The performance of fused fiber couplers is wavelength dependent. Wavelength spectral compensation is a technique to decrease the effect of the wavelength dependence, which is an essential task for many applications in fiber optic communication systems. Fiber devices such as wavelength-flattened couplers (WFCs) can be fabricated using wavelength spectral compensation methods. In this dissertation, wavelength spectral compensation techniques in fused biconical taper (FBT) couplers including both multimode and single-mode fiber couplers are studied in detail. In multimode fiber coupler operation, a novel theoretical model based on frustrated total internal reflection (FTIR) has been developed to effectively describe the power coupling and loss mechanism. Experimental results support the theoretical predictions. In single-mode fiber couplers, the conventional technique of fabricating WFCs is discussed. An alternative analytical model has been developed based upon coupled mode theory, which provides a relatively simple and mathematically sound explanation to the wavelength spectral compensation. Aiming to simplify WFC fabrication, a new way of constructing WFCs is proposed and demonstrated by connecting regular single-mode fiber couplers, some of which serve as wavelength spectral compensators. WFCs of various structures including 2x2, 1x3, 1x2ᴺ, and 4x4 have been developed, and the experimental data agree with theoretical predictions of performance. Potential applications and future research directions in wavelength spectral compensation are also presented. / Ph. D.

A novel fiber optic structure, termed stochastic ordered hole fibers, has been developed that contains an ordered array of six hollow tubes surrounding a hollow core, combined with a nanoporous glass creating a unique fully three dimensional pore/fiber configuration. The objective of this study is to increase the functionality of these stochastic ordered hole fibers, as well as porous clad fibers, by integrating electronic device components such as conductors, and semiconductors, and optically active materials on and in the optical fiber pore structures. Conductive copper pathways were created on/in the solid core fibers using an electroless deposition technique. A chemical vapor deposition system was built in order to attempt the deposition of silicon in on the porous clad fibers. Additionally, conductive poly(3,4-ethylenedioxythiophene)- poly(styrene sulfonate) (PEDOT:PSS) and photoactive polymer blend poly(3- hexylthiophene) and 1-(3-methoxycarbonyl)-propyl-1-phenyl-)6,6)C61 (P3HT: PCBM) were deposited on the fibers using dip coating techniques. Quantum dots of Cadmium Selenide (CdSe) with particle sizes of ranging from 2- 10 nm were deposited in the stochastic ordered hole fibers. SEM and EDS analysis confirm that copper, polymer materials, and quantum dots were deposited in the pore structure and on the surface of the fibers. Finally, resistance measurements indicate that the electrolessly deposited copper coatings have sufficient conductivity to be used as metallic contacts or resistive heating elements. / Master of Science

The electrostatic self-assembly (ESA) method presents an effective application in the field of biosensing due to the uniform nanoscale structure. In previous research, a single mode fiber (SMF) sensor system had been investigated for the thin-film measurement due to the high fringe visibility. However, compared with a SMF sensor system, a multimode fiber (MMF) sensor system is lower-cost and has larger sensing area (the fiber core), providing the potential for higher sensing efficiency. In this thesis, a multimode fiber-optic sensor has been developed based on extrinsic Fabry-Perot interferometry (EFPI) for the measurement of optical thickness in self-assembled thin film layers as well as for the immunosensing test. The sensor was fabricated by connecting a multimode fiber (MMF) and a silica wafer. A Fabry-Perot cavity was formed by the reflections from the two interfaces of the wafer. The negatively charged silica wafer could be used as the substrate for the thin film immobilization scheme. The sensor is incorporated into the white-light interferometric system. By monitoring the optical cavity length increment, the self-assembled thin film thickness was measured; the immunoreaction between immunoglobulin G (IgG) and anti-IgG was investigated. / Master of Science

