In recent years, additive manufacturing (AM) has become one of the most revolutionary and promising technologies in manufacturing. The process of making a product layer by layer is also often referred to as 3D printing. Once employed purely for prototyping, AM is now increasingly used for small series production, for example in aerospace applications. The paper starts with a motivation for AM in hydraulic applications and the development of an AM internal gear pump. For a better understanding of the manufacturing process, a brief introduction to AM highlighting the advantages and challenges is given. The AM internal gear pump is part of an electrohydraulic power pack, which is used to power an electrohydraulic actuator (EHA). The power pack contains all necessary peripherals to realise the hydraulic system of the EHA. The AM process allows for new design possibilities, but the process differs strongly compared to subtractive manufacturing processes and therefore is outlined here. The paper concludes by presenting measurement results of the AM internal gear pump.

Additive manufacturing (AM) is a promising manufacturing process that provides that ability to fabricate components with complex geometries with relatively low lead times compared to other manufacturing processes. This allows for more freedom of design, as prototypes can easily be produced throughout the development process. AM is also especially beneficial in tooling applications, where internal geometries such as cooling channels are required in order to improve the quality of the manufactured parts. These geometries are more difficult to produce with more conventional manufacturing methods such as forging or casting. Currently, Laser Powder Bed Fusion (LPBF) shows the most promise in the field of Additive Manufacturing (AM) of metals, as it offers the freedom to produce complex components with little post processing required. Additionally, post processing with Hot Isostatic Pressing (HIP) can be implemented to significantly enhance the final properties of the material.  The LPBF-process can produce many different defects within the parts such as: part porosity and lack of fusion. This is mainly due to the layer-by-layer configuration of the process. Parts can also experience large thermal fluctuations and rapid cooling rates which can generate large residual stresses. This can result in significant cracking in certain high alloyed materials which can impact part quality and  material properties. If the cracking is severe enough, it will result in failure of the entire component and render the entire parts completely useless. Post processing with HIP may remove some of these defects and reduce the residual stresses in the material and thus produce a material with properties that are satisfactory. The purpose of this thesis is to investigate the processability of a high alloy cold work tool steel with LPBF. The main focus is the influence of the processing parameters and part geometry on the quality of the produced parts. Furthermore, the influence of the processing parameters on defects and microstructure will also be investigated. The aim is to produce parts that can be enhanced with HIP as a post processing treatment. Additionally, the impact of HIP on the properties of the part will also be investigated in order to determine if the there are any improvements in terms ofreduction in part defects and the removal of any undesired microstructural features which are produced from the process. The experimental results showed that the processability of the tool steel is difficult. Several sample volumes were produced with varying processing parameters and scanning strategies, and all the specimens from all sample volumes exhibited some cracking. Parts produced with a combination of contouring and hatching strategy, where there is an internal structure showed the most promise, as these parts exhibited the least amount of severe cracking. However, additional research of the processing parameters and scanning strategies is required in order to reduce the amount of cracking of the external shell structure and thus, achieve proper densification of the parts when post processing with HIP. / Additiv tillverkning (AM) är en lovande tillverkningsprocess som ger möjligheten att tillverka komponenter med komplexa geometrier med relativt låga ledtider jämfört med andra tillverkningsprocesser. Detta ger större frihet i under designprocessen eftersom prototyper enkelt kan produceras under hela utvecklingsprocessen. AM är också särskilt fördelaktigt i verktygstillämpningar, där interna geometrier såsom kylkanaler krävs för att förbättra kvaliteten på de tillverkade delarna. Dessa geometrier är svårare att tillverka med mer konventionella tillverkningsmetoder som smidning eller gjutning. För närvarande visar det sig att Laser Powder Bed Fusion (LPBF) är det mest lovande inom området additiv tillverkning av metaller, eftersom processen erbjuder friheten att producera komplexa komponenter samt att efterbearbetning som krävs blir mindre. Dessutom kan efterbearbetning med Hot Isostatic Pressing (HIP) implementeras för att avsevärt förbättra materialets slutliga egenskaper. LPBF-processen kan ge upphov till många olika defekter i delarna såsom: delporositet och lack of fusion. Detta beror främst på att processen sker lagervis vilket kan ge upphov att många småfel. Delar kan också uppleva stora termiska fluktuationer och snabba kylningshastigheter som kan generera stora restspänningar. Det kan resultera i stor sprickbildning i vissa höglegerade material vilket kan påverka delarnas kvalitet och materialegenskaper. Om sprickorna som bildas är stora eller djupa nog kommer detta att resultera i att hela komponenten blir oanvändbar. Efterbearbetning med HIP kan ta bort en del av dessa defekter och minska restspänningarna i materialet och därmed producera ett material med goda egenskaper. Syftet med detta arbete är att undersöka bearbetbarheten hos ett höglegerat kallbearbetningsstål med som produceras med LPBF. Huvudfokus är påverkan av processparametrar och detaljgeometrin på kvaliteten på de producerade delarna. Vidare kommer också processparametrarnas inverkan på defekter och mikrostruktur att undersökas. Syftet är att producera delar som kan förbättras med HIP som efterbehandlingsbehandling. Dessutom kommer effekterna av HIP på delens egenskaper också att undersökas för att avgöra om det finns några förbättringar i termer av minskning av deldefekter och avlägsnande av alla oönskade mikrostrukturella egenskaper som produceras från processen. De experimentella resultaten visade att verktygsstålets bearbetbarhet är svår. Flera provvolymer producerades med varierande processparametrar och skanningsstrategier, och alla prover från alla provvolymer uppvisade viss sprickbildning. Delar som tillverkats med en kombination av kontur och hatch, där det finns en inre struktur visade sig mest lovande, eftersom dessa delar uppvisade minst sprickbildning. Ytterligare arbete av processparametrarna och skanningsstrategier krävs dock för att minska mängden sprickbildning i den yttre skalstrukturen och därmed uppnå korrekt förtätning av delarna vid efterbearbetning med HIP.

