Cette thèse est une tentative vers la conception de la bande Ka émetteur-récepteur RF pour les réseaux de capteurs sans fil (WSN), pour lesquelles la consommation d'énergie, le coût et la taille sont des paramètres critiques. Au sens de la consommation d'énergie, un transmetteur RF est la partie la plus cruciale d'un nœud de capteur. Nous avons choisi STMicroelectronics 90nm global purpose (GP) pour atteindre la technologie CMOS à faible puissance, faible coût et de petite taille. Pour la première fois, nous avons introduit la bande Ka dans le context de WSN, a fin de bénéficier de l'immunité élevée du réseau et la petite taille antenne. Étant donné que la technologie que nous avons choisi et du kit associé fonderie de conception n'est pas pour la conception RF, nous avons été obligés de mettre au point un outil de conception individuelle pour la bande à ondes millimétriques. De cette façon, nous avons développé une solution simple et précise le modèle MOS transistor, comprenant charge et le modèle de capacité, modèle de bruit et le modèle complet des effets parasites. Nous avons proposé une nouvelle structure pour les inducteurs de la ligne de transmission et un modèle précis de RLGC a été développé pour la conception et la simulation de ces inducteurs. Et puis par la simulation de la pleine d'onde (full wave) électromagnétique dans le logiciel HFSS, nous avons extrait des parameters du modele d'incucteurs , et d'autres éléments passifs, telles que des pads RF et T-jonctions. Comme notre première expérience, nous avons conçu et optimisé une LNA à 30 GHz, en utilisant notre outil de conception. Le LNA conçu a été fabriqué dans STMicroelectronics 90nm global dans le processus de GP CMOS et a été mesurée dans le laboratoire IMEP. Les résultats des mesures montrent 10dB gain de puissance et de 4,8 dB figre bruit (noise figure) avec 4mW DC la consommation de puissance. Dans l'étape suivante, nous avons conçu et optimisé mieux 30GHz LNA. La simulation post-layout montre 13.9dB gain de puissance et 3.6d figre bruit, avec seulement 3 mW de consommation de puissance. Nous avons proposé un lien simple radio et un structure simple a ete presente pour le récepteur_émetteur. Dans le récepteur, nous avons utilisé la structure hétérodyne, ou dans la quelle nous avons utilise de l'idee de Mixer Harmonique paire et oscillateur couple, à surmonter de nombreux problèmes se pose en mm bande des ondes dans la technologie CMOS. Le Mixer a été conçu en utilisant les résultats d'analyse et de simulation dans le kit de conception de fonderie: 4dB gain de conversion et de 5,8 double side band figre de bruit avec 2.2Mw consommation de puissance, un excellent résultat en comparaison avec les œuvres similaires rapports comme IF Stage 2GHz qui a été conçu comme multi-slice-amplificateur de la chaîne de detection pour accroître (ugmenter)la performance du récepteur et d'atteindre plus faible consommation d'énergie. Enfin, le récepteur a été simulé dans MATLAB et--87dBm de sensibilité, 890KHz de bande passante, avec 6.65mW consommation d'énergie sont obtenus. L'émetteur a été conçu aussi simple que possible, en utilisant idée power oscillateur, délivrant 6mW puissance RF de l'antenne. L'émetteur a généralement les 25% de power efficacité qui est très bon résultat en comparaison avec les œuvres déclarées.

<p>The current consumption of the IQ modulator is a significant part of the totalcurrent consumption of a mobile transmitter platform and reducing it is of greatinterest. Also, as the WCDMA/LTE standards specifies full duplex transmissionsand Tx and Rx are most often using the same antenna, it is crucial to have asolution with low noise generation. Two new proposals have been studied with theaim to reduce the current consumption and noise contribution of the IQ modulator.</p><p>A current mode envelope tracking IQM is the first of the studied designs. Thisimplementation lowers the bias currents in the circuit in relation to the amplitudeof the baseband input signals, meaning that a low input amplitude results in alowering of the current consumption. It proves to be very efficient for basebandsignals with a high peak-to-average ratio. Simulations and calculations have shownthat an average current reduction of 56 % can be achieved for an arbitrary LTEbaseband signal.</p><p>The second is an entirely new passive mixer design where the baseband voltagesare sequentially copied to the RF node, removing the need for V-to-I conversion inthe mixer which reduces current consumption and noise. Results from simulationshas proven that this design is fully capable of improving both current consumptionas well as the noise levels. With an output power of 4.0 dBm, the power consumptionwas 43.3 mW, including clock generating circuits. This, combined with thefact that the design is small and simple, means that there is definitely a possibilityto replace the present IQM design with a passive mixer.</p>

