Blends of poly butylene terephthalate (PBT) and polycarbonate (PC) form a very important class of commercial blends in numerous applications requiring materials with good chemical resistance, impact resistance even at low temperatures, and aesthetic and flow characteristics. PC and PBT are usually blended in a twin screw extruder (TSE). Product melt volume flow rate (MVR) is a property used to monitor product quality while blending the PC/PBT in a twin screw extruder. It is usually measured off line in a quality control laboratory using extrusion plastometer on samples collected discretely during the compounding operation. Typically a target value representing the desired value of the quality characteristics for an in-control process, along with upper and lower control limits are specified. As long as the MVR measurement is within the control limits, the sample is approved and the whole compounded blend is assumed to meet the specification. Otherwise, the blend is rejected. Because of infrequent discrete sampling, corrective actions are usually applied with delay, thus resulting in wasted material. It is important that the produced PC/PBT blend pellets have consistent properties. Variability and fault usually arise from three sources: human errors, feed material variability, and machine operation (i.e. steady state variation). Among these, the latter two are the major ones affecting product quality. The resulting variation in resin properties contributes to increased waste products, larger production cost and dissatisfied customers. Motivated by this, the objective of this project was to study the compounding operation of PC/PBT blend in a twin screw extruder and to develop a feasible methodology that can be applied on-line for monitoring properties of blends on industrial compounding operations employing available extruder input and output variables such as screw speed, material flow rate, die pressure and torque. To achieve this objective, a physics-based model for a twin screw extruder along with a MVR model were developed, examined and adapted for this study, and verified through designed experiments. This dynamic model for a TSE captures the important dynamics, and relates measurable process variables (screw speed, torque, feed rates, pressure etc.) to ones that are not being measured (material holdups and compositions at the partially and filled section along a TSE barrel). This model also provides product quality sensors or inferential estimation techniques for prediction of viscosity and accordingly MVR. The usefulness of the model for inferential MVR sensing and fault diagnosis was demonstrated on experiments performed on a 58 mm co-rotating twin-screw extruder for an industrial compounding operation at a SABIC Innovative Plastics plant involving polycarbonate – poly butylene terephthalate blends. The results showed that the model has the capability of identifying faults (i.e., process deviation from the nominal conditions) in polymer compounding operations with the twin screw extruder. For instance, the die pressure exhibited a change as a function of changes in raw materials and feed composition of PC and PBT. In the presence of deviations from nominal conditions, the die pressure parameters are updated. These die pressure model parameters were identified and updated using the recursive parameter estimation method. The recursive identification of the die pressure parameters was able to capture very well the effects of changes in raw material and/or composition on the die pressure. In addition, the developed MVR model showed a good ability in monitoring product MVR on-line and inferentially from output process variables such as die pressure which enables quick quality control to maintain products within specification limits and to minimize waste production.

In this work, the compounding of polycarbonate (PC) / poly-butylene terephthalate (PBT) blends was studied for the purpose of improving quality of products with reduced wastage and finally to satisfaction of end users. The effect of material rheological characteristics and processing conditions on compounding of PC /PBT was investigated through statistical experiments carried out on a 58 mm twin-screw extruder at SABIC Innovative Plastics Limited (formerly GE Plastics Limited) in Cobourg, Ontario. Melt Volume-Flow Rate (MVR) is the most commonly used property to monitor the quality of products of PC/PBT blends. The MVR was studied with different sampling times and correlations between product properties (melt flow) and processing conditions (screw speed, flow rates) were discussed. The rheological behavior of PC/PBT blends was investigated by dynamic and capillary rheometers. The effects of processing conditions (screw speed, feed rate) on viscosity were measured and it was found that the Cox-Merz rule is not valid for PC/PBT blends. The change of morphology of PC/PBT blends was observed under a scanning electron microscope (SEM) by using different types of samples. Those samples were (i) PC/PBT blends pellets, (ii) PC/PBT blend samples, but collected after completing the rheological tests in the parallel plate rheometer, and (iii) PC/PBT blend samples, but collected after completing the rheological tests in the capillary rheometer. There was evidence that the samples collected after completing the tests in the parallel and capillary rheometer might be degraded due to temperature and time.

The diploma thesis brings a description and realization of new measuring devices which are designed to support student´s laboratory practice of air flow measurement techniques. The new devices and laboratory exercises help students get experience of several methods of measuring which they get to know during mandatory Bachelor's and Master's study programmes. The paper also includes a theoretical background, the knowledge of which is necessary for mastering the issue. Moreover, the paper comprises a literary search of sensors and a market research. The second part of the thesis presents possibilities of the laboratory workplace, and the results of the measurements of the new laboratory devices used for sample laboratory exercises.

