L'interférométrie sismique, tout comme l'interférométrie optique, étudie les phénomènes d'interférence entre des couples de signaux sismiques afin de mettre en évidence des différences entre ces signaux (par exemple Curtis et al. 2006). Les traitements utilisés consistent le plus souvent à corréler les enregistrements entre différents capteurs pour remonter aux fonctions de Green, (ou réponse impulsionnelle) entre ces récepteurs (par exemple, Derode et al. (2003), Wapenaar et al. (2004), Larose et al. (2006), Sanchez-Sesma et Campillo (2006)). Ce principe a déjà été appliqué avec succès dans les domaines de la sismologie (Campillo et Paul (2003)), des ultrasons (Weaver et Lobkis (2001)), de l'exploration sismique (Schuster (2001) et Wapenaar et al. (2004)), et même de l'hélio-sismologie (Duvall et al. (1993)) Dans tous ces cas, l'analyse des corrélations a conduit à une description détaillée des milieux de propagation, en l'occurrence l'intérieur de la Terre dans le cas de la sismologie. La sismique passive, par opposition à la sismique active utilisant les sources cohérentes artificielles (explosifs, canons à air, vibrateurs...), exploite les sources cohérentes naturelles (séismes...). Depuis peu la sismique passive exploite également des champs d'ondes aléatoires engendrées à des temps inconnus par une multitude de sources inconnues dans le sous-sol qui sont enregistrées à différentes positions de récepteurs. L'analyse par interférométrie sismique des enregistrements à deux capteurs permet de remonter aux fonctions de Green, ou réponse impulsionnelle, entre ces deux récepteurs (Derode et al. (2003)). Cette thèse, à vocations à la fois expérimentale et applicative, a deux buts : - vérifier au laboratoire, sur des expériences ultrasonores et avec différents types de roches, l'efficacité du monitoring de substitution de fluides par l'analyse interférométrique ultrasonore - appliquer sur le terrain les méthodes d'interférométrie sismique passive à des expériences ponctuelles de surveillance sismique passive d'exploitation du sous-sol. Ce manuscrit présente, après une synthèse bibliographique, la mise au point d'une nouvelle méthode de mesure des constantes élastiques d'un échantillon de roche (sèche ou saturée de fluide) basée sur les principes de l'interférométrie ultrasonore et de la spectroscopie par résonance ultrasonore. La méthode a été testée et validée (reproductibilité, fidélité, fiabilité…) sur un matériau standard de propriétés connues (aluminium). On expose que les effets de substitution fluide sont tout-à-fait mesurables avec la méthode sur divers échantillons de roches sèches puis saturées (en eau ou en éthylène glycol) et les résultats sont en accord raisonnable avec la théorie poroélastique de Biot-Gassmann. En outre, un certain nombre de faiblesses de la méthode ont été mises en évidence, à savoir la limitation à des roches assez homogènes et peu atténuantes. La dernière partie de ce manuscrit met en évidence des variations de vitesse des ondes dans un champ d'hydrocarbures (informations relatives à ce champ confidentielles) concomitantes avec le début de l'injection de vapeur dans celui-ci (pour récupération assistée de l'huile). / Seismic interferometry, like optic interferometry, studies the interferences phenomena between couples of seismic signals, with the aim of pointing at differences between those signals (Curtis et al. 2006 for instance). The data processing consists, generally, in correlating the recordings between different stations to retrieve the Green's function between these sensors (Derode et al. (2003), Wapenaar et al. (2004), Larose et al. (2006), Sanchez-Sesma et Campillo (2006)). This principle has already been successfully applied in the field of seismology (Campillo and Paul (2003)), ultrasound (Weaver et Lobkis (2001)), seismic exploration and even helioseismology (Duvall et al. (1993)). In all these cases, the analysis of the correlations leads to a detailed description of the propagation medium. Contrary to active seismic which uses artificial coherent sources (explosives, air guns…), passive seismic exploits natural coherent sources (seisms…). Since a few years, passive seismics also exploits random wave fields generated at unknown times by many unknown sources in the ground, and recorded at different stations positions. The analysis with cross-correlation of pairs of recordings, from pairs of sensors, leads to the Green's function between the two sensors (Derode et al. (2003)). This thesis has two objectives: -to check, at the lab scale, the effectiveness of monitoring of fluids substitution with noise correlation (ultrasound scale) in rocks -to apply noise correlation methods to passive seismic monitoring of a hydrocarbons field. This thesis presents, after a state of the art, the set-up of a new method to measure elastic constants of a rock sample (dry or fluid-saturated), based on ultrasound interferometry principle and resonant ultrasound spectroscopy. The method has been tested and validated (reproducibility, accuracy, precision…) on a standard material (aluminium). We show that the effects of a fluids substitution are measurable on various rock samples (dry or saturated, with water or with ethylene glycol) with this method. Plus the results are in agreement with Biot-Gassmann's theory. Besides, several weaknesses of the method were pointed, that is to say the method does not work on heterogeneous or attenuating medium. The last part of this thesis exposes speed of waves variations in a hydrocarbons field, when steam is injected simultaneously inside the reservoir (enhanced oil recovery operation).

