Há uma concentração de aglomerados globulares moderadamente pobres em metais no bojo galáctico, e muitos deles mostram um Ramo Horizontal Azul (BHB). Essas características juntas apontam para uma idade antiga. Para entender melhor a origem desses aglomerados, o estudo de seu padrão de abundâncias pode ajudar a identificar o tipo das primeiras supernovas nas partes centrais da Galáxia. O NGC 6522 na janela do Baade é um representante desta classe de aglomerados. Análises de abundância de estrelas individuais nesses aglomerados confirmaram sua metalicidade de [Fe/H] -1.0, enriquecimento em elementos-$\\alpha$ e detectaram uma variação nas abundâncias dos elementos pesados de processo-s. Entre os maiores enriquecimentos em Y e Ba, a explicação usual da transferência de massa de uma companheira do ramo assintótico das gigantes pode não se aplicar, e um enriquecimento por estrelas massivas de alta rotação foi sugerido. A fim de estudar melhor as abundâncias em NGC 6522, obtivemos um programa com o FLAMES em 2012, a partir da qual, com os dados de UVES, mostramos que o enriquecimento em elementos-s ainda poderia ser acomodado com o modelo de transferência de massa de uma estrela companheira. Além disso, obtivemos novos dados com o FLAMES em 2016. No presente trabalho analisamos outras 6 estrelas observadas em alta resolução com UVES, e 32 estrelas em resolução média-alta observadas com GIRAFFE, onde foram selecionadas por suas velocidades radiais em torno de -14,3 km/s com uma abrangência de ±15 km/s. Os parâmetros atmosféricos e as abundâncias dos elementos leves C, N, O, elementos de Z ímpar Na e Al, elementos-$alpha$ Mg, Si, Ca, Ti, elementos de pico de ferro Mn, Cu, Zn, elementos de processo-s Y, Zr, Ba, La, Ce, Nd e o elemento de processo-r Eu são derivados para a amostra UVES e preliminarmente para a amostra GIRAFFE. Entre as estrelas UVES, duas delas mostram um enriquecimento significativo nos elementos do processo-s e uma com alto valor nas razões [Y/Ba] e [Zr/Ba], sugerindo um enriquecimento por estrelas massivas de alta rotação. / There is a concentration of moderately metal-poor globular clusters in the Galactic bulge, and many of them show a Blue Horizontal Branch (BHB). These characteristics together point to an old age. In order to better understand the origin of these clusters, the study of their abundance pattern can help identifying the kind of the earliest supernovae in the central parts of the Galaxy. NGC 6522 in Baades Window is a representative of this class of clusters. Abundance analyses of individual stars in this clusters have confirmed its metallicity of [Fe/H]-1.0, enhanced -elements, and detected a variation in the abundances of the s-process heavy elements. Among the highest enhancements of Y and Ba, the usual explanation of mass transfer from a companion in the Asymptotic Giant Branch might not apply, and an enrichment by early fast-rotating massive stars was suggested. In order to further study the abundances in NGC 6522 we obtained a run with FLAMES- UVES in 2012, from which with the UVES data we have shown that the enhancement in s-elements could still be accommodated with the companion transfer model. We further obtained new data with FLAMES-UVES in 2016. In the present work we analyze another 6 stars observed at high resolution with UVES, and 32 stars at medium-high resolution observed with GIRAFFE. The latter were selected from their radial velocities of -14.3±15 km/s. The abundances of the light elements C, N, O, odd-Z elements Na, Al, -elements Mg, Si, Ca, Ti, iron-peak elements Mn, Cu, Zn, s-process elements Y, Zr, Ba, La, Ce, Nd and r-process element Eu are derived. Among the UVES stars, two of them show a significant enrichment in s-process elements and one of them show high [Y/Ba] and [Zr/Ba] ratios, suggesting that an early enrichment by fast rotating massive stars is a probable scenario.