Advances toward increased integration and complexity of radio frequency (RF) andmixed-signal integrated circuits reduce the effectiveness of contemporary testmethodologies and result in a rising cost of testing. The focus in this research is on thecircuit-level implementation of alternative test strategies for integrated wirelesstransceivers with the aim to lower test cost by eliminating the need for expensive RFequipment during production testing.The first circuit proposed in this thesis closes the signal path between the transmitterand receiver sections of integrated transceivers in test mode for bit error rate analysis atlow frequencies. Furthermore, the output power of this on-chip loopback block wasmade variable with the goal to allow gain and 1-dB compression point determination forthe RF front-end circuits with on-chip power detectors. The loopback block is intendedfor transceivers operating in the 1.9-2.4GHz range and it can compensate for transmitterreceiveroffset frequency differences from 40MHz to 200MHz. The measuredattenuation range of the 0.052mm2 loopback circuit in 0.13µm CMOS technology was 26-41dB with continuous control, but post-layout simulation results indicate that theattenuation range can be reduced to 11-27dB via optimizations.Another circuit presented in this thesis is a current generator for built-in testing ofimpedance-matched RF front-end circuits with current injection. Since this circuit hashigh output impedance (>1k up to 2.4GHz), it does not influence the input matchingnetwork of the low-noise amplifier (LNA) under test. A major advantage of the currentinjection method over the typical voltage-mode approach is that the built-in test canexpose fabrication defects in components of the matching network in addition to on-chipdevices. The current generator was employed together with two power detectors in arealization of a built-in test for a LNA with 14% layout area overhead in 0.13µm CMOStechnology (<1.5% for the 0.002mm2 current generator). The post-layout simulationresults showed that the LNA gain (S21) estimation with the external matching networkwas within 3.5% of the actual gain in the presence of process-voltage-temperaturevariations and power detector imprecision.

Many scientists and engineers are turning to lab-on-a-chip systems for cheaper and high throughput analysis of chemical reactions and biomolecular interactions. In this work, we developed several lab-on-a-chip modules based on novel manipulations of individual microbeads inside microchannels. The first manipulation method employs arrays of soft ferromagnetic patterns fabricated inside a microfluidic channel and subjected to an external rotating magnetic field. We demonstrated that the system can be used to assemble individual beads (1-3µm) from a flow of suspended beads into a regular array on the chip, hence improving the integrated electrochemical detection of biomolecules bound to the bead surface. In addition, the microbeads can follow the external magnet rotating at very high speeds and simultaneously orbit around individual soft magnets on the chip. We employed this manipulation mode for efficient sample mixing in continuous microflow. Furthermore, we discovered a simple but effective way of transporting the microbeads on-chip in the rotating field. Selective transport of microbeads with different size was also realized, providing a platform for effective sample separation on a chip. The second manipulation method integrates magnetic and dielectrophoretic manipulations of the same microbeads. The device combines tapered conducting wires and fingered electrodes to generate desirable magnetic and electric fields, respectively. By externally programming the magnetic attraction and dielectrophoretic repulsion forces, out-of-plane oscillation of the microbeads across the channel height was realized. Furthermore, we demonstrated the tweezing of microbeads in liquid with high spatial resolutions by fine-tuning the net force from magnetic attraction and dielectrophoretic repulsion of the beads. The high-resolution control of the out-of-plane motion of the microbeads has led to the invention of massively parallel biomolecular tweezers.