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Additive manufacturing (AM) – and laser powder bed fusion (LPBF) specifically – constructs geometry that would not be possible using standard manufacturing techniques. This geometric versatility allows integration of multiple components into a single part. While this practice can reduce weight and part count, there are also serious drawbacks. One is that the LPBF process can only build parts with a single material. This limitation generally results in over-designing some areas of the part to compensate for the compromise in material choice. Over-designing can lead to decreased functional efficiency, increased weight, etc. in LPBF parts. Methods to control the material composition spatially throughout a build would allow designers to experience the full benefits of functionality integration. Spatial composition control has been performed successfully in other AM processes – like directed energy deposition and material jetting – however, these processes are limited compared to LPBF in terms of material properties and can have inferior spatial resolution. This capability applied to the LPBF process would extend manufacturing abilities beyond what any of these AM processes can currently produce. A novel concept for spatial composition control – currently under development at Brigham Young University – utilizes liquid or liquid-encased dopants to selectively alter the composition of the powder bed, which is then fused with the substrate to form a solid part. This work is focused on evaluating the feasibility and usefulness of this novel composition control process. To do this, the present work evaluates two deposition methods that could be used; explores and maps the laser parameter process space for zirconia-doped SS 316L; and investigates the incorporation of zirconia dopant into SS 316L melt pools. In evaluating deposition methods, inkjet printing is recommended to be implemented as it performs better than direct write material extrusion in every assessed category. For the process space, the range of input parameters over which balling occurred expanded dramatically with the addition of zirconia dopant and shifted with changes in dopant input quantities. This suggests the need for composition-dependent adjustments to processing parameters in order to obtain desired properties in fused parts. Substantial amounts of dopant material were confirmed to be incorporated into the laser-fused melt tracks. Individual inclusions of 100 $nm$ particles distributed throughout the melt pool in SEM images. Howewver, EDX data shows that the majority of the incorporated dopant material is located around the edges of the melt pools. Variations of dopant deposition, drying, and laser scanning parameters should be studied to improve the resulting dopant incorporation and dispersion in single-track line scans. Area scans and multi-layer builds should also be performed to evaluate their effect on dopant content and dispersion in the fused region.