Le réseau d'imageurs Cherenkov atmosphériques HESS (High Energy Stereoscopic System) est présenté. La simulation des gerbes atmosphériques et de l'instrument est détaillée et comparée aux données obtenues pendant les six premiers mois de fonctionnement. Après la présentation des méthodes d'étalonnage et d'extraction du signal gamma, ces techniques sont appliquées aux données prises sur la nébuleuse du Crabe. On obtient un signal significatif permettant d'estimer un flux différentiel à 1 TeV en accord avec les résultats obtenus par d'autres expériences dans le même domaine en énergie. Ces résultats sont exploités pour estimer le potentiel de détection de HESS au signal gamma d'annihilation de neutralinos en provenance du centre galactique et de l'amas globulaire Omega du Centaure. Dans cette étude, une modélisation des halos de matière noire est confrontée aux observations astrophysiques.

High resolution spectra have been analyzed for two and three stars respectively in the candidate extragalactic globular clusters, NGC 5024 and NGC 5466, with the High-Resolution Spectrograph on the 9.2 m Hobby-Eberly Telescope. The goal of this investigation is to evaluate the proposed extragalactic origins of these two globular clusters. Evidence of a tidal tail in NGC 5466 (Belokurov et al., 2006) and the association of NGC 5024 with the Sagittarius stream (Martinez-Delgado et al., 2004) targeted the clusters as likely remnants of recent accretion events and thus potentially of extragalactic origin. Determination of their chemical abundance patterns could provide unique evidence to either support or dispute these claims. NGC 5024 has been associated with a proposed wrap in the Sagittarius stream which could be supported if the chemistry of NGC 5024 is similar to other clusters associated with the stream. NGC 5466 has the longest tidal tail known, which hints at an origin in a now dispersed dwarf spheroidal galaxy. Additional evidence for these clusters' capture origins has been compiled by Yoon & Lee (2002), demonstrating that these two low metallicity clusters, along with five others, are aligned in a single highly inclined plane in the outer halo. Confirmation that these clusters are remnants of dwarf galaxies would support a Galactic history which includes recent accretion events. Such evidence may bolster the cold dark matter hierarchical clustering scenario, which postulates the presence of a significant amount of substructure in the Milky Way. Unfortunately, at the metallicity of the target clusters ([Fe/H] = -1.9), the chemical distinction between Galactic stars and known dSph stars is not significant. The low [alpha/Fe] of dSph stars seen at higher metallicity is not apparent at [Fe/H] = -1.9 in either Galactic or dSph stars. Aside from a few mild discrepancies, NGC 5024 and NGC 5466 appear chemically similar to the Galactic field stars and globular clusters compiled by Pritzl et al. (2005). A moderate enhancement in the [Ba/Y] ratios relative to the halo field stars is the only positively detected chemical signature that is typically observed in dSph stars. Comparisons with Galactic GCs of similar age, metallicity and horizontal branch morphology (NGC 2298, NGC 6397 and NGC 5897) reveal a few other differences, but these could be attributed to systematic effects in the different analysis techniques. Although NGC 5024 has a similar metallicity to the GC Arp 2 that was stripped from the merging Sagittarius dwarf, neither Arp 2 (Mottini et al., 2008) nor the clusters in this study show any particularly unusual chemical abundance patterns. Thus, no conclusive evidence in support of or in opposition to the target clusters' proposed extragalactic origins has been discovered.

