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871	Méthodes de microscopie par holographie numérique interférentielle en couleurs avec un éclairage partiellement cohérent Dohet-Eraly, Jérôme 19 April 2017 (has links) La présente thèse traite de méthodes en microscopie holographique numérique (MHN) en couleurs, avec un éclairage de cohérence spatiale partielle. Le principal inconvénient de la microscopie optique classique est sa faible profondeur de champ, rendant difficile l’observation de phénomènes dynamiques dans des échantillons épais. Au contraire, la MHN offre une reconstruction en profondeur grâce à la propagation numérique de l’hologramme. La MHN interférométrique donne aussi le contraste quantitatif de la phase, utile pour analyser des objets transparents. Un éclairage à plusieurs longueurs d’onde dans une configuration appropriée permet la MHN en couleurs. L’imagerie en flux et en couleurs de particules en MHN est ici développée, avec une méthode pour la correction automatique de la balance des couleurs et des défauts permanents. Elle est appliquée pour l’analyse du plancton dans des échantillons d’eau de surface et fournit des images de haute qualité pour les intensité et phase optiques. En outre, la réduction du bruit obtenue en diminuant la cohérence spatiale de l’éclairage en MHN est également étudiée, avec deux modèles évaluant quantitativement ce phénomène en fonction de la cohérence spatiale de la lumière et de la distance entre la source de bruit et le plan d’enregistrement. De plus, la MHN différentielle est aussi abordée. Celle-ci fournit les phases différentielles, la phase étant calculée par intégration. Cependant, les défauts présents conduisent à des aberrations lors du calcul de la phase, qui affectent sa qualité et empêchent la reconstruction holographique. Un traitement spécifique est développé, permettant la reconstruction numérique en profondeur. Enfin, en MHN, un critère est essentiel pour déterminer automatiquement la distance de netteté de l’objet. Deux critères de netteté sont ici mis au point, fonctionnant indépendamment de la nature de l’objet observé (amplitude, phase ou mixte). L’un, monochromatique, est basé sur l’analyse de l’amplitude et sur un filtrage passe-haut ;l’autre, qui détecte rapidement le plan de netteté en MHN en couleurs, compare la phase dans le domaine de Fourier entre les couleurs. Les méthodes développées dans la thèse montrent le potentiel élevé de la MHN en couleurs avec un éclairage partiellement cohérent spatialement, suggérant un avenir prometteur pour cette technique. / The thesis deals with methods and developments in color digital holographic microscopy (DHM), with a partial spatial coherence illumination. The principal drawback of classical optical microscopy is its poor depth of field, which makes difficult the observation of dynamic phenomena in thick samples. On the contrary, DHM provides reconstruction in depth thanks to numeric propagation of the recorded hologram. Another feature of interferometric DHM is the quantitative phase contrast imaging, useful for analyzing transparent objects. Usual DHM is limited to monochromatic case, but multispectral illumination in an appropriate setup leads to color DHM. Color in-flow imaging of particles in DHM is developed in the thesis, with a method for the automatic correction of color balance and permanent defects. It is applied to analyze plankton microorganisms in untreated pond water samples, and provides high quality images, for both optical phase and intensity. Moreover, noise reduction obtained when decreasing the spatial coherence of the illumination in DHM is also investigated in the thesis, with the development of two models that quantitatively assess the noise reduction as a function of both the spatial coherence of the illumination, and the defocus distance of the noise source. Furthermore, differential DHM (DDHM) is also studied in the thesis. As DHM gives the optical phase, DDHM provides differential phases, from which phase is retrieved by integration. However, misalignments and defects give some aberrations, which affect phase quality and hinder refocusing. A specific hologram processing is developed, giving an accurate phase image and enabling holographic reconstruction in depth. Finally, in DHM, a criterion is essential to automatically achieve the refocusing distance of the object. Two refocusing criteria are developed in the thesis, both working independently of the nature of the observed object (amplitude, phase, or both mixed). The first one, monochromatic, is based on amplitude analysis and on a high-pass filtering process. The second one, which gives fast refocusing in multispectral DHM, compares the phase in the Fourier