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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.
51

Radical Hotel : En affärsplan

Thunholm, Mattias, Boström, Marcus January 2008 (has links)
<p>Vi åsyftar att undersöka möjligheterna att starta upp och driva det mindre hotellet. Vi vill med denna affärsplan undersöka marknaden och upptäcka eventuella brister i idén före den blir verklighet.</p><p>Frågeställning: Hur etableras och drivs det mindre hotellet på ett framgångsrikt sätt?</p><p>Vi har gjort en kvalitativ fallstudie på tre hotellföretag och använts oss av semi-strukturerade intervjuer med berörda personer på de tre olika hotellen. Teorin har insamlats genom relevant litteratur inom ekonomi och marknadsföring samt via elektroniska källor.</p><p>Vi har visat på att det finns goda möjligheter att skapa en hotellverksamhet i en stad som Göteborg. Dock under vissa förutsättningar; att vi får tag i en lokal som passar våra behov samt att vi får en omsättningsbaserad hyra så vi slipper tunga investeringskostnader.</p>
52

Design of filter cloth analyser : Development of a portable filter cloth selection tool for filters used to regenerate the acid used in the pickling process during the production of  stainless steel

Andersson Egerlid, Axel, Westin, Fredrik January 2018 (has links)
The stainless steel industry is an industry which manufactures one of the most used ma-terials in the world. Even though the vast size of the industry many might not reflect werethe steel comes from when buying their IKEAcutlery etc. But in fact this industry is moreintricate and complex than one might think.During the manufacturing process, the steelgoes through several processes. One of thoseprocesses is done by treating the steel withstrong acid. This chemical process is calledpickling. The pickling process is what createsthe characteristic smooth and shiny surface ofa product made in stainless steel.This thesis is about the development of a testunit that is able to effectively test the ASRA(Acid Sludge Removal Apparatus) filter cloths.The ASRA is a filtration system developed by Scanacon in Stockholm that filtrates and puri-fies acid that is used during the pickling pro-cess of a steel manufacture process. Today, it is complicated, time consuming and dangerous totest and evaluate different filter cloths in orderto find the cloth that provides the best result,since the tests has to be conducted on the realsystems. The aim of this thesis was therefore tosolve these problems. Scanacon wanted to findan alternative solution, that would not includeinteraction with the real filtration system. Theyalso wanted a portable and safe solution. To solve the problem a iterative design pro-cess called RDCD which stands for research, design, create &amp; delivery was developed. Theprocesses was heavily influenced by the CDIO process (Conceive, Design, Implement &amp; Ope-rate). After the research phase was conducted it was decided that a small filter analysis productwould be the best way to solve the problem. The product was then developed one com-ponent at a time. During the project several prototypes and test was created and conductedin order to validate the design.The result is a small filtration unit speciallydesigned to simulate the ASRA system. Theproduct is able to rapidly test various filtercloths in an easy way, without putting the user in harm’s way. After the tests has been perfor-med can the user can identify which cloth that worked the best. The product is small enoughto be possible to be carried in a hard case bag,which in turn affords portability. / Stålindustrin är en industri som tillverkar ettav de mest använda materialen i världen. Trotsindustrins enorma storlek är det kanske intemånga som reflekterar varifrån stålet kommerifrån när man köper exempelvis IKEA bestick.Men faktum är att den här industrin är mycketmer invecklad och komplex än vad man kan tro. Under tillverkningsprocessen går stålet ige-nom flera processer. En av de här processerna genomförs genom att behandla stålet med starksyra. Den kemiska processen kallas för betningoch är det som ger en produkt tillverkad i stålden karaktäristiska lena och glänsande ytan. Den här examensrapporten handlar om ut-vecklandet av en test enhet som effektivt kan testa filter dukarna till ASRA (Acid SludgeRemoval Apparatus) systemet. ASRA systemetär ett filtreringssystem utvecklat av Scanaconi Stockholm som filtrerar och renar syran som används under betningsprocessen vid stål-tillverkning. Idag är det komplicerat, tidskrä-vande och farligt att testa och utvärdera olika filterdukar för att ta reda på vilken duk somger bäst resultat, eftersom att testerna måstegenomföras på de riktiga systemen. Målet fördet här examensarbetet var därför att lösa dehär problemen. Scanacon ville ha en alternativlösning som inte kräver interaktion med deriktiga systemen. De ville också ha en portabeloch säker lösning. För att lösa problemet utvecklades en itera-tiv designprocess kallad RDCD som står för research, design, create &amp; delivery. Processen var tungt influerat av CDIO (Conceive, De-sign, Implement &amp; Operate) processen. Efter att researchfasen var genomförd bestämdesdet att en liten filteranalysatorprodukt var detbästa sättet att lösa problemet på. Produktenutvecklades sedan en komponent i taget. Underprojektets gång har flera prototyper byggts och flera tester genomförts för att validera designen. Resultatet är en liten filtreringsenhet som är specialdesignad för att simulera ASRA syste-met. Produkten kan snabbt testa oliak filterdu-kar på ett enkelt sätt, utan utsätta användaren för fara. Efter att testerna genomförts kananvändaren identifiera vilken duk som funkatbäst. Produkten är tillräckligt liten för att fåplats i en hårdplast väska, vilket ger produktenden efterfrågade portabiliteten.
53