Deux systèmes aqueux à 20°C constitués de protéines globulaires de pois et d’alginate de sodium ont été considérés au cours de cette étude, dans des conditions de solvant fixées à pH 7,2 et 0,1 M NaCl. Dans un premier temps, le comportement de phase de globulines faiblement dénaturées (i) ou pré-agrégées thermiquement (ii) en mélange avec de l’alginate a été comparé à différentes échelles d’observation, en termes de diagrammes de phase et de microstructure analysée par microscopie confocale. Attribuée à un phénomène général d’incompatibilité thermodynamique, la séparation de phase a été décrite tout particulièrement sous des aspects morphologiques et cinétiques à l’échelle microscopique, selon la composition de départ en biopolymères et le mode de préparation des globulines. Par la suite, une gélification de chacun des deux systèmes a été opérée à froid, par libération de calcium ionique in situ à partir d’un sel de calcium de carbonate peu soluble au-dessus de pH 7, sous l’effet acidifiant d’une hydrolyse lente de la glucono-δ-lactone (GDL). L’intérêt d’un tel procédé reposait sur l’obtention de gels remplis à mixtes lorsque l’alginate seul ou l’alginate et la phase protéique pouvaient gélifier en présence de calcium. Des corrélations entre propriétés rhéologiques mesurées en régime dynamique (modules G’ et G’’) et données de microstructure ont été effectuées, par l’intermédiaire de l’analyse de texture d’image selon la méthode de cooccurrence. Chaque mélange témoignait d’une séparation de phase bloquée cinétiquement par sa gélification. Par rapport aux gels d’alginate seul ou gels remplis où l’alginate seul pouvait gélifier via le calcium, les gels mixtes témoignaient d’un effet de synergie remarquable d’un point de vue élasticité finale des gels. Dans le même temps, les globulines pré-agrégées ne montraient pas d’aptitude à la gélification selon le procédé appliqué ici. En outre, des effets ségrégatifs induisaient un enrichissement des protéines et du polyoside dans deux phases coexistantes, renforçant de ce fait des interactions entre biopolymères du même type. Les gels mixtes les plus élastiques présentaient une structure enchevêtrée avec un réseau protéique prédominant. Les observations en microscopie électronique à transmission effectuées par un marquage différentiel des deux biopolymères suggèreraient qu’il puisse se former localement des interactions attractives inter-biopolymères, probablement via le calcium, à l’interface des deux phases initialement immiscibles. Ce pontage consoliderait globalement la cohésion entre les deux réseaux protéique et polyosidique / Two aqueous systems at 20°C in 0.1 M NaCl and pH 7.2 containing globular pea proteins and sodium alginate were investigated in this study. First, phase behavior of (i) either low-denatured mixed globulins or (ii) their thermally pre-aggregated counterparts - alginate mixtures was compared using a multi-scale approach, by means of phase diagram and microstructure analysis by confocal microscopy. Thermodynamic incompatibility was the main driving force leading to phase separation within the mixtures, which presented according to their initial biopolymer composition both different morphological and time-evolution features of coexisting phases. Thereafter, a cold-set gelation for each system was performed, as the slow hydrolysis of glucono-δ-lactone (GDL) acidified the media and mediated the release in situ of calcium ions from calcium carbonate, practically insoluble at pH higher than 7. Such procedure would allow gelation via calcium of alginate only or both alginate and the protein phase, giving rise to filled and mixed gels, respectively. An attempt to correlate rheological measurements (G’, G’’ dynamic moduli) with microstructural data was carried out according to image texture analysis by the cooccurrence method. Phase separation was kinetically entrapped by gelation. Compared to single-alginate gels or native globulins-alginate filled gels where alginate was the only gelling agent via calcium, mixed gels reflected in fact great synergism effect regarding final gel elasticity. Meanwhile, pre-aggregated pea globulins could not form a gel with the gelation procedure of choice here. Besides, stronger segregative effects were evidenced by increasing initial biopolymer composition thus enhancing self-biopolymer interaction in their respective enriched-coexisting phases. The strongest mixed gels displayed entangled structure. According to a differential labelling of each incompatible biopolymer, observations with transmission electron microscopy suggested inter-biopolymer attractive interaction at the interface of coexisting phases, probably via calcium cations. Salt-bridging would reinforce cohesiveness between both protein and alginate networks