domain among wavelengths. Methods developed in the thesis show the high potential of color DHM with a partial spatial coherence illumination, suggesting a promising future for this technique. / Doctorat en Sciences de l'ingénieur et technologie / info:eu-repo/semantics/nonPublished Optique Sciences de l'ingénieur Sciences bio-médicales et agricoles Microscopie Holographie numérique Holographie en couleurs Interférométrie Optique de Fourier Traitement d’images Cohérence spatiale partielle Imagerie en flux Interférences différentielles Remise au net automatique Microscopy Digital holography Color holography Interferometric imaging Fourier optics Digital image processing Partial spatial coherence In-flow imaging Differential interferometry Automatic refocusing
872	Contribution to a Simulator of Arrays of Atomic Force Microscopes / Contribution à la modélisation et au contrôle d'une matrice d'AFM Hui, Hui 06 May 2013 (has links) Dans cette thèse, nous établissons un modèle à deux échelles à la fois pour desmatrices de cantilevers unidimensionnels et bidimensionnels en régime de fonctionnementélastodynamique avec des applications possibles aux réseaux de microscopesà force atomique (AFM). Son élaboration est basée sur une analyseasymptotique pour les structures minces élastiques, une approximation à deuxéchelles et une mise à l’échelle utilisée pour l’homogénéisation des milieux fortementhétérogènes. Nous complétons la théorie de l’approximation à deux échellespour les problèmes aux limites du quatrième ordre posés dans des domaines mincespériodiques connexes seulement dans certaines directions. Notre modèle reproduitla dynamique globale du support ainsi que les mouvements locaux des cantilevers.Pour simplifier la suite du travail, nous concentrons nos travaux à l’étude de matricesde leviers constituées de lignes découplées en régime dynamique. Comme lesupport des leviers est élastique, l’effet du couplage entre levier est pris en compte.La vérification du modèle est soigneusement réalisée. Nous montrons que chaquemode propre peut être décomposé en produits d’un mode de base avec un modede levier. Nous présentons une méthode de discrétisation du modèle et effectuonssa vérification numérique en la comparant avec des résultats de simulation paréléments finis du problème d’élasticité tridimensionnel. Par ailleurs, nous avonsélaboré de nouveaux outils d’aide à la conception de réseaux d’AFM. Une boîte àoutils d’optimisation robuste est interfacée avec le modèle permettant d’optimiserun design avant micro-Fabrication. Un algorithme d’estimation de l’état statiquecombinant la mesure de déplacements mécaniques par interférométrie et le modèlea été introduit. Nous avons également synthétisé un régulateur quadratiquelinéaire (LQR) pour un réseau de cantilevers en mode dynamique comprenant actionneurset capteurs régulièrement espacées. Dans le but de mettre en oeuvre lecontrôle en temps réel, nous proposons une approximation semi-Décentralisée quipeut être réalisé par un circuit électronique distribué analogique. Plus précisément,notre processeur analogique peut être réalisé par un réseau périodique derésistances (PNR). La méthode d’approximation de commande est basée sur deuxconcepts généraux, à savoir sur un calcul fonctionnel (c’est-À-Dire des fonctionsd’opérateurs) et sur la formule de représentation d’une fonction d’opérateur deDunford-Schwartz. Cette méthode d’approximation est étendue pour la résolutiond’un problème de filtrage optimal robuste de type H∞ de la dynamique d’un réseaude leviers couplés avec sources aléatoires de bruit. / In this dissertation, we establish a two-Scale model both for one-Dimensionaland two-Dimensional Cantilever Arrays in elastodynamic operating regime withpossible applications to Atomic Force Microscope (AFM) Arrays. Its derivationis based on an asymptotic analysis for thin elastic structures, a two-Scale approximationand a scaling used for strongly heterogeneous media homogenization. Wecomplete the theory of two-Scale approximation for fourth order boundary valueproblems posed in thin periodic domains connected in some directions only. Ourmodel reproduces the global dynamics as well as each of the cantilever motion. Forthe sake of simplicity, we present a simplified model of mechanical behavior of largecantilever arrays with decoupled rows in the dynamic operating regime. Since thesupporting bases are assumed to be elastic, cross-Talk effect between cantileversis taken into account. The verification of the model is carefully conducted. Weexplain not only how each eigenmode is decomposed into products of a base modewith a cantilever mode but also the method used for its discretization, and reportresults of its numerical validation with