Formal Modeling Can Improve Smart Transportation Algorithm Development

Wathugala, Wathugala Gamage Dulan Manujinda 06 1900 (has links)
201 pages / Ensuring algorithms work accurately is crucial, especially when they drive safety critical systems like self-driving cars. We formally model a published distributed algorithm for autonomous vehicles to collaborate and pass thorough an intersection. Models are built and validated using the “Labelled Transition System Analyser” (LTSA). Our models reveal situations leading to deadlocks and crashes in the algorithm. We demonstrate two approaches to gain insight about a large and complex system without modeling the entire system: Modeling a sub system - If the sub system has issues, the super system too. Modeling a fast-forwarded state - Reveals problems that can arise later in a process. Some productivity tools developed for distributed system development are also presented. Manulator, our distributed system simulator, enables quick prototyping and debugging on a single workstation. LTSA-O, extension to LTSA, listens to messages exchanged in an execution of a distributed system and validates it against a model.
54

Nova metodologia para o desenvolvimento de inferências baseadas em dados

Fleck, Thiago Dantas January 2012 (has links)
As inferências têm diversas aplicações na indústria de processos químicos, sendo essenciais no sucesso de projetos de controle avançado. O desempenho do controle será sempre ligado ao desempenho da inferência, sendo importante a manutenção da sua qualidade ao longo do tempo. Neste trabalho, uma nova metodologia é sugerida para o desenvolvimento de inferências baseadas em dados seguindo uma abordagem segmentada com o objetivo de facilitar a sua manutenção. A nova proposta consiste em modelar a parte estacionária separada da parte dinâmica, diferentemente do que é feito na metodologia tradicional, onde o modelo dinâmico é gerado diretamente dos dados de processo. O modelo estacionário é obtido através de uma regressão PLS (Partial Least Squares), enquanto as dinâmicas são inseridas posteriormente utilizando-se um algoritmo de otimização. A técnica é aplicada a uma coluna de destilação e o resultado obtido é semelhante ao de inferências dinâmicas e estáticas desenvolvidas com métodos tradicionais. Outras etapas do desenvolvimento de inferências também são investigadas. Na seleção de variáveis, métodos estatísticos são comparados com a busca exaustiva e se conclui este último deve ser usado como padrão, visto que custo computacional não é mais um problema. Também são apresentadas boas práticas no pré-tratamento de dados, remoção do tempo morto do cromatógrafo modelado e detecção de estados estacionários. / Soft-sensors have several applications in the chemical processes industry and are essential for the success of advanced control projects. Its performance will always be linked to the performance of the soft-sensor, so it is important to maintain its quality over time. In this paper, a new methodology is suggested for the development of data-based soft-sensors following a segmented approach in order to facilitate its maintenance. The new proposal is to model the stationary part separated from the dynamic, unlike the traditional methodology where the dynamic model is generated directly from process data. The stationary model is obtained by a PLS (Partial Least Squares) regression, while the dynamics are inserted using an optimization algorithm. The technique is applied to a distillation column and its performance is similar to dynamic and static soft-sensors developed using traditional methods. Other steps in the development of soft-sensors are also investigated. In variable selection issue, statistical methods are compared with the testing of all possibilities; the latter should be used as default, since computational cost is no longer a problem. We also present best practices in data pre-processing, gas chromatograph dead-time removal and steady state detection.
55