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Submitted by Fabio Sobreira Campos da Costa (fabio.sobreira@ufpe.br) on 2017-02-21T15:12:08Z No. of bitstreams: 2 license_rdf: 1232 bytes, checksum: 66e71c371cc565284e70f40736c94386 (MD5) Dissertação_JoséVianneyMendonçaDeAlencastroJr.pdf: 648691 bytes, checksum: f2fbc98e547f0284f5aef34aee9249ca (MD5) / Made available in DSpace on 2017-02-21T15:12:08Z (GMT). No. of bitstreams: 2 license_rdf: 1232 bytes, checksum: 66e71c371cc565284e70f40736c94386 (MD5) Dissertação_JoséVianneyMendonçaDeAlencastroJr.pdf: 648691 bytes, checksum: f2fbc98e547f0284f5aef34aee9249ca (MD5) Previous issue date: 2016-09-09 / A lei de Newcomb-Benford, também conhecida como a lei do dígito mais significativo, foi descrita pela primeira vez por Simon Newcomb, sendo apenas embasada estatisticamente após 57 anos pelo físico Frank Benford. Essa lei rege grandezas naturalmente aleatórias e tem sido utilizada por várias áreas como forma de selecionar e validar diversos tipos de dados. Em nosso trabalho tivemos como primeiro objetivo propor o uso de um método substituto ao qui-quadrado, sendo este atualmente o método comumente utilizado pela literatura para verificação da conformidade da Lei de Newcomb-Benford. Fizemos isso pois em uma massa de dados com uma grande quantidade de amostras o método qui-quadrado tende a sofrer de um problema estatístico conhecido por excesso de poder, gerando assim resultados do tipo falso negativo na estatística. Dessa forma propomos a substituição do método qui-quadrado pelo método de Kolmogorov-Smirnov baseado na Função de Distribuição Empírica para análise da conformidade global, pois esse método é mais robusto não sofrendo do excesso de poder e também é mais fiel à definição formal da Lei de Benford, já que o mesmo trabalha considerando as mantissas ao invés de apenas considerar dígitos isolados. Também propomos investigar um intervalo de confiança para o Kolmogorov-Smirnov baseando-nos em um qui-quadrado que não sofre de excesso de poder por se utilizar o Bootstraping. Em dois artigos publicados recentemente, dados de exoplanetas foram analisados e algumas grandezas foram declaradas como conformes à Lei de Benford. Com base nisso eles sugerem que o conhecimento dessa conformidade possa ser usado para uma análise na lista de objetos candidatos, o que poderá ajudar no futuro na identificação de novos exoplanetas nesta lista. Sendo assim, um outro objetivo de nosso trabalho foi explorar diversos bancos e catálogos de dados astronômicos em busca de grandezas, cuja a conformidade à lei do dígito significativo ainda não seja conhecida a fim de propor aplicações práticas para a área das ciências astronômicas. / The Newcomb-Benford law, also known as the most significant digit law, was described for the first time by astronomer and mathematician Simon Newcomb. This law was just statistically grounded after 57 years after the Newcomb’s discovery. This law governing naturally random greatness and, has been used by many knowledge areas to validate several kind of data. In this work, the first goal is propose a substitute of qui-square method. The qui-square method is the currently method used in the literature to verify the Newcomb-Benford Law’s conformity. It’s necessary because in a greatness with a big quantity of samples, the qui-square method can has false negatives results. This problem is named Excess of Power. Because that, we proposed to use the Kolmogorov-Smirnov method based in Empirical Distribution Function (EDF) to global conformity analysis. Because this method is more robust and not suffering of the Excess of Power problem. The Kolmogorov-Smirnov method also more faithful to the formal definition of Benford’s Law since the method working considering the mantissas instead of single digits. We also propose to invetigate a confidence interval for the Kolmogorov-Smirnov method based on a qui-square with Bootstrapping strategy which doesn’t suffer of Excess of Power problem. Recently, two papers were published. I this papaers exoplanets data were analysed and some greatness were declared conform to a Newcomb-Benford distribution. Because that, the authors suggest that knowledge of this conformity can be used for help in future to indentify new exoplanets in the candidates list. Therefore, another goal of this work is explorer a several astronomicals catalogs and database looking for greatness which conformity of Benford’s law is not known yet. And after that , the authors suggested practical aplications for astronomical sciences area.