full three-Dimensional Finite Element simulations.We show new tools developed for Arrays of Microsystems and especiallyfor AFM array design. A robust optimization toolbox is interfaced to aid for designbefore the microfabrication process. A model based algorithm of static stateestimation using measurement of mechanical displacements by interferometry ispresented. We also synthesize a controller based on Linear Quadratic Regulator(LQR) methodology for a one-Dimensional cantilever array with regularly spacedactuators and sensors. With the purpose of implementing the control in real time,we propose a semi-Decentralized approximation that may be realized by an analogdistributed electronic circuit. More precisely, our analog processor is made by PeriodicNetwork of Resistances (PNR). The control approximation method is basedon two general concepts, namely on functions of operators and on the Dunford-Schwartz representation formula. This approximation method is extended to solvea robust H∞ filtering problem of the coupled cantilevers for time-Invariant systemwith random noise effects. Modelisation à deux echelles Matrice de leviers Homogénéisation Vérification de modèle Conceptionpar optimisation robuste Mesure d'interférométrie Contôle semi-décentralisé Calcul fonctionel Formule intégrale de Cauchy Cantilever arrays Two scale modeling Homogenization Modele verification Optimization design Interferometry measurements Semi decentralized control Functional calculus Cauchy integral formula 620.1
873	Brilliant radiation sources by laser-plasma accelerators and optical undulators Debus, Alexander January 2012 (has links) This thesis investigates the use of high-power lasers for synchrotron radiation sources with high brilliance, from the EUV to the hard X-ray spectral range. Hereby lasers accelerate electrons by laser-wakefield acceleration (LWFA), act as optical undulators, or both. Experimental evidence shows for the first time that LWFA electron bunches are shorter than the driving laser and have a length scale comparable to the plasma wavelength. Furthermore, a first proof of principle experiment demonstrates that LWFA electrons can be exploited to generate undulator radiation. Building upon these experimental findings, as well as extensive numerical simulations of Thomson scattering, the theoretical foundations of a novel interaction geometry for laser-matter interaction are developed. This new method is very general and when tailored towards relativistically moving targets not being limited by the focusability (Rayleigh length) of the laser, while it does not require a waveguide. In a theoretical investigation of Thomson scattering, the optical analogue of undulator radiation, the limits of Thomson sources in scaling towards higher peak brilliances are highlighted. This leads to a novel method for generating brilliant, highly tunable X-ray sources, which is highly energy efficient by circumventing the laser Rayleigh limit through a novel traveling-wave Thomson scattering (TWTS) geometry. This new method suggests increases in X-ray photon yields of 2-3 orders of magnitudes using existing lasers and a way towards efficient, optical undulators to drive a free-electron laser. The results presented here extend far beyond the scope of this work. The possibility to use lasers as particle accelerators, as well as optical undulators, leads to very compact and energy efficient synchrotron sources. The resulting monoenergetic radiation of high brilliance in a range from extreme ultraviolet (EUV) to hard X-ray radiation is of fundamental importance for basic research, medical applications, material and life sciences and is going to significantly contribute to a new generation of radiation sources and free-electron lasers (FELs). info:eu-repo/classification/ddc/539 ddc:539
874	Combination of Borehole Seismic and Downhole Logging to Investigate the Vicinity of the COSC‑1 Borehole in Western Scandinavia Krauß, Felix 05 July 2018 (has links) In dieser Arbeit werden bohrlochseismsiche Messungen sowohl mit Bohrlochmessungen als auch mit oberflächenseismischen Messungen ausgewertet und verglichen um das bohrlochnahe Umfeld der Forschungsbohrung COSC-1 (Collisional Orogeny in the Scandinavian Caledonides) zu beschreiben. Die bohrlochseismischen Daten zeigen deutlich hohe Reflektivität und seismische Anisotropie der erbohrten geologischen Einheit, der Seve-Decke. Diese Decke zeichnet sich durch einen häufigen Wechsel von mafischen und felsischen Gesteinen aus, welcher auch durch eine Clusteranalyse der Bohrlochmessungen deutlich wird. Die Ergebnisse der Clusteranalyse korrelieren gut mit den seismisch abgebildeten Untergrundstrukturen und den seismischen Geschwindigkeiten. Abschließend