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This research investigates the modeling of randomly distributed surface-breaking microcracks and their effects on higher harmonic generation in Rayleigh surface waves. The modeling is based on micromechanical considerations of rough surface contact. The nonlinear behavior of a single microcrack is described by a hyperelastic effective stress-strain relationship. Finite element simulations of nonlinear wave propagation in a solid with distributed microcracks are performed. The evolution of fundamental and second harmonic amplitudes along the propagation distance is studied and the acoustic nonlinearity parameter is calculated. The results show that the nonlinearity parameter increases with crack density and root mean square roughness of the crack faces. While, for a dilute concentration of microcracks, the increase in acoustic nonlinearity is proportional to the crack density, this is not valid for higher crack densities, as the microcracks start to interact. Finally, it is shown that odd higher harmonic generation in Rayleigh surface waves due to sliding crack faces introduces a friction nonlinearity.

iv Summary Schmidt hammer is the instrument which is used for the assessment of rock mechanical properties and this instrument is classified as the indirect method. This method is based on the assessment of rebound value (R) of the Schmidt hammer, which is measurred by the amount of rebound of the impact plunger from the surface of tested rock. Schmidt hammer is called as the non-destructive method of rock assessment and it is called as in situ testing method as well. The main objective of this work is provement, that Schmidt hammer testing is destructive method and define degree of damage which is caused in the rock mass. Sedimentary rocks were used for the testing, mostly sandstones and arkose sandstones with different types of cement. This made it possible to test the fraction of the rock mass and the relation between fraction and type of cement. The clasts of the rocks had different properties than it was possible to find the relation between grain size and fraction of the rock. Already in procedure of the testing by Schmidt hammer it was obvious, that this metod is definitely destructive. Rock surface after hitting by plunger of Schmidt hammer gains macroscopically observeable destruction. On the surface is the circular track of the plunger and the surface is grinded. It is possible to wipe the small...

Les dépôts effectués sur substrats de silicium sont très courants notamment dans le domaine de la microélectronique. Les propriétés physiques recherchées pour ce type de structures dépendent fortement de celles de la couche. Il apparaît donc essentiel de connaître les paramètres élastiques ainsi que l’épaisseur des films considérés. De plus, la détection de certains défauts concernant la couche est souvent recherchée. L’objectif de ce travail a été de contribuer à la caractérisation de structures du type couche sur substrat. Pour cela, les ultrasons-lasers présentent de nombreux avantages puisqu’ils autorisent entre autres leur contrôle non destructif sans contact. Les ondes acoustiques de surface dans une gamme de fréquence s’étendant jusqu’à 45 MHz ont été utilisées. Nous avons développé différents modèles analytiques et les résultats expérimentaux ont aussi été comparés à certaines simulations par éléments finis. Plus particulièrement, nous avons montré qu’il était possible d’obtenir l’ensemble des paramètres élastiques du substrat et de la couche ainsi que l’épaisseur de cette dernière. Par ailleurs, nous nous sommes aussi intéressés à la détection de certains défauts en régime impulsionnel mais aussi quasi-monochromatique. Des résultats originaux concernant l’effet d’une absence de couche de forme déterminée sur le premier mode de Rayleigh ou bien encore de problèmes d’adhésion ont été présentés. Sur ce dernier point, une méthode innovante permettant de distinguer un fort niveau d’adhésion d’un faible a aussi été introduite. / Thin films deposited on silicon substrates are very common especially in microelectronic applications. The physical properties expected for these types of structures depend on the properties of the layer. Therefore, it is essential to know elastic parameters and thickness of the films considered. Furthermore, some layer defects detection is often required. The aim of this work was to contribute to the characterization of structures composed of a single layer deposited on a substrate. For this, laser ultrasonics offers many advantages since it is nondestructive and non-contact method. Surface acoustic waves excited in a frequency range up to 45 MHz are used. Analytical models have been developed and experimental results have also been compared with some finite element simulations. More specifically, we have shown that it was possible to obtain the thickness of the layer and all elastic parameters of both substrate and layer. In addition, we have been interested in the detection of various defects with a broadband and quasi-monochromatic excitation. Original results concerning the effect of a lack of layer with a specific geometry on the first Rayleigh mode or even adhesion problems were presented. Concerning this last point, an innovative method to tell difference between high and low adhesion was introduced.