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Globular clusters are tracers of the formation and evolution of their host galaxies. Kinematics, chemical abundances, age and position of the clusters allows tracing interactions between Milky Way and surrounding galaxies and outlines their chemical enrichment history. In this thesis we analyse mid-resolution spectra of about 800 red giant stars in 51 Galactic globular clusters. It is the first time that [Fe/H] and [Mg/Fe] derived in a consistent way are published for such a huge sample of globular clusters, almost 1/3 of the total number of catalogued clusters. Our metallicities are showed to be more precise than previous works based on mid-resolution spectroscopy. A turnover at [Fe/H] ~ -1.0 is found in the plot [Fe/H] vs. [Mg/Fe] for bulge and halo, although bulge seems to have a more metal-rich turnover, i.e, bulge has more efficient formation than the halo. Comparing the abundances with age the timescale for SNIa to start to become important is 1Gyr. [Fe/H] vs. age corroborates the different star formation efficiency of bulge and halo while [Mg/Fe] does not follow that. Halo was formed in mini halos or dwarf galaxies, and two multiple population clusters had their origin analysed to check it. M 22 seems to have been formed in the Milky Way while NGC 5824 possibly was originated in a dwarf galaxy, although our results are inconclusive for NGC 5824. The Galactic bulge seems to have been formed fast i.e., probably the oldest globular cluster is there. In fact HP 1 has a bluer horizontal branch than expected for its metallicity and we interpret that as an age effect. We determine its distance using light curves of variable stars in order to constrain future age determinations via colour-magnitude diagram. Finally, we investigate interaction between Milky Way and its neighbour galaxy SMC. We find that some star clusters are being stripped out of the SMC main body, which is consistent with tidal stripping scenario for the interaction between the galaxies, instead of ram pressure that would only affect gas. / Aglomerados globulares são traçadores da formação e evolução de suas galáxias. Cinemática, abundâncias químicas, idades e posições dos aglomerados permitem traçar interações entre Via Láctea e galáxias vizinhas e suas histórias de enriquecimento químico. Nesta tese analisamos espectros de média resolução de mais de 800 estrelas gigantes vermelhas em 51 aglomerados globulares Galácticos. É a primeira vez que [Fe/H] and [Mg/Fe] determinados de modo consistente são publicados para uma amostra desse porte, ~1/3 dos objetos catalogados. Nossas metalicidades são mais precisas que trabalhos anteriores similares. Uma quebra em [Fe/H] ~ -1.0 é encontrada no gráfico [Fe/H] vs. [Mg/Fe] para o bojo e halo, embora bojo parece ter uma quebra em [Fe/H] maior, i.e, bojo tem formaçãao mais eficiente que o halo. Comparando abundâncias com idade, a escala de tempo para SNIa ficar importante é 1Gano. [Fe/H] vs. idade corrobora diferentes eficiências de formação do bojo e halo, mas [Mg/Fe] vs. idade não mostra isso. O halo foi formado em mini halos ou galáxias anãs, e dois aglomerados com dispersão em [Fe/H] tiveram suas origens analisadas. M 22 parece ter sido formado na Via Láctea e NGC 5824 possivelmente foi originado em uma galáxia anã, embora os resultados são inconclusivos para NGC 5824. O bojo parece ter sido formado rapidamente e deve possuir o aglomerado mais velho. De fato, HP 1 tem um ramo horizontal mais azul que o esperado para sua metalicidade e vemos isso como um efeito da idade. Determinamos sua distância usando curvas de luz de RR Lyrae de maneira a restringir futuras determinações de idade via diagrama cor-magnitude. Finalmente, investigamos a interação entre Via Láctea e sua galáxia vizinha SMC. Encontramos aglomerados sendo removidos do corpo central da SMC, consistente com cenário de remoção por força de maré para a interação entre as galáxias, em vez de ``ram pressure\'\' que afeta só gás.