Nova metodologia para o desenvolvimento de inferências baseadas em dados

Fleck, Thiago Dantas January 2012 (has links)
As inferências têm diversas aplicações na indústria de processos químicos, sendo essenciais no sucesso de projetos de controle avançado. O desempenho do controle será sempre ligado ao desempenho da inferência, sendo importante a manutenção da sua qualidade ao longo do tempo. Neste trabalho, uma nova metodologia é sugerida para o desenvolvimento de inferências baseadas em dados seguindo uma abordagem segmentada com o objetivo de facilitar a sua manutenção. A nova proposta consiste em modelar a parte estacionária separada da parte dinâmica, diferentemente do que é feito na metodologia tradicional, onde o modelo dinâmico é gerado diretamente dos dados de processo. O modelo estacionário é obtido através de uma regressão PLS (Partial Least Squares), enquanto as dinâmicas são inseridas posteriormente utilizando-se um algoritmo de otimização. A técnica é aplicada a uma coluna de destilação e o resultado obtido é semelhante ao de inferências dinâmicas e estáticas desenvolvidas com métodos tradicionais. Outras etapas do desenvolvimento de inferências também são investigadas. Na seleção de variáveis, métodos estatísticos são comparados com a busca exaustiva e se conclui este último deve ser usado como padrão, visto que custo computacional não é mais um problema. Também são apresentadas boas práticas no pré-tratamento de dados, remoção do tempo morto do cromatógrafo modelado e detecção de estados estacionários. / Soft-sensors have several applications in the chemical processes industry and are essential for the success of advanced control projects. Its performance will always be linked to the performance of the soft-sensor, so it is important to maintain its quality over time. In this paper, a new methodology is suggested for the development of data-based soft-sensors following a segmented approach in order to facilitate its maintenance. The new proposal is to model the stationary part separated from the dynamic, unlike the traditional methodology where the dynamic model is generated directly from process data. The stationary model is obtained by a PLS (Partial Least Squares) regression, while the dynamics are inserted using an optimization algorithm. The technique is applied to a distillation column and its performance is similar to dynamic and static soft-sensors developed using traditional methods. Other steps in the development of soft-sensors are also investigated. In variable selection issue, statistical methods are compared with the testing of all possibilities; the latter should be used as default, since computational cost is no longer a problem. We also present best practices in data pre-processing, gas chromatograph dead-time removal and steady state detection.
56

Le spectromètre thermophorétique circulaire, un nouvel instrument pour mesurer la thermophorèse : application aux agrégats de suies de morphologie fractale / The spectromètre thermophorétique circulaire (SMTC), a new device for the study of the thermophoresis : Application on the fractals soot particles

Brugière, Edouard 03 December 2012 (has links)
Dans le but de montrer l’influence de la morphologie fractale d’un agrégat sur son comportement thermophorétique, un nouveau dispositif expérimental a été développé ; le SpectroMètreThermophorétique Circulaire (SMTC). Cet instrument permet de mesurer la vitesse moyenne de thermophorèse des particules dans une zone de sélection comprise entre une plaque chaude et une plaque froide. Pour cela, nous avons développé une fonction de transfert spécifique au principe de l’instrument sur la base des travaux existant sur les analyseurs différentiels de mobilité électrique.Une qualification expérimentale du SMTC a été réalisée avec des billes de latex monodispersées de tailles comprises entre 64 nm et 500 nm. Le bon accord entre les vitesses de thermophorèse obtenues et la théorie de Beresnev et Chernyak (1995) nous a permis de valider le fonctionnement de l’instrument.Par la suite, nous avons comparé les vitesses de thermophorèse expérimentales obtenues avec le SpectroMètre Thermophorétique Circulaire pour des particules sphériques et des agrégats produits par un générateur d’aérosol à combustion. Contrairement aux résultats obtenus avec les billes de latex, nous observons une augmentation de la vitesse de thermophorèse des agrégats avec leur diamètre de mobilité électrique.Grâce à une étude morphologique des agrégats, nous avons remarqué que la vitesse de thermophorèse est dépendante du nombre de particules primaires de l’agrégat. Ces résultats expérimentaux confirment pour la première fois les données théoriques de Mackowski (2006)obtenues par des simulations Monte-Carlo. De plus, une comparaison avec les travaux de Messerer et al. (2003) montre que la vitesse de thermophorèse des agrégats semble indépendante de la taille des particules primaires. / In order to show the influence of the morphology of a fractal aggregate on its thermophoretic behavior, a new experimental device has been developed; the SpectroMètre ThermophorétiqueCirculaire (SMTC). This instrument is used to measure the mean thermophoretic velocity of particles selected between a hot plate and a cold plate thanks to a transfer function based on the geometry of the radial flow differential mobility analyser RF-DMA or SMEC (Spectromètre de Mobilité Electrique Circulaire). For the experimental validation, effective thermophoretic velocities of monodispersed spherical latex particles for diameters ranging from 64 nm to 500 nm and a temperature gradient equal to 50 750 K/m are measured and compared with theoretical values. The good agreement between the experimentals results and theoretical values of Beresnev and Chernyak (1995) helps us to validate the operation of the instrument.Then we compare experimental thermophoretic velocity obtained with the SMTC for spherical particles and aggregates produced by a combustion aerosol generator. Contrary to the results obtained with the PSL particles, we observe that the thermophoretic velocity of aggregates increases with the electrical mobility diameter. Thanks to a morphological study of the aggregates, we showed that the thermophoretic velocity depends on the number of primary particles of the aggregate. These experimental results confirm,for the first time, the theoretical data of Mackowski (2006) obtained by a Monte Carlo simulation. Moreover, a comparison with the experimental results of Messerer et al. (2003) shows that thethermophoretic velocity of aggregates seems independent of the primary particle size.
57