wurde die virtual source method als Beispiel der seismischen Interferometrie an einem Teildatensatz erfolgreich getestet. Mit dem Ansatz wurde eine künstliche Messgeometrie mit seismischen Quellen und Empfängern im Bohrloch erzeugt, welche eine gute Datenqualität aufzeigen. / In this thesis, the vicinity of the scientific borehole COSC-1 (Collisional Orogeny in the Scandinavian Caledonides) is investigated by the combination of a borehole seismic survey with downhole logging data and a surface seismic survey. The borehole seismic data show a significantly higher reflectivity and seismic anisotropy within the drilled geological unit, the Seve Nappe. This nappe is characterised by frequent changes of mafic and felsic lithologies that are also highlighted by a cluster analysis. The results of the cluster analysis correlate well with structures of the subsurface as imaged by the surface seismic survey and with seismic velocities. Additionally, the virtual source method as example for seismic interferometry is applied to a data subset. This approach created a virtual survey geometry with seismic sources and receivers within the borehole and a good data quality. info:eu-repo/classification/ddc/550 ddc:550
875	Konzeption und Umsetzung neuer Technologien zur biaxialen Winkelmessung und elektrooptischen Pseudostreckenmessung Fuhrland, Matthias 30 November 2007 (has links) Ein Ziel der Arbeit war die Entwicklung eines Verfahrens zur 3D-Positionierung auf Basis elektrooptischer Pseudostreckenmessung. Ein zweites Ziel war die Entwicklung eines Reflexgoniometers zur zweiachsigen Winkelmessung. Im Rahmen der Arbeit wurden die Grundlagen zur instrumentellen Umsetzung beider Verfahren erarbeitet, die Genauigkeitspotentiale ermittelt und mögliche Anwendungen für die einzelnen Schlüsseltechnologien und deren Kombination abgeleitet. In einer Prototyp-Entwicklung wurden Vorschläge für die wesentlichen Funktionselemente des räumlichen Weg- bzw. Winkelmesssystems gemacht. Hierzu gehören das kardanisch aufgehängte Etalon, die temperaturstabilisierte Laseroptik und die temperaturkalibrierte CCD der Winkelmesseinheit (Reflexgoniometer), die Systeme zur Erzeugung und Detektion ultrakurzer Laserpulse, eine elastische Optik, Möglichkeiten zur Formung des transversalen Strahlprofils, das TCSPC-System und die zur Auswertung und Kalibrierung notwendigen Algorithmen, wie z.B. die Autokollimation eines Lasers. (&quot;Veröffentlicht von der Deutschen Geodätischen Kommission Reihe C (Dissertationen) unter der Nummer C 614 (München 2008; ISBN 3 7696 5053 0; 2; 144 S.&quot;) / One goal of the thesis was the development of a method for three-dimensional positioning based on electro-optical measurement of pseudo ranges. Another goal was the development of a reflex goniometer for biaxial angle measurement. Within the scope of this thesis the basics for the instrumental realisation of both methods were developed, the accuracy potentials were determined and possible applications for the separate key technologies and their combination were deduced. In a prototype development proposals were made for the main functional elements of the spatial distance and angle measurement systems. These include the gimbal mounted etalon, the temperature stabilised laser optics and the temperature calibrated CCD of the angle measurement device (reflex goniometer), the systems for creation and detection of ultrashort laser pulses, an elastic optical device, possibilities of transversal beam shaping, the TCSPC system and the algorithms which are necessary for analysis and calibration, e.g. the autocollimation of a laser. info:eu-repo/classification/ddc/550 ddc:550
876	Heat Transfer, Fluid Dynamics, and Autoxidation Studies in the Jet Fuel Thermal Oxidation Tester (JFTOT) Sander, Zachary Hugo January 2012 (has links) No description available. Aerospace Engineering Chemical Engineering Chemistry Energy Engineering Fluid Dynamics Mechanical Engineering Petroleum Engineering JFTOT CFD heat transfer oxidation autoxidation deposition ellipsometry jet fuel thermal oxidation tester oxygen consumption FT fischer tropsh hrj jp-8 jet a-1 thermal stability fluid mechanics astm d3241 flir interferometry udri