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This study aims to improve the Additive Manufacturing (AM) design space for the popular multi-component Ni alloy Inconel 625 (IN625) thorough investigating the microstructural evolution, namely the solidification microstructure and the solid-state phase transformations during the Laser Powder Bed Fusion (LPBF) process. Highly non-equilibrium solidification and the complex reheating conditions during the LPBF process result in the formation of various types of solidification microstructures and grain morphologies which consequently lead to a wide range of mechanical properties. Understanding the melt’s thermal conditions, alloy chemistry, and thermodynamics during the rapid solidification and solid-state phase transformation in AM process will help to control material properties and even produce a material with specific microstructural features suited to a given application. This research helps to better understand the process-microstructure-property relationships of LPBF IN625. First, a set of simple but effective analytical solidification models were employed to evaluate their ability to predict the solidification microstructure in AM applications. As a case study, Solidification Microstructure Selection (SMS) maps were created to predict the solidification growth mode and grain morphology of a ternary Al-10Si-0.5Mg alloy manufactured by the LPBF process. The resulting SMS maps were validated against the experimentally obtained LPBF microstructure available in the literature for this alloy. The challenges, limitations, and potential of the SMS map method to predict the microstructural features in AM were comprehensively discussed. Second, The SMS map method was implemented to predict the solidification microstructure and grain morphology in an LPBF-built multi-component IN625 alloy. A single-track LPBF experiment was performed utilizing the EOSINT M280 machine to evaluate the SMS map predictions. The resulting microstructure was characterized both qualitatively and quantitatively in terms of the solidification microstructure, grain morphology, and Primary Dendrite Arm Spacing (PDAS). Comparing the experimentally obtained solidification microstructure to the SMS map prediction, it was found that the solidification mode and grain morphology were correctly predicted by the SMS maps. Although the formation of precipitates was predicted using the CALculation of PHAse Diagrams (CALPHAD) approach, it was not anticipated from the analytical solution results. Third, to further investigate the microsegregation and precipitation in IN625, Scanning Transmission Electron Microscopy (STEM) using Energy-Dispersive X-ray Spectroscopy (EDS), High-Angle Annular Dark-Field Scanning Transmission Electron Microscopy (HAADF-STEM), Scheil-Gulliver (with solute trapping) model, and DIffusion-Controlled TRAnsformations (DICTRA) method were employed. It was found that the microstructural morphology mainly consists of the Nickel-Chromium (gamma-FCC) dendrites and a small volume fraction of precipitates embedded into the interdendritic regions. The precipitates predicted with the computational method were compared with the precipitates identified via HAADF-STEM analysis inside the interdendritic region. The level of elemental microsegregation was overestimated in DICTRA simulations compared to the STEM-EDS results; however, a good agreement was observed between the Scheil and STEM-EDS microsegregation estimations. Finally, the spatial variations in mechanical properties and the underlying microstructural heterogeneity of a multi-layer as-built LPBF part were investigated to complete the process-structure-properties relationships loop of LPBF IN625. Towards this end, numerical thermal simulation, electron microscopy, nano hardness test, and a CALPHAD approach were utilized to investigate the mechanical and microstructural heterogeneity in terms of grain size and morphology, PDAS, microsegregation pattern, precipitation, and hardness along the build direction. It was found that the as-built microstructure contained mostly columnar (Nickel–Chromium) dendrites were growing epitaxially from the substrate along the build direction. The hardness was found to be minimum in the middle and maximum in the bottom layers of the build’s height. Smaller melt pools, grains, and PDAS and higher thermal gradients and cooling rates were observed in the bottom layers compared to the top layers. Microsegregation patterns in multiple layers were also simulated using DICTRA, and the results were compared with the STEM-EDS results. The mechanism of the formation of precipitates in different regions along the build direction and the precipitates’ corresponding effects on the mechanical properties were also discussed. / Thesis / Doctor of Philosophy (PhD)

<p dir="ltr">The increasing use of additive manufacturing technologies such as Laser Powder Bed Fusion (LPBF) has enabled the manufacturing of parts with complex features such as optimized cooling channels. However, due to the layer-by-layer deposition of LPBF requiring an approximation of design intent, cooling channels manufactured by LPBF are affected by surface roughness effects and manufacturing inaccuracies. Consequently, the effect of implementing them on the mechanical properties of parts should be studied to understand their limits of applicability. This study aims to determine the effect of helical cooling channels in LPBF GRCop-42 specimens on their high-cycle fatigue properties. We present monotonic tensile testing and high-cycle fatigue testing results for three specimen types (no channel, straight channel and helical channel) of LPBF GRCop-42 under uniaxial loading, tested at two temperature conditions (room and 500°C). We show that at room temperature, the no channel specimens had the highest fatigue strength, followed by the straight channel and then helical channel specimens. The relative significance of potential causes for the detriment in fatigue life for the straight and helical channeled specimens were quantified using finite element analysis (FEA) and analytical fatigue models (based on Murakami-type defect corrections), and the findings from this analysis were validated by experimental observations from fracture surface analysis. Our results demonstrate that for the straight channel specimens, manufacturing-induced porosity around the channel is relatively a stronger driver for the detriment of fatigue life, compared to surface roughness. For the helical channel specimens, intended to simulate complex cooling channels in real-world applications, the effects of surface roughness combined with multiaxial stress concentrations around the channel were the primary driver for the lesser fatigue life. We anticipate our results will be useful for designers and manufacturers of LPBF components with complex features, and those involved in the potential implementation of LPBF GRCop-42 parts in high-cycle fatigue applications.</p>