Warhead penetration in concrete protective structures

Hansson, Håkan January 2011 (has links)
The analysis of penetration of warheads in concrete protective structures is an important part of the study of weapon effects on protective structures. This type of analysis requires that the design load in the form of a warhead is determined, and its characteristic and performance within a protective structure is known. Constitutive equations for concrete subjected to weapon effects have been a major area of interest for a long time, and several material models for concrete behaviour are developed. However, it is not until recent years that it has been possible to use finite element (FE) analyses to simulate the behaviour of concrete targets during projectile penetration with acceptable results. The reason for this is a combination of several factors, e.g. development of suitable material models for concrete, enhancement of numerical methodology and affordable high capacity computer systems. Furthermore, warhead penetration has primary been of interest for the armed forces and military industry, with a large part of the conducted research being classified during considerable time. The theoretical bases for concrete material behaviour and modelling with respect to FE analyses of projectile penetration are treated in the thesis. The development of weapons and fortifications are briefly discussed in the thesis. Warheads may be delivered onto a protective structure by several means, e.g. artillery, missiles or aerial bombing, and two typical warhead types were used within the study. These warhead types were artillery shells and unitary penetration bombs for the use against hardened targets, with penetration data for the later warhead type almost non-existing in the literature. The penetration of warheads in concrete protective structures was therefore studied through a combination of experimental work, empirical penetration modelling and FE analyses to enhance the understanding of the penetration phenomenon. The experimental data was used for evaluation of empirical equations for concrete penetration and FE analyses of concrete penetration, and the use of these methods to predict warhead penetration in protective structures are discussed within the thesis. The use of high performance concrete increased the penetration resistance of concrete targets, and the formation of front and back face craters were prevented with the use of heavily reinforced normal strength concrete (NSC) for the targets. In addition, the penetration depths were reduced in the heavily reinforced NSC. The evaluated existing empirical penetration models did not predict the behaviour of the model scaled hardened buried target penetrators in concrete structures with acceptable accuracy. One of the empirical penetration models was modified to better describe the performance of these penetrators in concrete protective structures. The FE analyses of NSC gave reasonable results for all simulation cases, with the best results obtained for normal impact conditions of the penetrators. / Analyser avseende stridsdelars penetration i skyddskonstruktioner av betong viktigt för studier av vapenverkan mot skyddskonstruktioner. Dessa analyser förutsätter att dimensionerande last i form av stridsdel bestäms, samt att dess karakteristik och verkan mot skyddskonstruktioner är kända. Konstitutiva modeller för betong utsatta för vapenverkan har varit av stort intresse under en lång tid och ett flertal materialmodeller har utvecklats. Det är emellertid först på senare år som det varit möjligt att använda finita element (FE) analyser for att simulera beteendet för betongmål vid projektilpenetration med acceptabla resultat. Anledningen till detta kan tillskrivas kombinationen av ett flertal faktorer, t ex utvecklingen av lämpliga materialmodeller, förbättringar av numerisk metodik och utvecklingen av kostnadseffektiva beräkningsdatorer. Penetration av stridsdelar har dessutom i huvudsak varit av intresse för militären och försvarsindustrin, vilket har resulterat i att en stor del av den bedrivna forskningen har varit hemligstämplad under lång tid. Grunderna avseende betongs materialbeteende och beskrivning av detta med avseende på FE-analyser av projektilpenetration behandlas i denna licentiatuppsats. Den fortifikatoriska utvecklingen och utvecklingen av vapen diskuteras kortfattad i uppsatsen. Ett flertal olika typer av stridsdelar är av intresse avseende verkan mot skyddskonstruktioner, t ex artillerigranater, missiler eller flygbomber. I denna studie beaktades två typiska stridsdelar, artillerigranater och penetrerande bomber. De senare är specifikt konstruerade för användande mot skyddskonstruktioner och företrädesvis mot betongkonstruktioner. Det visade sig dessutom att data avseende penetration i betong för denna typ av penetrerande stridsdelar i stort sett inte var publicerade. Penetration av stridsdelar i betong studerades därför med en kombination av experimentella metoder, empiriska penetrationsmodeller och FE-analyser för att öka förståelsen för problemställningen. De experimentella modellresultaten användes för att utvärdera både de empiriska penetrationsmodellerna och FE-analyserna avseende betongpenetration, med båda metodernas användande diskuterat i uppsatsen. Användandet av högpresterande betong ökade penetrationsmotståndet för betongmålen i jämförelse med standardbetongmålen. Det var även möjligt att förhindra kraterbildningen på fram- och baksidan av de kraftigt armerande standardbetongmålen, detta medförde även en reducerad penetration för projektilerna i målen. De existerande empiriska penetrationsmodellerna kunde inte förutsäga penetrationen av modellprojektilerna i betongmålen med godtagbara resultat. Istället vidareutvecklades en av dessa modeller för att bättre beskriva denna typ av penetrerande stridsdelar i skyddskonstruktioner av betong. Finita elementanalyserna av standardbetongmålen visade sig ge ett rimligt beteende för alla analyserade modeller, med de bästa resultaten erhållna för vinkelrätt anslag för de modellprojektilerna av de penetrerande stridsdelarna. / QC 20111116
58