Elevators are a necessary component of the modern urban and suburban life. The guide rails the car and counterweight move on are the most sensitive parts when it comes to de-habilitating damage that can be caused by an earthquake. Conventional sensors are becoming obsolete in sensing for today's multistory buildings because they don't monitor the structural health of the guide rails. This sensing task falls into the fiber sensing niche market because of a fiber sensor's ability to be multiplexed. Previous work by Taplin and Jackson showed demodulation of the interference spectrum of two Fabry-Perot cavities using Fourier analysis. The goal of this research is to use Fourier analysis to demodulate the spectrum of four multiplexed extrinsic Fabry-Perot fiber interferometers for strain measurements. Comparisons of fiber, foil, and theoretical strains are made. Also, experiments showing the system's air-gap stability and crosstalk are provided. / Master of Science

High voltage power transformer is one of the most important and expensive components in today's power transmission and distribution systems. Any overlooked critical fault generated inside a power transformer may lead to a transformer catastrophic failure which could not only cause a disruption to the power system but also significant equipment damage. Accurate and prompt information on the health state of a transformer is thus the critical prerequisite for an asset manager to make a vital decision on a transformer with suspicious conditions. Partial discharge (PD) is not only a precursor of insulation degradation, but also a primary factor to accelerate the deterioration of the insulation system in a transformer. Monitoring of PD activities and the concentration of PD generated combustible gases dissolved in the transformer oil has been proven to be an effective procedure for transformer health state estimation. However current commercially available sensors can only be installed outside of transformers and offer indirect or delayed information. This research is aimed to investigate and develop several sensor techniques for transformer health monitoring. The first work is an optical fiber extrinsic Fabry-Perot interferometric sensor for PD detection. By filling SF6 into the sensor air cavity of the extrinsic Fabry-Perot interferometer sensor, the last potential obstacle that prevents this kind of sensors from being installed inside transformers has been removed. The proposed acoustic sensor multiplexing system is stable and more economical than the other sensor multiplexing methods that usually require the use of a tunable laser or filters. Two dissolved gas analysis (DGA) methods for dissolved hydrogen or acetylene measurement are also proposed and demonstrated. The dissolved hydrogen detection is based on hydrogen induced fiber loss and the dissolved acetylene detection is by direct oil transmission measurement. / Ph. D.

From the monitoring of deep ocean conditions to the imaging and exploration of the vast universe, optical sensors are playing a unique, critical role in all areas of scientific research. Optical fiber sensors, in particular, are not only widely used in daily life such as for medical inspection, structural health monitoring, and environmental surveillance, but also in high-tech, high-security applications such as missile guidance or monitoring of aircraft engines and structures. Measurements of physical parameters are required in harsh environments including high pressure, high temperature, highly electromagnetically-active and corrosive conditions. A typical example is fossil fuel-based power plants. Unfortunately, current optical fiber sensors for high-temperature monitoring can work only for single point measurement, as traditional fully-distributed temperature sensing techniques are restricted for temperatures below 800°C due to the limitation of the fragile character of silica fiber under high temperature. In this research, a first-of-its-kind technology was developed which pushed the limits of fully distributed temperature sensing (DTS) in harsh environments by exploring the feasibility of DTS in optical sapphire waveguides. An all sapphire fiber-based Raman DTS system was demonstrated in a 3-meters long sapphire fiber up to a temperature of 1400°C with a spatial resolution of 16.4cm and a standard deviation of a few degrees Celsius. In this dissertation, the design, fabrication, and testing of the sapphire fiber-based Raman DTS system are discussed in detail. The plan and direction for future work are also suggested with an aim for commercialization. / Ph. D.

Since the invention of Laser (in 1960) and low loss optical fiber (in 1966) [1], extensive research in fiber-optic sensing technology has made it a well-defined and matured field [1]. The measurement of physical parameters (such as temperature and pressure) in extremely harsh environment is one of the most intriguing challenges of this field, and is highly valued in the automobile industry, aerospace research, industrial process monitoring, etc. [2]. Although the semiconductor based sensors can operate at around 500oC, sapphire fiber sensors were demonstrated at even higher temperatures [3]. In this research, a novel sensor structure is proposed that can measure both pressure and temperature simultaneously. This work effort consists of design, fabrication, calibration, and laboratory testing of a novel structured temperature compensated pressure sensor. The aim of this research is to demonstrate an accurate temperature measurement, and pressure measurement using a composite Fabry-Perot interferometer. One interferometer measures the temperature and the other accurately measures pressure after temperature compensation using the temperature data from the first sensor. / Master of Science