This thesis conducts numerical and experimental studies of the nonlinear electrokinetic motion of heterogeneous particles in microfluidic systems and their corresponding applications in laboratory-on-a-chip (LOC) systems. Induced-charge electrokinetic (ICEK) phenomena flow is generated by applying an external electric field to a conducting particle immersed in an aqueous solution. As a result of this field, micro-vortices form around the conducting particle. Using this phenomenon, many shortcomings of classical electrokinetics (e.g. poor mixing, leakage, back flow problem) can be improved. This thesis proposes and investigates a complete 3-D numerical multi-physics method to calculate the induced zeta potential on the conducting surface of a heterogeneous object. To model the ICEK motion of a heterogeneous particle in a DC electric field, the moving grid technique is used to conduct the particle-fluid simulation. It was numerically shown that the vortices form near the conducting surface of a particle. Both transitional and rotational motions of heterogeneous particles are investigated. A set of novel experiments are designed and conducted to investigate several aspecs of ICEK. It is demonstrated for the first time that four vortices form around a conducting sphere in contact with an aqueous solution while the DC electric field is applied. The motions of heterogeneous particles are experimentally studied. The speed of a heterogeneous particle is compared with the same size non-conducting particle under the same experimental conditions and it is shown that the heterogeneous particle moves significantly faster than the non-conducting particle. It is also shown that the micro-vortices on the conducting section of the heterogeneous particle act like an engine and push the particle to move faster. These experiments verify the results of our simulation studies. We introduce three applications for induced-charge electrokinetic phenomena in ths thesis: ICEK micro-valve, ICEK micro-mixer, and ICEK micro-motor, which can be used in microfluidics and lab-on-a-chip devises. This ICEK micro-valve significantly improves many shortcomings of other micro-valves reported in the literature (such as leakage, considerable dead volume and complicated fabrication processes). Our ICEK micro-mixers take the advantages of induced micro-vortices and boost the mixing process in a micro-channel. As a result well mixed homogeneous (100%) mixture could be obtained at the downstream of the mixer. Our proposed no-contact ICEK micro-motor rotates as long as the DC electric field is being applied. This thesis develops a new understanding of several ICEK phenomena and applications related to heterogeneous particles. The 3D numerical model developed in this thesis along with the experimental studies are capable of describing the ICEK motion of a heterogeneous particle and is a considerable step to calculate the ICEK phenomena for real-world applications. This thesis, for the first time, experimentally visualized and verified the induced micro-vortices around conducting particles under applied DC electric field. The proposed ICEK micro-mixers, valve and motor can be used in various LOC devices and applications.

In this study, we were particularly interested in looking at the possibility that cross metathesis of olefins in melt phase could be used to produce polydimethylsiloxane (PDMS) modified polypropylene (PP). The intention of this project was also to study and quantify relationships among the main experimental factors in the reaction: temperature, catalyst concentration and molar ratio of PP to PDMS, through a 2-level factorial statistical design. In order to examine if PP-PDMS copolymers were synthesized in the melt phase, measurement of the chemical, physical and viscoelastic properties of the synthesized copolymers was necessary. Techniques including proton (¹H)-nuclear magnetic resonance (NMR), differential scanning calorimetry (DSC), thermal gravimetric analysis (TGA), rheometry and scanning electron microscopy (SEM), were all used to characterize the synthesized copolymers. ¹H NMR measurements confirmed the presence of PDMS in the copolymers. They also provided a quantitative measurement of PP to PDMS molar ratio in copolymers by determining the integration of PP PDMS repeating unit signals in NMR spectra. Compared to virgin PP, a lower melting enthalpy of the PP phase in the copolymer was observed from DSC results. This implied that the PDMS component influenced the thermal behavior of the PP crystalline phase in the copolymers. Moreover, TGA measurements indicated that a higher thermal stability was obtained for PP-PDMS copolymers than that for virgin PP wax and this was expected since PDMS is known for its excellent stability at high temperature. Rheological analysis showed that the presence of PDMS in the copolymers gave lower complex viscosities and loss moduli, but higher storage moduli than those for virgin PP. Furthermore, the morphology of copolymers was examined by SEM and elemental analysis at the surface using an energy dispersive X-ray (EDX) analyzer on the SEM. It was found that micrographs of copolymers showed round domains on the surface, which were not observed in virgin PP wax and those round segments were confirmed to contain silicon. Torque values used in a batch mixer for polymerizations and the remaining weight % of copolymers at 350°C were used to conduct statistical analysis, through which models used to describe the relationships between experimental factors and these physical responses were determined.