Behavioral Analysis of Volvo Cars Instrument Panel During Airbag Deployment

Nazari, Amir, Nourozi, Behrouz January 2016 (has links)
Airbags are a passive safety technology, required to function with zero failure rate. Advances in Computer Aided Engineering have allowed vehicle manufacturers to predict material and system behavior in the event of a crash. The sudden and rapid nature of a vehicle frontal crash, together with strict requirements put on safety make this a sensitive task. This thesis focuses on the front passenger airbag deployment and the instrument panel’s response. Various airbag modelling techniques are studied and presented in this document. This work is part of a larger-scale attempt to model a generic-sled that is physically representative of a real vehicle. Various component tests are to be performed in the sled environment, as opposed to a real vehicle, to save costs. Various modules are added to the sled once their behavior is verified by testing and in simulations. Software are advanced enough to identify location and magnitude of stress concentrations that develop during crash. LS-DYNA is used for explicit finite element simulations of the instrument panel (IP) in question with different airbag models. Verification has been achieved by design of experiment (DOE); with tests conducted to capture both the movements of the airbag housing and IP movements in response. These movements are broken down in various phases, facilitating implementation in the sled environment. Simplifications are made both to the computer models as well as the physical testing environment. The effects of these simplifications are quantified and discussed. Theoretical background is provided where fit while assumptions are justified wherever made. DYNAmore recommendations regarding costeffective calculations as well as result verification are followed. The obtained results show that the FE models replicate the real event with acceptable precision. The findings in this work can, by minor tweaks, be implemented on other IP models in the Volvo Cars range, leading to cost-saving solutions. This thesis provides the necessary information for sled implementations as well as future improvement suggestions. / Krockkudde är en s.k. passiv säkerhetsteknik som krävs att fungera felfritt. Framsteg inom Computer Aided Engineering har tillåtit biltillverkare att förutsäga material och systembeteende i samband med krock. Den plötsliga karaktären av krock, tillsammans med höga säkerhetskrav, gör detta till en känslig uppgift. Denna avhandling fokuserar på passagerarsidans krockkudde och instrumentbrädans (IP) respons under uppblåsning. Olika metoder för modellering av krockkuddar har studerats och presenteras i detta dokument. Arbetet är en del av en större skala försök att modellera en generisk-släde som är fysiskt representativ av en riktig bil; där olika komponent-tester skall utföras för att minska kostnader. När olika modulers beteende verifieras läggs de till släden. Denna verifiering sker genom finita element (FE) simuleringar så väl som fysiska tester. FE mjukvara är idag tillräckligt avancerad för att identifiera samt visualisera spänningskoncentrationer som uppstår i en konstruktion vid krock. LS-DYNA används i detta arbete för explicita FE simuleringar av en Volvo XC90 IP, lastad med olika krockkudde-modeller. Modell verifiering har uppnåtts genom försöksplanering (DOE); med tester utförda för att fånga rörelser av IP så väl som krockkudde-behållaren. Dessa rörelser är sedan uppdelade i olika faser för enklare genomförande i släde miljön. Förenklingar och antaganden görs både till FE modeller och fysiska testmiljön. Effekter av dessa har kvantifierats och relevant teoretisk bakgrund har inkluderats. Dokumentet innehåller även diskussion kring val av mätutrustning samt förbättringsförslag för fortsatt arbete. DYNAmore rekommendationer gällande kostnadseffektiva beräkningar och verifiering av simulerings-resultat har följts. Under arbetet visade sig att FE modellerna kan återskapa händelsen med hög noggrannhet; dessa trotts svårigheter i modellering av plast material. Möjligtvis kan man, genom mindre modifieringar, relatera slutsatserna i detta arbete till olika IP modeller i företagets produktkatalog vilket förmodligen leder till ytterligare kostnadsbesparingar. Denna avhandling ger den information som behövs för genomföranden i den generiska miljön.
59