Due to their compact size, sensitivity, and ability to be multiplexed, intrinsic Fabry-Perot interferometers (IFPIs) are excellent candidates for almost any multi-point temperature or strain application, and it is well-known that using a single-mode lead-in fiber, a multi-mode fiber section as the Fabry-Perot cavity, and an additional single-mode fiber as the tail results in a structure that generates strong interference fringes while remaining robust. Though the basic principles behind these sensors are understood, to the best of the author's knowledge there hasn't been a thorough investigation into the design and fabrication of a chain of multiplexed IFPI sensors for industrial use in an environment where serious issues associated with the size of the test coupon, sensor placement, and mechanical reinforcement of the fiber could arise. This thesis details the preparation and results of this investigation. It turns out that fabricating a sensor chain with appropriate sensor spacing and excellent temperature response characteristics proved a significant challenge, and issues addressed include inter-sensor interference, high-temperature mechanical reinforcement for bare fiber sections, and high bending losses. After overcoming these problems, a final sensor chain was fabricated and characterized. This chain was then subjected to a battery of tests at the National Energy Technology Laboratory (NETL), where four multiplexed sensors were installed on a 2â x2â coupon in a simulated gas turbine environment. Final results are presented and analyzed. The work that went into developing this chain lays the foundation for future efforts in developing quasi-distributed temperature sensors by identifying potential obstacles and fundamental limitations for certain approaches. / Master of Science

A technology for fabricating fiber optic pressure sensors is described. This technology is based on intermediate-layer bonding of a fused silica ferrule to a patterned, micro-machined fused silica diaphragm, providing low temperature fabrication of optical pressure sensor heads that can operate at high temperature. Fused silica ferrules and fused silica diaphragms are chosen to reduce the temperature dependence. The fused silica diaphragms have been micro-machined using wet chemical etching in order to form extrinsic Fabry-Perot (FP) interferometric cavities. Sol-gel is used as an intermediate-layer for both fiber-ferrule bonding and ferrule-diaphragm bonding at relatively low temperature (250 °C). The pressure sensors fabricated in the manner can operate at temperatures as high as 600 °C. The self-calibrated interferometric-intensity-based (SCIIB) technology, which combines fiber interferometry and intensity-based sensing method into a single sensor system, is used to test and monitor the pressure sensor signal. The light returned from the FP cavity is split into two channels. One channel with longer coherence length can test the effective interference generated by the FP cavity, while the other channel with shorter coherence length can get signal proportional only to the source power, fiber attenuation, and other optical losses. The ratio of the signals from the two channels can compensate for all unwanted factors, including source power variations and fiber bending losses. [11] / Master of Science

Force and moment balances have proved to be essential in the measurement and calculation of aerodynamic properties during wind tunnel testing. With the recent advancements of technology, new fiber optic sensors have been designed to replace the conventional foil strain gage sensors commonly found on balances, thereby offering several distinct advantages. The use of fiber optic sensors on a balance brings with it some potential advantages over conventional strain gage balances including increased resolution and accuracy, insensitivity to electromagnetic interference, and the capability of use at high temperatures. By using the fiber optic sensors, some of the limitations of the conventional balance can be overcome, leading to a better overall balance design. This thesis considers an initial trial application of new fiber optic sensors on a conventional, six-component sting balance while retaining the original foil strain gage sensors for comparison. Tests were conducted with a blunt, 10º half-angle cone model in the Virginia Tech 9x9 inch Supersonic Wind Tunnel at Mach 2.4 with a total pressure of 48 psia and ambient total temperature of 25.3ºC. Results showed a close comparison between the foil strain gages and the fiber optic sensor measurements, which were set up to measure the normal force and pitching moment on the blunt cone model. A Finite Element Model (FEM) of the sting balance was produced in order to determine the best locations for the fiber optic sensors on the sting balance. Computational Fluid Dynamics (CFD) was also used in order to predict and compare the results acquired from all of the sensors. / Master of Science