877	EXPERIMENTAL STUDY OF LUBRICANT DROPLETS IN A ROTARY COMPRESSOR AND OPTICAL DIAGNOSTICS OF EVAPORATION PROCESS Puyuan Wu (13949580) 13 October 2022 (has links) <p> </p> <p>Part I studies the lubricant sprays and droplets in a rotary compressor. Air conditioning (AC) systems are now widely used in residential and commercial environments, while the compressor is the most important element in the AC system, and rotary compressors are often used in split AC appliances, whose number is estimated to reach 3.7 billion in 2050. In a rotary compressor, the lubricant oil atomizes into small droplets due to the differential pressure in and out of the cylinder. Part of the lubricant oil droplets carried by the refrigerant vapor will ultimately exhaust from the compressor through the discharge pipe. The ratio of the discharged oil volume to the total oil volume is characterized as the Oil Discharge Ratio (ODR). High ODR will reduce the reliability of the compressor and deteriorate the heat transfer of the condenser and the evaporator, resulting in decreased efficiency. Thus, controlling the ODR is a key issue for the design of the rotary compressor.</p> <p>In Part I, rotary compressors were modified to provide optical access into its internal space, i.e., the lower cavity (refers to the space between the cylinder and the motor), above the rotor/stator, and at the discharge tube level. The modified rotary compressors’ operation was supported by a test rig which provided a wide range of operating conditions, e.g., pressure and frequency. Thus, in-situ optical measurements, e.g., shadowgraph and holograph, can be performed to visualize the lubricant sprays and droplets in the rotary compressor. An image processing routine containing the Canny operator and Convolutional Neural-Network was developed to identify droplets from high-resolution shadowgraph images, while Particle Image Velocimetry (PIV) and Optical Flow Velocimetry (OFV) were applied to calculate the spray and droplet’s velocities with time-resolved shadowgraph images. Parallel Four-Step Phase Shifting Holograph (PFSPSH) located the droplets’ positions in a three-dimensional volume under the specific operating condition.</p> <p>Both primary and secondary atomization were observed in the rotary compressor, while primary atomization is the major source of droplet production. The droplet size distributions versus the frequency, vertical direction, radial direction, and pressure are obtained. It is observed that the droplet characteristic mean diameters increase with the frequency and pressure. They also become larger in the outer region above the rotor/stator and keep constant in the radial direction at the discharge tube level. The penetration velocity of the lubricant spray is calculated in the lower cavity. An outward shift of the jet core combined with an outward velocity component was observed. Additionally, horizontal swirling velocity above the rotor/stator and at the discharge tube level and the vertical recirculation velocity above the rotor/stator are characterized. The volume fraction of droplets was also characterized under the specific operating condition. The results provide detailed experimental data to set up the boundary conditions used in CFD. They also show that the droplets in the upper cavity are mostly from the discharge process of the cylinder in the lower cavity. The results support a droplet pathway model in the rotary compressor, which can guide the optimization of future rotary compressors.</p> <p>Evaporation is commonly seen in hydrology, agriculture, combustion, refrigeration, welding, etc. And it always accompanies heat and mass transfer at the liquid-gas interface and is affected by the substance’s properties, the environment’s pressure, temperature, convection, and so on. PFSPSH in Part I aims to retrieve the phase information for holograph reconstruction. Part II further explores the application of the PFSPSH technology in Part I to observe the evaporation process of acetone, where the phase disturbance caused by the vapor is used to reconstruct the vapor concentration in space. The method is called Parallel Four-Step Phase Shifting Interferometer (PFSPSI). The first case studies the evaporation process of the acetone contained in a liquid pool with uniform air flow in a low-speed wind tunnel. The mole fractions of the acetone vapor near the liquid-air interface with different air speeds are characterized. The second case studies the evaporation process of acetone droplets levitated by an ultrasound levitator. The mole fraction of the acetone vapor near the liquid-air interface is characterized by assuming an axisymmetric field and using the analytical solution of the inverse Abel transform. The asymmetric pattern of the acetone vapor field is observed, which is considered due to the drastic sound pressure change at the stand wave location produced by the ultrasound levitator. The mass transfer of the evaporation process by the vapor’s mole fraction is calculated and compared with the mass transfer calculated by the droplet size change. It is observed that the mass transfer by the vapor’s mole fraction is generally smaller than the mass transfer calculated by the droplet size change, which can be explained by the convection process induced by the acoustic streaming.</p> rotary compressor lubricant oil droplet size distributions droplet velocity distribution lubricant pathway phase shifting interferometry evaporation processes levitated droplets vapor mole fraction