Development of a real-time transient analyser for the SKA

Botha, Antheun 04 1900 (has links)
Thesis (MEng)--Stellenbosch University, 2014. / ENGLISH ABSTRACT: The extension of the Karoo Array Telescope (KAT), MeerKAT, will be the most sensitive radio telescope in the southern hemisphere until it is superseded by the completion of the Square Kilometre Array (SKA). These instruments are to be constructed in the Karoo which is an area in South-Africa that is protected against Radio Frequency Interference (RFI) by the Astronomy Geographical Advantage (AGA) act. However, the telescope is also vulnerable to self-generated interference and specialised measurement systems are required to monitor RFI levels. The development of a ReAl Time Transient AnalYser (RATTY) is described and two Experimental Development Models (XDM) are compared. The first uses a mixing philosophy, and the second direct-sampling. The selection of these models was based on the evaluation of several analogue Front-End (FE) designs. A stripline-filter design process is presented along with the results obtained for custom filters developed for the FEs. Several analyses were compared to measurements performed with one of the devices and good agreement was shown between the system characteristics. Issues regarding the Spurious Free Dynamic Range (SFDR) of the FE designs were identified in the process and measurement-corrected simulations used to predict the achievable ranges. The outcome of the XDM comparison promotes the continued development of a direct-sampling strategy to fulfil the short-term goals of the project. A static calibration procedure is demonstrated for the mixing system and implemented to account for different FE configurations. An overview of the digital and software components of the RATTY system is given and Electromagnetic Compatibility (EMC) principles are applied during the construction of both systems. / AFRIKAANSE OPSOMMING: Die finale fase van die Karoo Reeks Teleskoop (KAT), MeerKAT, sal die sensitiefste radio teleskoop in die suidelike halfrond wees. Dit sal egter oortref word deur die vierkante kilometer reeks, wat die sensitiefste radio teleskoop ter wêreld sal word. Beide instrumente sal vatbaar wees vir radiofrekwensie steurings en sal opgerig word in ‘n wet-beskermde omgewing. Die teleskope is ook vatbaar vir radiofrekwensie steurings wat deur interne stelsels opgewek kan word. Dus word gespesialiseerde meetapparate benodig om die betrokke area en substelsels van die teleskope te monitor. Die ontwikkeling van ‘n meetinstrument vir die ontleding van kort-durasie tydseine (RATTY) word beskryf en twee eksperimentele ontwikkelings modelle word vergelyk. Hierdie modelle is gebaseer op die verfyning van voorafgaande ontwerpe vir die analoog substelsel van die instrument en hierdie proses word verduidelik. Die eerste model volg ‘n menger strategie waar die tweede model direkte-monstering implementeer. ‘n Dubbel-laag, mikrostrookfilter ontwerpsproses word beskryf en die gemete resultate vir die ontwikkelde filters word bespreek. Verskeie ontledings is aangewend en vergelyk met die gemete resultate van die stelsels. Hieruit word bevredigende ooreenkomste getref. Die beperkings van die modelle, weens interne distorsie, word geïdentifiseer in dié proses en verdere skattings word gemaak d.m.v. simulasies. Die eksperimentele modelle word vergelyk en die voorkeur van ‘n direkte-monsterings stelsel word gemotiveer. Die digitale en sagteware komponente word oorsigtelik behandel. Tydens die konstruksie van die modelle word die toepassing van elektromagnetiese verenigbaarheids beginsels verduidelik. Laastens word ‘n eenvoudige kalibrasie toegepas op die menger stelsel en ‘n toepassing daarvan word behandel.
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Extraction des hémicelluloses de pâtes papetières pour la production de pâte à dissoudre / Hemicellulose extraction of paper grade pulp for dissolving pulp production