Carbon fibre reinforced ceramic composites (Cf/C-SiC) have been explored as lightweight and durable disc in a friction brake. This composite was manufactured through infiltration of liquid silicon into a Cf/C perform. It has heterogeneous microstructure, composed of three key phases, silicon carbide, Cf/C, and un-reacted residual silicon. The development of the transfer layer on the friction surface of Cf/C-SiC was studied through microstructural image registration of the surface after a range of braking stops on a laboratory-scale dynamometer test rig. When an organic pad was used as the counter face brake pad, it was found that a steady transfer layer was developed in silicon regions right after initial stops; in carbon-fibre/carbon (Cf/C) regions and most of the silicon carbide region, the friction surfaces were unsteady and any possible friction transfer layers were hardly built up. Large voids and cracks/crevices likely became pools to quickly and efficiently collect the transferred materials generated by the friction, but the compacts formed inside the pools were susceptible to be stripped off by further braking operation. Three types of friction surfaces were generalized: type I, the friction transfer layer had a steady relationship with the matrix and respectable longevity; type II, the transfer layer had an unstable relationship with the matrix and poor durability; type III, the friction transfer layer had a steady relationship with the matrix but short lifetime. After testing against organic pads under the laboratory scale dynamometer testing condition, the friction surface of each key phase in Cf/C-SiC composites disc was studied by transmission electron microscopy (TEM). It was found that the transfer layer developed on Si consists of fine particles of metal silicides, silicates and minerals. The substrate damage of Si was not observed, while the precipitates having high oxygen content were found in the substrate. Formation of an interfacial bonding between transfer layer and silicon substrate is believed to be the key factor for the formation of a stable transfer layer on Si. However, the interfacial bonding between transferred materials and SiC was not detected. Kinks are common features developed on the friction surface of SiC. The interface between carbon fibre and carbon matrix was experienced mechanical damage, in form of microcracks, and the transferred material was developed in the interface. Instead of transfer layer, a thin amorphous film, produced by friction induced amorphisation of carbon fibre, was developed on top of carbon fibre.

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The goal of this research is to investigate the fundamentals of fracturing processes in heterogeneous materials such as concrete using geophysical methods and dynamic micromechanical models. This work describes how different aspects of fracture formation in concrete can be investigated using a combination of Acoustic Emission (AE) techniques, ultrasonic wave velocity imaging, and high resolution Computed Tomography (CT). Fracture formation and evolution were studied during shear failure of large reinforced concrete beams and compressive failure of concrete samples. AE analysis includes studying complex spatial and temporal fracture development that precedes shear failure. Predominant microcrack mechanisms were analyzed at different stages of fracture formation. CT images were used to investigate the influence of concrete microstructure on fracture topography. Combined AE and CT damage evaluation techniques revealed different aspects of fracture development, thus expanding our understanding of AE events and their mechanisms. These images show how aggregate particles influence fracture nucleation and development. An emphasis has been placed on the role of coarse aggregates during the interlocking of fracture surfaces at transferring shear stresses. Ultrasonic wave velocity and AE techniques have been applied to uniaxial compression tests of concrete with various aggregate sizes and strengths similar to that of the concrete beams. AE parameters, p-wave velocities, and stress-strain data have been analyzed concurrently to image damage evolution under compression. Influence of material composition on microcracking and material state changes during loading has been investigated in detail. The results of compressive tests were used as building blocks for developing realistic micromechanical numerical models of concrete. The models were designed using a distinct element code, where material is modelled through the combination of bonded particles. A number of procedures were developed to transfer the exact microstructure of material incorporating its visual representation into the model. The models’ behaviour has been verified against experimental data. It was shown that these models exhibit realistic micromechanical behaviour. The results of the experimental investigation of concrete fracturing were expanded by modelling more cases with aggregate size and strength variations. It was shown that geophysical imaging techniques, along with advanced micromechanical numerical modelling, can help us understand damage formation and evolution.