878	LIQUID FUEL TRANSPORT PHENOMENA IN ROTATING DETONATION ENGINES Matthew Hoeper (19824417) 10 October 2024 (has links) <p dir="ltr">Interest in using detonation-based combustion cycles for use propulsion and power generation has gained considerable attention in the last 10 years or so. The rotating detonation engine (RDE), in particular, has garnered the most attention as a possible replacement for current generation combustion systems. RDEs are continuous flow devices that typically operate in a non-premixed fashion. Reactants are injected into an annular combustion chamber that is usually several millimeters wide. One or more detonation waves propagate azimuthally around the annulus, consuming the reactants. The products then expand out of the combustor where it can produce thrust or be passed into a turbine. The detonation wave front in RDEs travel at speeds between 1-3 km/s which poses additional complexity beyond traditional combustors. There are large gaps in the research community for RDEs that use one or more liquid based propellants. Questions regarding liquid breakup, atomization, breakup, recovery all remain unanswered both experimentally and numerically. This work seeks to understand these fundamental physical phenomena that drive these devices by applying advanced, high-speed laser and other optical diagnostics. </p><p dir="ltr"> A 120 mm nominal diameter rotating detonation combustor that operates on non-premixed hydrogen-air was modified to remove a hydrogen orifice and was replaced with a single liquid fuel injector. This simple, yet important, modification enables the study of a one-way coupling between a liquid fuel jet and a detonation wave at relevant spatio-temporal scales. Planar laser-induced fluorescence was performed at rates up to 1 MHz to quantify the quasi-steady jet dynamics and the recovery behavior of the single liquid jet. Long-duration PLIF imaging lasting 30-40 detonation periods at 300 kHz was also performed for statistical significance. A diesel liquid-in-crossflow injector was observed to breakup or be removed from the PLIF plane within only a few microseconds. After the detonation wave passes through the spray there is a significant dwell period can last between 20-40% of the detonation period before the new fuel is issued into the channel. The quasi-steady liquid jet trajectory was also compared to a jet-in-crossflow from literature and there is decent agreement in the jet near-field. </p><p dir="ltr"> The same hardware scheme with a different liquid fuel injector was tested in conjunction with an alternative imagine scheme. The first technique was able to capture details in the radial-axial plane but could not resolve any motion in the azimuthal direction. A volume-based illumination scheme was used for LIF to image a liquid fuel jet in the azimuthal-axial plane. For this experiment the location of the liquid fuel jet was moved into a different position and as a result experiences significantly different behavior than the jet in crossflow. The breakup and evaporation process takes place over a much longer period of time and there is no pause of liquid fuel injection. Similarly, LIF was performed at 300 kHz for 30 detonation cycles to enable sadistically quantification and phase averaging. Filtered OH* and CH* chemiluminescence imaging was also performed over the same field of view as the LIF imaging. Estimation of the velocity field was calculated using optical flow from the Jet-A LIF images. The velocity results agree well with the recovery analysis from the PLIF measurements.</p><p dir="ltr"> Using the same liquid fuel injection scheme, Jet-A droplet diameter and velocity was measured <i>in-situ</i> during a hot-fire experiment using phase Doppler interferometry (PDI). Although a point technique, PDI was used to measure thousands of droplets during a single test at multiple locations and with multiple conditions. As a means of comparison, cold flow experiments were performed with water in the exit plume. Droplet diameters were measured between 1-20 µs in both cases. PDI results were compared with the optical flow results and there is agreement in median velocities and some differences in the minimum and maximum velocity values. Possible sources of error in the diameter measurement are discussed as well.</p> Combustion Detonation rotating detonation engine (RDE) Laser Diagnostics Laser induced fluorescence (LIF) Phase Doppler Interferometry Optical flow.