Arnoul Jarriault, Benoît 17 December 2015 (has links)
Les pâtes à dissoudre, composées à 95% de cellulose, sont la matière première pour la production de fibres cellulosiques régénérées (viscose, Lyocell…) et de dérivés cellulosiques (ester, éther ou nitrate de cellulose). En tant qu’alternative aux matériaux issus de ressources pétrolières, ces produits connaissent actuellement un fort regain d’intérêt. Ainsi, la production de pâte à dissoudre devrait croître fortement au cours de la prochaine décennie. L’objectif de cette thèse est de proposer des procédés de conversion d’une pâte papetière de résineux en pâte à dissoudre. Pour cela les hémicelluloses présentes dans les pâtes kraft papetières doivent être extraites. Trois méthodes d’extraction d’hémicelluloses ont ainsi été étudiées : (1) une extraction alcaline à froid (CCE) dans des conditions non conventionnelles, (2) un procédé se divisant en deux étapes successives : un stade acide à haute température (150°C) suivie d’une extraction alcaline à chaud (AHCE) et (3) une hydrolyse enzymatique par trois enzymes commerciales (une xylanase, une mannanase, une cellulase). Les deux premières méthodes ont permis de produire des pâtes avec des caractéristiques proches des pâtes à dissoudre commerciales. Cependant, dans les trois voies d’extraction étudiées, l’extraction d’hémicelluloses n’a jamais atteint 100%. Des prétraitements des pâtes (raffinage, explosion à la vapeur, oxydation TEMPO) ont alors été testés pour améliorer l’extraction des hémicelluloses. De nouvelles séquences de purification basées sur la combinaison d’une étape de raffinage suivie d’une extraction alcaline à froid (CCE) peuvent être ainsi imaginées. La dernière partie de ces travaux de thèse s’est intéressée au gonflement des pâtes à dissoudre. Les travaux ont abouti à la création d’une nouvelle méthode simple et rapide de caractérisation du gonflement des fibres de pâte cellulosique. Cette méthode de mesure peut être, dans certaines conditions, considérée comme une mesure alternative de la réactivité des pâtes à dissoudre habituellement caractérisée par le test Fock. / Dissolving pulps, which are composed of 95% cellulose, are the raw materials for the production of regenerated cellulose fibres for textile application and for the production of cellulose derivatives. These products are alternatives to oil based materials. A growing demand in such products is expected in the next decades. Therefore, additional capacities in the production of wood dissolving pulp must be created. The purpose of this work is to develop hemicellulose removal processes with the aim to convert a softwood kraft paper pulp into a dissolving pulp. Three extraction methods were tested: (1) A cold caustic extraction process (CCE) performed under conventional and unconventional conditions; (2) A process consisting in an acid stage at high temperature (up to 150°C) followed by a hot caustic extraction (A-HCE); (3) An enzymatic hydrolysis using xylanase, mannanase, and cellulase. Conversion was quite successful with the two first processes. However, 100% of hemicellulose removal was never reached. In order to improve the hemicellulose extraction efficiency, several pre-treatments were tested (refining, steam explosion, TEMPO oxidation). The addition of a refining stage allows a reduction of the NaOH concentration during CCE extraction without affecting the hemicellulose extraction efficiency. The last part of this thesis work focus on the dissolving pulp swelling. A new and rapid test for the characterization of fibre swelling was developed. This method was used as an approach to the assessment of dissolving pulp reactivity in the viscose process in place of the Fock’s method.

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