Submitted by Jesiel Ferreira Gomes (jesielgomes@ufcg.edu.br) on 2018-04-17T23:15:52Z No. of bitstreams: 1 FELIPE DE OLIVEIRA APOLINÁRIO – DISSERTAÇÃO (PPGEPM) 2016.pdf: 5151929 bytes, checksum: f4706d54cb97c9b01a64299ddb28cd7d (MD5) / Made available in DSpace on 2018-04-17T23:15:52Z (GMT). No. of bitstreams: 1 FELIPE DE OLIVEIRA APOLINÁRIO – DISSERTAÇÃO (PPGEPM) 2016.pdf: 5151929 bytes, checksum: f4706d54cb97c9b01a64299ddb28cd7d (MD5) Previous issue date: 2016-09-06 / Capes / O presente trabalho teve como objetivo analisar a influência da saturação fluida nas propriedades elásticas de rochas carbonáticas, bem como a eficácia dos modelos de substituição de fluidos e de simulação computacional. Foram estudadas 9 amostras de rochas carbonáticas, sendo dois calcários laminados e sete tufas. As medições de velocidade foram realizadas em amostras secas, saturadas com água ou com óleo, sob diferentes pressões efetivas. A simulação de propagação de ondas foi feita no COMSOL Multiphysics 5.1, utilizando o Avizo Fire 8.1 para a criação das amostras digitais. Análise por difração de raios X (DRX) foi realizada para determinar a composição das amostras de rocha. Os resultados obtidos nos ensaios laboratoriais e nas simulações computacionais foram comparados com as estimativas dos modelos de substituição de fluidosGassmann, Biot e Brown & Korringa. Foi observado que a saturação das amostras com agua ou óleo geraram aumentos nas velocidades de propagação de onda P, porém sem apresentar um comportamento padrão. Para o caso das ondas S, a saturação por óleo predominantemente gerou aumentos nas velocidades, com exceção para os casos em que as amostras possuíam porosidade secundária do tipo vugular, devido à pouca influência que o óleo oferece para o módulo de cisalhamento nestes casos. A saturação por água resultou em diminuições das velocidades de propagação de onda S devido ao aumento da densidade total. Também foi constatado que o modelo de Gassmann foi o mais efetivo na estimativa de velocidades de onda P e S, enquanto que o de Biot mostrou-se eficaz apenas para a estimativa de velocidades de ondas S, sendo ineficiente para a estimativa de velocidades de ondas P, com erros de até 20%. A simulação computacional gerou resultados superdimensionados, porém que evidenciam que um aperfeiçoamento da metodologia, tal como o aumento do número de pontos de leitura pode gerar resultados mais próximos dos obtidos laboratorialmente e de maior confiabilidade. / This research aimed to analyze the influence of the saturating fluid in carbonate rocks, as well as verify the effectiveness of the fluid substitution models and computational simulations of wave propagation. To do so, nine carbonate rock samples were analyzed, which two of them were laminated limestones and seven were carbonate tufas. The measurement of velocities were made in dry, water saturated and oil saturated samples, under different effective pressures. The wave propagation simulations were made in COMSOL Multiphysics 5.1 using Avizo Fire 8.1 to generate the digital rock samples. The results obtained in lab procedures and in computer simulations were compared with the estimated velocities of the fluid substitution models of Gassmann, Biot and Brown & Korringa. It was observed that the saturation of the samples with water or oil resulted in an increasing of P-wave velocities, however without a pattern. The saturation with oil resulted in most cases in an increasing of S-wave velocities, the exceptions occurred in samples which had vugular porosity, due to the small influence of the oil in the shear modulus in this cases. T he saturation with water resulted in a decreasing of S-wave velocities due to the increment of the bulk density. It was found that the Gassmann’s model was more effective than the other two models in estimating P-wave and S-wave velocities. Biot’s model generated unsatisfying results to P-wave velocities, with errors up to 20%. However, this model had a good accuracy in estimating S-wave velocities. The computer simulations produced mainly overestimated results, though it was shown that an optimization of methodology, such as and addition in the number of the measure points, could improve the quality of the data, providing more representative results.