Advances toward increased integration and complexity of radio frequency (RF) andmixed-signal integrated circuits reduce the effectiveness of contemporary testmethodologies and result in a rising cost of testing. The focus in this research is on thecircuit-level implementation of alternative test strategies for integrated wirelesstransceivers with the aim to lower test cost by eliminating the need for expensive RFequipment during production testing.The first circuit proposed in this thesis closes the signal path between the transmitterand receiver sections of integrated transceivers in test mode for bit error rate analysis atlow frequencies. Furthermore, the output power of this on-chip loopback block wasmade variable with the goal to allow gain and 1-dB compression point determination forthe RF front-end circuits with on-chip power detectors. The loopback block is intendedfor transceivers operating in the 1.9-2.4GHz range and it can compensate for transmitterreceiveroffset frequency differences from 40MHz to 200MHz. The measuredattenuation range of the 0.052mm2 loopback circuit in 0.13µm CMOS technology was 26-41dB with continuous control, but post-layout simulation results indicate that theattenuation range can be reduced to 11-27dB via optimizations.Another circuit presented in this thesis is a current generator for built-in testing ofimpedance-matched RF front-end circuits with current injection. Since this circuit hashigh output impedance (>1k up to 2.4GHz), it does not influence the input matchingnetwork of the low-noise amplifier (LNA) under test. A major advantage of the currentinjection method over the typical voltage-mode approach is that the built-in test canexpose fabrication defects in components of the matching network in addition to on-chipdevices. The current generator was employed together with two power detectors in arealization of a built-in test for a LNA with 14% layout area overhead in 0.13µm CMOStechnology (<1.5% for the 0.002mm2 current generator). The post-layout simulationresults showed that the LNA gain (S21) estimation with the external matching networkwas within 3.5% of the actual gain in the presence of process-voltage-temperaturevariations and power detector imprecision.

Today, the advances in Complementary MetalOxideSemiconductor (CMOS) technology have guided the progress in the wireless communications circuits and systems area. Various new communication standards have been developed to accommodate a variety of applications at different frequency bands, such as cellular communications at 900 and 1800 MHz, global positioning system (GPS) at 1.2 and 1.5 GHz, and Bluetooth andWiFi at 2.4 and 5.2 GHz, respectively. The modern wireless technology is now motivated by the global trend of developing multi-band/multistandard terminals for low-cost and multifunction transceivers. Exploring the unused 10-66 GHz frequency spectrum for high data rate communication is also another trend in the wireless industry. In this dissertation, the challenges and solutions for designing a multi-band/multistandard mobile device is addressed from system-level analysis to circuit implementation. A systematic system-level design methodology for block-level budgeting is proposed. The system-level design methodology focuses on minimizing the power consumption of the overall receiver. Then, a novel millimeter-wave dual-band receiver front-end architecture is developed to operate at 24 and 31 GHz. The receiver relies on a newly introduced concept of harmonic selection that helps to reduce the complexity of the dual-band receiver. Wideband circuit techniques for millimeterwave frequencies are also investigated and new bandwidth extension techniques are proposed for the dual-band 24/31 GHz receiver. These new techniques are applied for the low noise amplifier and millimeter-wave mixer resulting in the widest reported operating bandwidth in K-band, while consuming less power consumption. Additionally, various receiver building blocks, such as a low noise amplifier with reconfigurable input matching network for multi-band receivers, and a low drop-out regulator with high power supply rejection are analyzed and proposed. The low noise amplifier presents the first one with continuously reconfigurable input matching network, while achieving a noise figure comparable to the wideband techniques. The low drop-out regulator presented the first one with high power supply rejection in the mega-hertz frequency range. All the proposed building blocks and architecture in this dissertation are implemented using the existing silicon-based technologies, and resulted in several publications in IEEE Journals and Conferences.