879	Untersuchung photorefraktiver Materialien mittels optischer Ptychographie / Investigation of photorefractive materials using optical ptychography Bernert, Constantin 05 January 2017 (has links) (PDF) In der vorliegenden Arbeit wird die neuartige Mikroskopiemethode der Ptychographie für die Untersuchung photorefraktiver Materialien genutzt. Photorefraktive Materialien zeichnen sich durch die Generation lichtinduzierter Brechungsindexänderungen aus. Die Ptychographie bietet die Möglichkeit, neben der generierten Brechungsindexänderung im photorefraktiven Material auch die für die Generation genutzte Intensitätsverteilung des Laserstrahls zu bestimmen. Es wird sowohl die Abhängigkeit der Brechungsindexänderung von der Zeit der Generation als auch die Abhängigkeit von der Polarisation des Lasers gemessen. Durch den Vergleich der gewonnenen Werte mit einer numerischen Simulation des photorefraktiven Effekts werden mikroskopische Parameter der lichtinduzierten Ladungswanderung ermittelt. Zudem wird aus der polarisationsabhängigen ptychographischen Messung das Raumladungsfeld und die korrespondierende Ladungsdichte im Material berechnet. Die Ptychographie liefert damit einen neuen Zugang zum quantitativen Verständnis der Photorefraktivität. / In the present thesis the novel microscopy technique of ptychography is applied to the investigation of photorefractive materials. Photorefractive materials exhibit a change of the refractive index due to the exposure to light. The method of ptychography determines the refractive index change of the material together with the intensity distribution of the laser beam that was used for its generation. In one part of the experiment the time dependence of the refractive index change versus the generation time is investigated, in the other part of the experiment the dependence of the refractive index change to the polarisation of the laser beam is examined. Microscopic parameters of the photorefractive charge migration are determined with the utilisation of a numerical simulation of the photorefractive effect and its comparison with the measurement. Finally, the whole space charge field with the corresponding space charge density is calculated from a set of ptychographic measurements of one refractive index change with different polarisation directions of the laser. The presented experiments and their evaluation show, that the method of ptychography opens a new possibility for a quantitative understanding of the photorefractive effect. Photorefraktivität photorefraktiv Photorefraktiver Effekt photorefraktives photorefraktiver photorefraktive lichtinduziert lichtinduzierte lichtinduzierter lichtinduziertes Lithiumniobat LiNbO3 LiNbO3:Fe linbo3 linbo3:fe Ladungstransport Brechungsindexänderung Brechungsindexänderungen Raumladungsfeld elektrooptischer Effekt Pockels Effekt photovoltaischer Effekt photovoltaische Stromdichte photovoltaische photovoltaischer Photovoltaik photovoltaissches Ptychographie ptychographisch ptychographische ptychographisches Interferometrie interferometrisch interferometrische interferometrische Untersuchung interferometrisches Holographie holographisches holographische holographische Untersuchung digitale Holographie photorefractive effect photorefractive photo refractive light-induced lightinduced light induced Lithium niobate Lithiumniobate LiNbO3 LiNbO3:Fe linbo3 linbo3:fe charge transport chargetransport refractive index change refractive index changes space charge field electrooptic effect electrooptic Pockels effect photovoltaic effect photovoltaic current photovoltaic ptychography ptychographic interferometry interferometric holography holographic digital holography ddc:530 rvk:VG 8600 Photorefraktivität Photorefraktiver Effekt Lithiumniobat Ladungstransport Brechungsindexänderung elektrooptischer Effekt Pockels Effekt photovoltaischer Effekt photovoltaische Stromdichte Photovoltaik Ptychographie Interferometrie Holographie digitale Holographie Photorefractive Effect Lithium niobate charge transport charge migration refractive index change electrooptic effect Pockels effect photovoltaic effect photovoltaic current ptychography interferometry holography digital holography