No description available.

La thèse a pour but d’étudier les effets de changements de mouillabilité de roches dans des conditions d’injections d’eau douce en tant que méthode de récupération d’hydrocarbures. Afin d’identifier le ou les mécanismes à l’origine du gain additionnel de récupération nous avons utilisé un microtomographe RX. Nous avons ainsi imagé les états de saturations finales d’un milieu poreux rempli de saumures et d’huiles. Une fois le drainage primaire réalisé nous avons effectué deux phases d’imbibitions : avec une saumure (récupération secondaire) puis une imbibition d’eau douce (récupération tertiaire). L’analyse de la mouillabilité à l’échelle du pore a permis de mettre en évidence l’effet de la température et de la salinité sur la mouillabilité. Nous avons montré que les changements de mouillages des roches n’étaient pas occasionnées par la seule expansion de la couche électrique en revanche des changements de mouillabilité ont été montrés. Ces changements s’expliquant par des transitions de mouillages de second ordre observées non seulement pour des gouttes d’huiles sur de l’eau mais également sur un substrat en verre. Au final, la mouillabilité en milieux poreux doit être mise en évidence à une échelle sous-Micrométrique ce qui est relativement nouveau dans le domaine pétrolier. / The aim of the thesis is to study rock wettability change effects caused by Low Salinity brine injection as tertiary recovery method. To identify the underlying mechanism or mechanisms of additional oil recovery X-Ray imaging technology was applied. We have also imaged the end-Point saturations of filled by brine and water core samples. Once the primary drainage is realized we carried out two phases imbibitions: with high salinity brine (waterflooding) and with low salinity brine (tertiary recovery mode). The wettability analysis at pore scale permitted to put in evidence the thermal and saline effects playing a decisive role in rock wettability. We have showed wettability changes are not caused by only electrical double layer expansion, however wettability changes was shown. These changes are explained by wettability transition of second order and observed not only for oil droplet on brine, but also for oil deposited on glass substrate. Finally, the pore space wettability needs to be evidenced at sub-Micrometric scale that is new for the petroleum domain.

Quantifying the influence of pressure on the effective elastic rock properties is important for applications in rock physics and reservoir characterization. Here I investigate the relationship between effective pressure and seismic velocities by performing inversion on the laboratory-measured data from a suite of clastic, carbonate and igneous rocks, using different analytic and discrete inversion schemes. I explore the utility of a physical model that models a natural fracture as supported by asperities of varying heights, when an effective pressure deforms the tallest asperities, bringing the shorter ones into contact while increasing the overall fracture stiffness. Thus, the model is known as the ?asperity-deformation? (ADM) or ?bed-of-nails? (BNM) model. Existing analytic solutions include one that assumes the host rock is infinitely more rigid than the fractures, and one that takes the host-rock compliance into account. Inversion results indicate that although both solutions can fit the data to within first-order approximation, some systematic misfits exist as a result of using the rigid-host solution, whereas compliant-host inversion returns smaller and random misfits, yet out-of-range parameter estimates. These problems indicate the effects of nonlinear elastic deformation whose degree varies from rock to rock. Consequently, I extend the model to allow for the pressure dependence of the host rock, thereby physically interpreting the nonlinear behaviors of deformation. Furthermore, I apply a discrete grid-search inversion scheme that generalizes the distribution of asperity heights, thus accurately reproduces velocity profiles, significantly improves the fit and helps to visualize the distribution of asperities. I compare the analytic and numerical asperity-deformation models with the existing physical model of elliptical ?pennyshape? cracks with a pore-aspect-ratio (PAR) spectrum in terms of physical meaning and data-fitting ability. The comparison results provide a link and demonstrate the consistency between the use of the two physical models, making a better understanding of the microstructure as well as the contact mechanism and physical behaviors of rocks under pressure. ADM-based solutions, therefore, have the potential to facilitate modeling and interpretation of applications such as time-lapse seismic investigations of fractured reservoirs.

