, comments are given regarding the implementation of the system for research on graphite/epoxy laminates, with additional remarks concerning efforts to evaluate aluminum/graphite tubes with the system. This includes physical descriptions of the composite systems. Subsequently, results are presented comparing parameters and forms of presentation which can be employed to relate results. Finally, conclusions are made on the application of the acousto-ultrasonic system to nondestructive testing of composite materials, with specific results on its application to graphite/epoxy plates. More specifically, comments are made on the variation of SWF factors with azimuthal angle on the graphite/epoxy plates, the identification of specific frequency peaks, and the relationships these may have to certain modes of vibration and material properties. For example, a low frequency mode was found to vary in a manner reminiscent of E_x and to show characteristics of an extensional Lamb wave. In general, results are presented and discussed in order to show how the system can be implemented to gain physical information on composite materials, such as the property of anisotropy. / Master of Science

This investigation was conducted to provide laboratory scale equipment that will facilitate an accurate study of the affect of ultrasonic energy on mass transfer in two-phase multiple-component liquid systems. A liquid-liquid extractor incorporating an ultrasonic generator and transducer was designed and constructed to the following specifications: (1) insonation frequency of 400 kilocycles per second, (2) insonation intensities equivalent to plate currents of 0 to 200 milliamperes, and (3) flow rate of solvent and feed through the reactor ranging approximately from one-half to 24 pounds per minute, in varying solvent-to-feed ratios. A special glass reactor, or contactor, was constructed from a standard, 60° pyrexx glass funnel and fitted with an acoustical window of 0.001-inch sheet nickel. Photographic studies were made of the two-phase mixing taking place inside the reactor in both the presence and absence of ultrasonic insonation. An all metal reactor, of the same general design as the glass reactor, was constructed for use with the extractor when investigations were to be made that would involve high pressures or sudden liquid surges through the reactor. An evaluation of the extractor was conducted employing the system moetons-water-1,1,2-trichloroethane. Stage efficiencies calculated for the individual tests, eleven in all, varied from 94.3 to 110.0 percent. An observed yellow color in the extract samples, probably due to dissolved impurities in the 1,1,2-trichloroethane, could have been responsible for the observation of refractive index readings that did not give true representation of the acetone concentration of the sample. Cavitation was observed in the reactor which the test system was undergoing ultrasonic insonation. The gross stirring effects resulting from cavitation in the liquids caused a mixing of the two phases that was more intense than that taking place in the reactor without insonation. / Master of Science