880	Untersuchung photorefraktiver Materialien mittels optischer Ptychographie Bernert, Constantin 04 October 2016 (has links) In der vorliegenden Arbeit wird die neuartige Mikroskopiemethode der Ptychographie für die Untersuchung photorefraktiver Materialien genutzt. Photorefraktive Materialien zeichnen sich durch die Generation lichtinduzierter Brechungsindexänderungen aus. Die Ptychographie bietet die Möglichkeit, neben der generierten Brechungsindexänderung im photorefraktiven Material auch die für die Generation genutzte Intensitätsverteilung des Laserstrahls zu bestimmen. Es wird sowohl die Abhängigkeit der Brechungsindexänderung von der Zeit der Generation als auch die Abhängigkeit von der Polarisation des Lasers gemessen. Durch den Vergleich der gewonnenen Werte mit einer numerischen Simulation des photorefraktiven Effekts werden mikroskopische Parameter der lichtinduzierten Ladungswanderung ermittelt. Zudem wird aus der polarisationsabhängigen ptychographischen Messung das Raumladungsfeld und die korrespondierende Ladungsdichte im Material berechnet. Die Ptychographie liefert damit einen neuen Zugang zum quantitativen Verständnis der Photorefraktivität.:1 Einleitung 2 Theoretische Vorbetrachtungen 2.1 Ptychographie 2.1.1 Messung 2.1.2 Modell und Rekonstruktion 2.1.3 Ortsauflösung 2.2 Photorefraktiver Efekt 2.2.1 Lithiumniobat - Musterbeispiel für die Photorefraktivität 2.2.2 Ein-Zentrum-Modell 2.2.3 Brechungsindexänderung 2.2.4 Hohe Intensitäten 2.3 Raumladungsfeld 2.3.1 Ableitung des Feldes aus den Messgrößen 2.3.2 Raumladungsverteilung 2.3.3 Oberflächendeformation 2.3.4 Dynamik der Ladungen und des Feldes 3 Messungen 3.1 Proben 3.1.1 Ptychographische Teststruktur 3.1.2 LiNbO3:Fe 3.2 Versuchsanordnung 3.2.1 Experimenteller Aufbau 3.2.2 Grenze der Ortsauflösung 3.2.3 Charakterisierung des Laserstrahls 3.2.4 Experimentelle Überprüfung der Näherungen 3.3 Dynamik der Brechungsindexänderung 3.4 Polarisationsabhängigkeit der Brechungsindexänderung 4 Auswertung 4.1 Dynamik des Raumladungsfeldes und der Ladungen 4.1.1 Simulation 4.1.2 Vergleich zwischen Messung und Simulation 4.1.3 Dynamik der Ladungsverteilung 4.1.4 Fazit 4.2 Berechnung des Raumladungsfeldes 4.2.1 Raumladungsfeld und Ladungsverteilung 4.2.2 Simulation 4.2.3 Asymmetrie der Ladungsverteilung 4.2.4 Fazit 5 Zusammenfassung Appendizes A Physikalische Konstanten B Tensoren für LiNbO3 C Ungenäherte Herleitung der Brechungsindexänderung D Implementierung eines iterativen Verfahrens zur Bestimmung der Dynamik des Ein-Zentrum-Modells E Quelltext der Implementierung des iterativen Verfahrens Literaturverzeichnis / In the present thesis the novel microscopy technique of ptychography is applied to the investigation of photorefractive materials. Photorefractive materials exhibit a change of the refractive index due to the exposure to light. The method of ptychography determines the refractive index change of the material together with the intensity distribution of the laser beam that was used for its generation. In one part of the experiment the time dependence of the refractive index change versus the generation time is investigated, in the other part of the experiment the dependence of the refractive index change to the polarisation of the laser beam is examined. Microscopic parameters of the photorefractive charge migration are determined with the utilisation of a numerical simulation of the photorefractive effect and its comparison with the measurement. Finally, the whole space charge field with the corresponding space charge density is calculated from a set of ptychographic measurements of one refractive index change with different polarisation directions of the laser. The presented experiments and their evaluation show, that the method of ptychography opens a new possibility for a quantitative understanding of the photorefractive effect.:1 Einleitung 2 Theoretische Vorbetrachtungen 2.1 Ptychographie 2.1.1 Messung 2.1.2 Modell und Rekonstruktion 2.1.3 Ortsauflösung 2.2 Photorefraktiver Efekt 2.2.1 Lithiumniobat - Musterbeispiel für die Photorefraktivität 2.2.2 Ein-Zentrum-Modell 2.2.3 Brechungsindexänderung 2.2.4 Hohe Intensitäten 2.3 Raumladungsfeld 2.3.1 Ableitung des Feldes aus den Messgrößen 2.3.2 Raumladungsverteilung 2.3.3 Oberflächendeformation 2.3.4 Dynamik der Ladungen und des Feldes 3 Messungen 3.1 Proben 3.1.1 Ptychographische Teststruktur 3.1.2 LiNbO3:Fe 3.2 Versuchsanordnung 3.2.1 Experimenteller Aufbau 3.2.2 Grenze der Ortsauflösung 3.2.3 Charakterisierung des Laserstrahls 3.2.4 Experimentelle Überprüfung der Näherungen 3.3 Dynamik der Brechungsindexänderung 3.4 Polarisationsabhängigkeit der Brechungsindexänderung 4 Auswertung 4.1 Dynamik des Raumladungsfeldes und der Ladungen 4.1.1 Simulation 4.1.2 Vergleich zwischen Messung und Simulation 4.1.3 Dynamik der Ladungsverteilung 4.1.4 Fazit 4.2 Berechnung des Raumladungsfeldes 4.2.1 Raumladungsfeld und Ladungsverteilung 4.2.2 Simulation 4.2.3 Asymmetrie der Ladungsverteilung 4.2.4 Fazit 5 Zusammenfassung Appendizes A Physikalische Konstanten B Tensoren für LiNbO3 C Ungenäherte Herleitung der Brechungsindexänderung D Implementierung eines iterativen Verfahrens zur Bestimmung der Dynamik des Ein-Zentrum-Modells E Quelltext der Implementierung des iterativen Verfahrens Literaturverzeichnis info:eu-repo/classification/ddc/530 ddc:530

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