[pt] As reservas de óleos pesados têm obtido grande importância devido à diminuição das reservas de óleos leves e ao aumento dos preços do petróleo. Porém, precisa-se de aumentar a viscosidades destes óleos pesados para que possam fluir até superfície. Para reduzir a viscosidade foi escolhida a técnica de recuperação térmica SAGD (Steam Assisted Gravity Drainage) pelos seus altos valores de recobro. A redução da viscosidade é atingida pela transmissão de calor ao óleo pela injeção de vapor, porém uma parte deste calor é transmitida à rocha. Esta transmissão de calor junto com a produção de óleo geram uma variação no estado de tensões no reservatório o que por sua vez geram fenômenos geomecânicos. Os simuladores convencionais avaliam de uma forma muito simplificada estes fenômenos geomecânicos, o que faz necessários uma abordagem mais apropriada que acople o escoamento dos hidrocarbonetos e a transmissão de calor com a deformação da rocha. As mudanças no reservatório, especialmente a variação da saturação, afetam as propriedades sísmicas da rocha, as quais podem ser monitoradas para acompanhar o avanço da frente de vapor. A simulação fluxo-térmica-composicional-geomecânica é integrada à sísmica de monitoramento 4D da injeção de vapor (a través da física de rochas). Existe uma grande base de dados, integrada por propriedades dos fluidos do reservatório (PVT) (usado no arquivo de entrada de simulação de fluxo) e uma campanha de mecânica das rochas. Foram simulados vários cenários geomecânicos considerando a plasticidade e variação da permeabilidade. Foram avaliadas várias repostas geomecânicas e de propriedades de fluidos no pico de pressão e final do processo SAGD. A resposta geomecânica pode ser observada, porém foi minimizada devido à baixa pressão de injeção, sendo o mecanismo de transmissão de calor um fator importante na produção de óleo (pela redução da viscosidade) e a separação vertical entre poços. Foi também significativa à contribuição da plasticidade no aumento da produção de hidrocarbonetos. A impedância acústica foi calculada usando a Equação de substituição de fluidos de Gassmann. Os sismogramas sintéticos de incidência normal (para monitorar o avanço da frente o câmara de vapor) mostraram a área afetada pela injeção de vapor, porém com pouca variação devida principalmente à rigidez da rocha. / [en] The heavy oil reserves have gained importance due to the decreasing of the present light oil reserves. Although it is necessary to reduce the oil viscosity and makes it flows to surface. For its high recovery factor the SAGD (Steam Assited Gravity Drainage) thermal process was selected. The viscosity reduction is achieved by heat transfer from steam to oil, but some part of this heat goes to rock frame. This heat transfer together with oil production change the initial in-situ stress field what creates geomechanical effects. The conventional flux simulators have a very simplified approach of geomechanical effects, so it is necessary to consider a more suitable approach that considers the coupling between oil flux and heat transfer with rock deformation. The changes within the reservoir, specially the saturation change, affect the seismical rock properties which can be used to monitor the steam chamber growth. The flux-thermal geomechanics is integrated to steam chamber monitoring 4D seismic (through the rock physics). There is a great data base, integrated by reservoir fluid properties (PVT) (used in reservoir simulation dataset) and a rock mechanics campaign. Several scenaries were simulated considering the plasticity and permeability variation. Several geomechanical responses and flux properties at peak pressure and end of SAGD process were evaluated. The geomechanical response can be observed, but was minimized due to low steam injection pressure, being the heat transfer an important in oil production (for the viscosity reduction) and the vertical well separation, too. The plasticity has a significant contribution in the increment of oil production. Acoustic impedance was calculated by using Gassmann fluid substitution approach. 2D Synthetic seismograms, normal incidence (to monitor the steam camera front advance), showed the area affected by steam injection, but with little variation due principally to rock stiffness.