Globular clusters are tracers of the formation and evolution of their host galaxies. Kinematics, chemical abundances, age and position of the clusters allows tracing interactions between Milky Way and surrounding galaxies and outlines their chemical enrichment history. In this thesis we analyse mid-resolution spectra of about 800 red giant stars in 51 Galactic globular clusters. It is the first time that [Fe/H] and [Mg/Fe] derived in a consistent way are published for such a huge sample of globular clusters, almost 1/3 of the total number of catalogued clusters. Our metallicities are showed to be more precise than previous works based on mid-resolution spectroscopy. A turnover at [Fe/H] ~ -1.0 is found in the plot [Fe/H] vs. [Mg/Fe] for bulge and halo, although bulge seems to have a more metal-rich turnover, i.e, bulge has more efficient formation than the halo. Comparing the abundances with age the timescale for SNIa to start to become important is 1Gyr. [Fe/H] vs. age corroborates the different star formation efficiency of bulge and halo while [Mg/Fe] does not follow that. Halo was formed in mini halos or dwarf galaxies, and two multiple population clusters had their origin analysed to check it. M 22 seems to have been formed in the Milky Way while NGC 5824 possibly was originated in a dwarf galaxy, although our results are inconclusive for NGC 5824. The Galactic bulge seems to have been formed fast i.e., probably the oldest globular cluster is there. In fact HP 1 has a bluer horizontal branch than expected for its metallicity and we interpret that as an age effect. We determine its distance using light curves of variable stars in order to constrain future age determinations via colour-magnitude diagram. Finally, we investigate interaction between Milky Way and its neighbour galaxy SMC. We find that some star clusters are being stripped out of the SMC main body, which is consistent with tidal stripping scenario for the interaction between the galaxies, instead of ram pressure that would only affect gas. / Aglomerados globulares são traçadores da formação e evolução de suas galáxias. Cinemática, abundâncias químicas, idades e posições dos aglomerados permitem traçar interações entre Via Láctea e galáxias vizinhas e suas histórias de enriquecimento químico. Nesta tese analisamos espectros de média resolução de mais de 800 estrelas gigantes vermelhas em 51 aglomerados globulares Galácticos. É a primeira vez que [Fe/H] and [Mg/Fe] determinados de modo consistente são publicados para uma amostra desse porte, ~1/3 dos objetos catalogados. Nossas metalicidades são mais precisas que trabalhos anteriores similares. Uma quebra em [Fe/H] ~ -1.0 é encontrada no gráfico [Fe/H] vs. [Mg/Fe] para o bojo e halo, embora bojo parece ter uma quebra em [Fe/H] maior, i.e, bojo tem formaçãao mais eficiente que o halo. Comparando abundâncias com idade, a escala de tempo para SNIa ficar importante é 1Gano. [Fe/H] vs. idade corrobora diferentes eficiências de formação do bojo e halo, mas [Mg/Fe] vs. idade não mostra isso. O halo foi formado em mini halos ou galáxias anãs, e dois aglomerados com dispersão em [Fe/H] tiveram suas origens analisadas. M 22 parece ter sido formado na Via Láctea e NGC 5824 possivelmente foi originado em uma galáxia anã, embora os resultados são inconclusivos para NGC 5824. O bojo parece ter sido formado rapidamente e deve possuir o aglomerado mais velho. De fato, HP 1 tem um ramo horizontal mais azul que o esperado para sua metalicidade e vemos isso como um efeito da idade. Determinamos sua distância usando curvas de luz de RR Lyrae de maneira a restringir futuras determinações de idade via diagrama cor-magnitude. Finalmente, investigamos a interação entre Via Láctea e sua galáxia vizinha SMC. Encontramos aglomerados sendo removidos do corpo central da SMC, consistente com cenário de remoção por força de maré para a interação entre as galáxias, em vez de ``ram pressure\'\' que afeta só gás.