This project was carried out for a Company in the mining and construction business, and focused on the development of a radar based material monitoring solution for conveyor belts. A minor prestudy showed that there are possible customer values related to material monitoring solutions for equipment relevant for the Company, and that such solutions using radar possibly can fulfil the application requirements. The main focus of the project was chosen based on this prestudy. The methods used were mainly experiments with the developed prototype, and a study of literature. The prototype was developed with an aim to measure mass flow and to monitor the material surface for deviances. Millimeter-wave pulsed coherent radar sensors were used, and data processing approaches included Kalman filtering. Results showed that mass flow can be calculated using the tested senors and data processing models, as the calculated mass flow was well in line with a belt scale reference, but that additional data is needed to prove consistency in the results. Results also showed that trends in the material surface can be observed in the radar data, indicating the possibilities to detect deviances. From a technical perspective, results and the possibilities for further development and improvement show that radar based solutions can be used for applications relevant for the Company. / Detta examensarbete genomfördes för ett företag inomgruv- och anläggningsbranschen och handlade om utvecklingen av en radarbaserad prototyp för mätningar av materialet på transportband. En mindre förstudie visade på möjliga kundvärden relaterade till sådana mätningar, samt att radar har potentialen att uppfylla kravspecifikationen för flera applikationer. Huvudfokuset för projektet valdes sedan utifrån denna förstudie. Metoderna som användes var främst experiment med den utvecklade prototypen samt litteraturstudier. Prototypen utvecklades med syfte att mäta massflöde samt att upptäcka avikelser i materialets yta. Radarsensorer med en frekvens på 60GHz användes, och för databehandling användes bland annat ett Kalman-filter. Resultaten visade att massflöde kan beräknas med de testade sensorerna och databehandlingsmodellerna, eftersom det beräknade massflödet låg i linje med referensdata från en bandvåg. Ytterligare data behövs emellertid för att visa hur resultaten påverkas av förändrade omständigheter, såsom storleken på fragmenten som mäts. Studien visade också att mönster i materialytan kan observeras i radardatan, vilket indikerar att det också är möjligt upptäcka avvikelser. Ur ett teknisktperspektiv visar resultaten och möjligheterna till vidareutveckling tillsammans att radarbaserade lösningar kan användas för applikationer relevanta för företaget.

New emission legislation regarding air pollution control, as instructed by the Department of Environmental Affairs (DEA) to Eskom Generation Power Stations, implies a particulate emission limit of 100 mg/Nm3 for all existing power stations by 2015 and 50 mg/Nm3 for all new and existing power stations by the year 2020. Some of Eskom’s power stations which are equipped with Electrostatic Precipitators (ESP’s) were not designed for this stringent legislation. It is also experienced that ESP’s and coal quality in Eskom have deteriorated over time, resulting in the performance of the ESP’s not meeting the legislative requirements. Eskom is in the process of introducing various ESP enhancement projects to improve performance and aligning the operating philosophy to comply with the more stringent particulate emission legislation. An ESP efficiency test was conducted at Lethabo Power Station to determine the current state of the plant and performance. The results of the test were compared with the original design base specifications to determine the relevant deficiencies which contribute to high emissions and poor ESP performance. It was aimed to develop an ESP simulation model and validate the outputs with the test data. This study endeavours to demonstrate the greater impact on ESP performance when the ESP is operated outside the design specification. It is further aimed to demonstrate that a solution to the problem of high emissions is not only contributed by the variables within the ESP itself. This study is a coal to stack evaluation considering the ESP variables and the upstream conditions of the ESP that form part of the entire process. The intention of this study is to demonstrate the importance of operating an ESP at the designed parameters and highlight the significance of proper maintenance. It was learned that before any ESP enhancement technology can be implemented, the ESP and upstream conditions must be in accordance with design specifications. The implementation of an ESP enhancement technology will have no merit or justification on a unit that is being operated outside of its design specifications. The results obtained from the ESP simulation model correlated well with the ESP efficiency test data. The expectation of the model to assist operators and engineers to operate ESP’s according to the designer’s specifications was conceded. / MIng (Mechanical Engineering), North-West University, Potchefstroom Campus, 2014

New emission legislation regarding air pollution control, as instructed by the Department of Environmental Affairs (DEA) to Eskom Generation Power Stations, implies a particulate emission limit of 100 mg/Nm3 for all existing power stations by 2015 and 50 mg/Nm3 for all new and existing power stations by the year 2020. Some of Eskom’s power stations which are equipped with Electrostatic Precipitators (ESP’s) were not designed for this stringent legislation. It is also experienced that ESP’s and coal quality in Eskom have deteriorated over time, resulting in the performance of the ESP’s not meeting the legislative requirements. Eskom is in the process of introducing various ESP enhancement projects to improve performance and aligning the operating philosophy to comply with the more stringent particulate emission legislation. An ESP efficiency test was conducted at Lethabo Power Station to determine the current state of the plant and performance. The results of the test were compared with the original design base specifications to determine the relevant deficiencies which contribute to high emissions and poor ESP performance. It was aimed to develop an ESP simulation model and validate the outputs with the test data. This study endeavours to demonstrate the greater impact on ESP performance when the ESP is operated outside the design specification. It is further aimed to demonstrate that a solution to the problem of high emissions is not only contributed by the variables within the ESP itself. This study is a coal to stack evaluation considering the ESP variables and the upstream conditions of the ESP that form part of the entire process. The intention of this study is to demonstrate the importance of operating an ESP at the designed parameters and highlight the significance of proper maintenance. It was learned that before any ESP enhancement technology can be implemented, the ESP and upstream conditions must be in accordance with design specifications. The implementation of an ESP enhancement technology will have no merit or justification on a unit that is being operated outside of its design specifications. The results obtained from the ESP simulation model correlated well with the ESP efficiency test data. The expectation of the model to assist operators and engineers to operate ESP’s according to the designer’s specifications was conceded. / MIng (Mechanical Engineering), North-West University, Potchefstroom Campus, 2014

The theme of diploma thesis is a design optimization of air distribution in swimming-pool hall with regard to free water surface evaporation. This problem was solved according to determined criterions with the aid of CFD simulation. Experimental measurement part of the thesis deals with evaporation problems where own formula for this physical phenomenon is determined. This formula is compared with already known algorithms. Author suggests that such formula might be integrated in CFD software.