The goal of this research is to investigate the fundamentals of fracturing processes in heterogeneous materials such as concrete using geophysical methods and dynamic micromechanical models. This work describes how different aspects of fracture formation in concrete can be investigated using a combination of Acoustic Emission (AE) techniques, ultrasonic wave velocity imaging, and high resolution Computed Tomography (CT). Fracture formation and evolution were studied during shear failure of large reinforced concrete beams and compressive failure of concrete samples. AE analysis includes studying complex spatial and temporal fracture development that precedes shear failure. Predominant microcrack mechanisms were analyzed at different stages of fracture formation. CT images were used to investigate the influence of concrete microstructure on fracture topography. Combined AE and CT damage evaluation techniques revealed different aspects of fracture development, thus expanding our understanding of AE events and their mechanisms. These images show how aggregate particles influence fracture nucleation and development. An emphasis has been placed on the role of coarse aggregates during the interlocking of fracture surfaces at transferring shear stresses. Ultrasonic wave velocity and AE techniques have been applied to uniaxial compression tests of concrete with various aggregate sizes and strengths similar to that of the concrete beams. AE parameters, p-wave velocities, and stress-strain data have been analyzed concurrently to image damage evolution under compression. Influence of material composition on microcracking and material state changes during loading has been investigated in detail. The results of compressive tests were used as building blocks for developing realistic micromechanical numerical models of concrete. The models were designed using a distinct element code, where material is modelled through the combination of bonded particles. A number of procedures were developed to transfer the exact microstructure of material incorporating its visual representation into the model. The models’ behaviour has been verified against experimental data. It was shown that these models exhibit realistic micromechanical behaviour. The results of the experimental investigation of concrete fracturing were expanded by modelling more cases with aggregate size and strength variations. It was shown that geophysical imaging techniques, along with advanced micromechanical numerical modelling, can help us understand damage formation and evolution.

A functional nanometer-scale hybrid coating layer with multi-walled carbon nanotubes (MWCNTs) and/or nanoclays, as mechanical enhancement to ‘heal’ surface microcracks and environmental barrier layer is applied to alkaliresistant glass (ARG) fibres. The nanostructured and functionalised traditional glass fibres show both significantly improved mechanical properties and environmental corrosion resistance. Early warning material damage can be achieved by carbon nanotubes concentrated interphases in the composites. / Eine funktionale nanometerskalige Hybridbeschichtung mit multi-walled carbon nanotubes (MWCNTs) und/oder Nanoclay wurde als mechanische Verbesserung des „Ausheilens“ von Oberflächen-Mikrorissen und Barriereschicht gegenüber Umwelteinflüssen auf alkaliresistente Glasfasern (ARG) appliziert. Die nanostrukturierten und funktionalisierten traditionellen Glasfasern zeigen signifikant verbesserte mechanische Eigenschaften und Korrosionsbeständigkeit. Die Frühwarnung des Materialversagens kann durch Carbon Nanotubes, konzentriert in der Grenzschicht der Composites, erreicht werden.

En raison de l'exigence de protection de l'environnement, les briques d'argile cuites sont face à une nouvelle tendance de développement. Briques d'argile cuites ne sont pas seulement satisfaits de la mécanique force mais aussi augmentation de l'utilisation de l'énergie. La conductivité thermique est un paramètre très important mesurer l'utilisation de l'énergie. Sur le principe de garantir essentiellement propriétés mécaniques, la réduction de la conductivité thermique a été l'un des développements importants objectifs dans l'industrie du bâtiment.Basé sur l'analyse de la microstructure, les pores microscopiques ont un effet sur la macroscopie constantes élastiques et conductivité thermique. Micropores parallèles résultant de la production les méthodes provoquent l'isotropie transversale des briques d'argile cuites. Cependant, ce n'est pas clair que l'influence des micropores sur les propriétés macroscopiques. Bien que certains modèles étudié l'effet de la porosité sur les propriétés mécaniques des briques d'argile cuite, ces modèles sont empiriques et ont ignoré de nombreuses informations microscopiques. Un des buts de la thèse est d'analyser l'influence de la forme, l'orientation et la distribution spatiale de microscopique facteurs sur les propriétés mécaniques et la conductivité thermique afin de fournir une référence optimiser la micro-structure des briques d'argile cuites. / Due to the environmental protection requirement, fired clay bricks are facing new development tendency. Fired clay bricks are not only satisfied with mechanical strength but also rising energy utilization. Thermal conductivity is a very important parameter to measure the energy utilization. On the premise of guaranteeing the basically mechanical properties, reducing thermal conductivity has been one of important development goals in building industry.Based on the analysis of micro-structure, microscopic pores have an effect on macroscopic elastic constants and thermal conductivity. Parallel micropores resulting from producing methods cause the transverse isotropy of fired clay bricks. However, it is not clear that the influence of micropores on the macroscopic properties. Though some models studied the effect of porosity on mechanical properties of fired clay bricks, these models are empirical and ignored many microscopic information. One of the goals of the thesis is to analyze the influence of shape, orientation and spatial distribution of microscopic factors on mechanical properties and thermal conductivity in order to provide a reference to optimize the micro-structure of fired clay bricks.