The aim of this study is to design a mixer with appropriate parts for uniform treatment of the material in household microwave ovens which can not be achieved with the turntable. The designed mixer&rsquo / s performance was tested by the help of color and surface temperature values. In the design of the mixer primarily mixing in the vertical and radial directions were sought and for this purpose blades and wings for directing the material especially in these directions were present. The rotational motion of the mixer was provided by a shaft actuated by the motor of the turntable where the motor was replaced by a speed adjustable one. Couscous macaroni beads wetted with CoCl2 solution were dried for processing in the microwave oven. The initial color values of the samples were L*= 52.0&plusmn / 0.35, a*= 8.8&plusmn / 0.21 and b*= 14.1&plusmn / 0.11 . The studied parameters were microwave power level (10%, 40%, 67% and 100% ), processing time (60,90, 120 sec), speed of rotation of the mixer (5,10,15 rpm) , location (4up, 4bt, 6up, 6bt) for the cases of with and without the mixer. v The macaroni beads were well arranged in a mixing container and then put into the microwave oven for operation. Same parameters with coloring experiments were used for the surface temperature determination. After operation the container was photographed by an IR camera. Whether the designed mixer was present or not, average a* and b* values decreased while temperature increased . All these values were significantly affected by the time and power increase. The L* value became an insignificant parameter to decide for the performance Location of the particles in the container appeared as a significant parameter affecting the a*, b* and temperature values without the mixer whereas, with the use of the mixer it became an insignificant parameter indicating uniform energy distribution. Speed of rotation of the mixer was a significant parameter for both cases. However, the color values obtained did not show the same trend with mixer which it showed without mixer. It is concluded that the designed mixer is effective in providing homogeneity of the product by providing sufficient mixing in the container hence the particles can receive about equal energy. Keywords: Microwave oven, particulate solids, mixing, mixer design, testing performance, uniform treatment

In this study, we were particularly interested in looking at the possibility that cross metathesis of olefins in melt phase could be used to produce polydimethylsiloxane (PDMS) modified polypropylene (PP). The intention of this project was also to study and quantify relationships among the main experimental factors in the reaction: temperature, catalyst concentration and molar ratio of PP to PDMS, through a 2-level factorial statistical design. In order to examine if PP-PDMS copolymers were synthesized in the melt phase, measurement of the chemical, physical and viscoelastic properties of the synthesized copolymers was necessary. Techniques including proton (¹H)-nuclear magnetic resonance (NMR), differential scanning calorimetry (DSC), thermal gravimetric analysis (TGA), rheometry and scanning electron microscopy (SEM), were all used to characterize the synthesized copolymers. ¹H NMR measurements confirmed the presence of PDMS in the copolymers. They also provided a quantitative measurement of PP to PDMS molar ratio in copolymers by determining the integration of PP PDMS repeating unit signals in NMR spectra. Compared to virgin PP, a lower melting enthalpy of the PP phase in the copolymer was observed from DSC results. This implied that the PDMS component influenced the thermal behavior of the PP crystalline phase in the copolymers. Moreover, TGA measurements indicated that a higher thermal stability was obtained for PP-PDMS copolymers than that for virgin PP wax and this was expected since PDMS is known for its excellent stability at high temperature. Rheological analysis showed that the presence of PDMS in the copolymers gave lower complex viscosities and loss moduli, but higher storage moduli than those for virgin PP. Furthermore, the morphology of copolymers was examined by SEM and elemental analysis at the surface using an energy dispersive X-ray (EDX) analyzer on the SEM. It was found that micrographs of copolymers showed round domains on the surface, which were not observed in virgin PP wax and those round segments were confirmed to contain silicon. Torque values used in a batch mixer for polymerizations and the remaining weight % of copolymers at 350°C were used to conduct statistical analysis, through which models used to describe the relationships between experimental factors and these physical responses were determined.