The rise of additive manufacturing has enabled new degrees of freedom in terms of design and functionality. In this context, this contribution addresses the design and characterization of structural unit cells that are intended as building blocks of highly porous lattice structures with tailored properties. While typical lattice structures are often composed of gyroid or diamond lattices, this study presents stackable unit cells of different sizes created by a generative design approach tomeet boundary conditions such as printability and homogeneous stress distributions under a given mechanical load. Suitable laser powder bed fusion (LPBF) parameterswere determined forAlSi10Mg to ensure high resolution and process reproducibility for all considered unit cells. Stacks of unit cells were integrated into tensile and pressure test specimens for which the mechanical performance of the cells was evaluated. Experimentally measured material properties, applied process parameters, and mechanical test results were employed for calibration and validation of finite element (FE) simulations of both the LPBF process as well as the subsequent mechanical characterization. The obtained data therefore provides the basis to combine the different unit cells into tailored lattice structures and to numerically investigate the local variation of properties in the resulting structures. / Durch die Einführung der Additiven Fertigung können neue Freiheitsgrade in Bezug auf Gestaltungsfreiheit und Funktionalität erreicht werden. In diesem Zusammenhang adressiert dieser Beitrag das Design und die Charakterisierung struktureller Einheitszellen als Bausteine für hochgradig poröse Gitterstrukturen mit maßgeschneiderten Eigenschaften. Während typische Gitterstrukturen oft auf Gyroid- oder Diamantstrukturen basieren, präsentiert dieser Beitrag stapelbare Einheitszellen unterschiedlicher Größe, die durch einen generativen Designansatz erstellt wurden. Hierdurch sollen verschiedene Randbedingungen wie eine gute Druckbarkeit und homogene Spannungsverteilung unter gegebenen mechanischen Lasten erreicht werden. Um eine hohe Auflösung und Reproduzierbarkeit der Einheitszellen zu erreichen, wurden für den verwendeten Werkstoff AlSi10Mg geeignete Druckparameter für das Laserstrahlschmelzen (LPBF) ermittelt. Stapel von Einheitszellen wurden in Zug- und Druckproben integriert, anhand derer die mechanische Stabilität der Zellen ermittelt wurde. Experimentell bestimmte Materialeigenschaften, die verwendeten Prozessparameter und die Ergebnisse der mechanischen Untersuchungen wurden anschließend für die Kalibrierung und Validierung Finiter Elemente (FE) Simulationen herangezogen, wobei simulationsseitig sowohl der Prozess des Laserstrahlschmelzens als auch die nachgelagerte mechanische Charakterisierung berücksichtigt wurden. Die hier präsentierten Ergebnisse sollen als Basis sowohl für eine gezielte Anordnung der Einheitszellen zu maßgeschneiderten Gitterstrukturen dienen als auch für die numerische Auswertung der lokal variierenden Eigenschaften der somit resultierenden Strukturen.

Today's economic and ecological directives demand for highly sustainable machine parts by low production cost and energy consumption. Consequently, it is crucial to guarantee a long service life by protecting all components against wear and corrosion. However, hydraulic components always include stressed surfaces, which suffer from heavy loads at high relative speeds. To prevent fretting, coating processes like thermal spraying or hard chrome have a long history in the field of hydraulics. New additive laser-based processes like EHLA and LPBF offer the potential to apply new coatings without environmentally hazardous substances such as chromium or to manufacture complex parts with new functionalities. So far, additively manufactured surfaces with relative movements are post-processed to obtain surface qualities similar to subtractive methods, as the tribological properties of additive surfaces have not been investigated to date. Therefore, this paper investigates the frictional behavior of 316L surfaces produced by laser-based EHLA and LPBF processes using a disc-disc tribometer.

No description available.