Magister Scientiae - MSc / Pressure drop within a field can be attributed to several factors. Pressure drop occurs when fractional forces cause resistance to flowing fluid through a porous medium. In this thesis, the sciences of petrophysics and rock physics were employed to develop understanding of the physical processes that occurs in reservoirs. This study focussed on the physical properties of rock and fluid in order to provide understanding of the system and the mechanism controlling its behaviour. The change in production capacity of wells E-M 1, 2, 3, 4&5 prompted further research to find out why the there will be pressure drop from the suits of wells and which well was contributing to the drop in production pressure. The E-M wells are located in the Bredasdorp Basin and the reservoirs have trapping mechanisms of stratigraphical and structural systems in a moderate to good quality turbidite channel sandstone. The basin is predominantly an elongated north-west and south-east inherited channel from the synrift sub basin and was open to relatively free marine circulation. By the southwest the basin is enclose by southern Outeniqua basin and the Indian oceans. Sedimentation into the Bredasdorp basin thus occurred predominantly down the axis of the basin with main input direction from the west. Five wells were studied E-M1, E-M2, E-M3, E-M4, and E-M5 to identify which well is susceptible to flow within this group. Setting criteria for discriminator the result generated four well as meeting the criteria except for E-M1. The failure of E-M1 reservoir well interval was in consonant with result showed by evaluation from the log, pressure and rock physics analyses for E-M1.iv Various methods in rock physics were used to identify sediments and their conditions and by applying inverse modelling (elastic impedance) the interval properties were better reflected. Also elastic impedance proved to be an economical and quicker method in describing the lithology and depositional environment in the absence of seismic trace.

The field of geosciences, including geophysics, plays a crucial role in addressing society's pressing concerns related to energy demand, climate change, resource preservation, and environmental protection. Reactive systems encountered in this context are characterized by intricate interactions among various phases, environmental conditions, physical and chemical processes. Achieving a comprehensive understanding of these processes and quantitatively evaluating reactive systems necessitates a holistic scientific approach. This approach encompasses efficient categorization of reactive systems, the development of appropriate experimental and computational tools, and the collection and dissemination of relevant data. In this context, this thesis contributes to geophysics and petrophysics with a focus on reactive systems. It presents and interprets laboratory datasets that address various complex aspects of rock behavior, including the presence of graphite, resulting anisotropy, and the challenging petrophysical characteristics of carbonate rocks. This compilation of research results provides a multifaceted perspective on the complex nature of rocks, including their mineralogical, physical, and chemical properties. It thus contributes to a deeper comprehension of electrical rock properties and their practical utility. Upon examining carbonate rocks and the response of graphitic schist to CO$_\mathrm{2}$ under reservoir conditions, it becomes clear that the impact of increased reactivity in a system on geophysical parameters varies depending on the specific characteristics of the rocks and systems under investigation. Consequently, geophysical methods aiming at a quantitative assessment of reactive systems must exhibit robustness and efficiency in order to be effectively applied in a site- and system-specific manner. Expanding on this foundation, computational methods have been developed to aid in the quantitative analysis of reactive processes in laboratory experiments. These methods also serve as tools for gaining insights into the origin of rock properties and the impact of microstructure variation. Furthermore, inversion techniques are introduced in conjunction with custom-designed experiments within the field of petrophysics. The resultant software tool is made publicly accessible. The research further delves into the exploration of how physical properties of rocks are influenced by their microstructure, as well as how the stochastic nature of pore space geometry can introduce variability and uncertainty in rock physics data. This investigation was carried out through microstructure modeling and finite element simulations. Leveraging these tailored computational techniques allowed for a comprehensive understanding of laboratory data, facilitating robust generalizations and contextualization for field applications and site-specific integrated interpretation. To illustrate the application in a complex natural reactive system, a field study focusing on coastal fumarolic vents in volcanic terrain was carried out and is presented. The challenges, prospects and visualization strategies for integrating simulation or inversion results from different methods are examined. Effective evaluation of complex sites requires open access to existing knowledge, including laboratory datasets. Consequently, this work documents and provides openly accessible examples of complex multi-method laboratory datasets to facilitate better understanding, re-evaluation and application in the field. Finally, the handling of multi-reactive systems in field applications is discussed. It involves the integration of three-dimensional subsurface models with petrophysical insights related to multi-reactive systems. These models are calibrated using additional complementary data from surface or borehole sources. This integrated approach enables a quantitative assessment of site-specific multi-reactive systems.