Made available in DSpace on 2014-12-17T14:07:05Z (GMT). No. of bitstreams: 1 YaraFG_DISSERT.pdf: 4146827 bytes, checksum: 3586f66a1b391a184d1b6034e91b85c0 (MD5) Previous issue date: 2012-12-20 / In the ceramics industry are becoming more predominantly inorganic nature pigments. Studies in this area allow you to develop pigments with more advanced properties and qualities to be used in the industrial context. Studies on synthesis and characterization of cobalt aluminate has been widely researched, cobalt aluminate behavior at different temperatures of calcinations, highlighting especially the temperatures of 700, 800 and 900? C that served as a basis in the development of this study, using the method of polymerization of complex (CPM), economic, and this method applied in ceramic pigment synthesis. The procedure was developed from a fractional factorial design 2 (5-2) in order to optimize the process of realization of the cobalt aluminate (CoAl2O4), having as response surfaces the batch analysis data of Uv-vis spectroscopy conducted from the statistic software 7.0, for this were chosen five factors as input variables: citric acid (stoichiometric manner), puff or pyrolysis time (h), temperature (? C), and calcinations (? C/min), at levels determined for this study. By applying statistics in the process of obtaining the CoAl2O4 is possible the study of these factors and which may have greater influence in getting the synthesis. The pigments characterized TG/DSC analyses, and x-ray diffraction (XRD) and scanning electron microscope (SEM/EDS) in order to establish the structural and morphological aspects of pigment CoAl2O4, among the factors studied it were found to statically with increasing calcinations temperature 700?< 800 <900 ?C, the bands of Uv-vis decrease with increasing intensity of absorbance and that with increasing time of puff or pyrolysis (h) there is an increase in bands of Uv-vis proportionally, the generated model set for the conditions proposed in this study because the coefficient of determination can explain about 99.9% of the variance (R?), response surfaces generated were satisfactory, so it s possible applicability in the ceramics industry of pigments / Na ind?stria cer?mica utilizam-se cada vez mais pigmentos de natureza predominantemente inorg?nica. Os estudos nessa ?rea permitem desenvolver pigmentos com qualidades e propriedades mais avan?adas para serem empregados em ?mbito industrial. Estudos de s?ntese e caracteriza??o do aluminato de cobalto t?m sido amplamente pesquisados, o comportamento do aluminato de cobalto em diferentes temperaturas de calcina??es, destacando principalmente as temperaturas de 700, 800 e 900?C utilizando o m?todo de polimeriza??o de complexos (MPC), m?todo este, econ?mico e aplicado em s?ntese de pigmentos cer?micos. O procedimento foi desenvolvido a partir de um planejamento fatorial fracionado 2(5-2) com o objetivo de otimizar o processo de realiza??o do aluminato de cobalto (CoAl2O4), tendo como superf?cies de respostas os dados da an?lise de espectroscopia do Uv-vis realizados a partir do software statistic 7.0, para isso, foram escolhidos cinco fatores como vari?veis de entrada: concentra??es de ?cido c?trico (de maneira estequiom?trica), tempo de puff ou pir?lise (h), temperatura (?C), tempo e taxas de calcina??es(?C/min), em patamares determinados para este estudo. Atrav?s da aplica??o estat?stica no processo de obten??o do CoAl2O4 foi poss?vel estudar entre estes fatores quais possam ter maior influ?ncia na obten??o da s?ntese. Os p?s-precursores foram caracterizados pelas an?lises termogravim?tricas TG/DSC, e os p?s-calcinados (pigmentantes) foram analisados pela difra??o de raios- x (DRX) e microscopia eletr?nica de varredura com energia dispersiva (MEV/EDS) a fim de comprovar os aspectos estruturais e morfol?gicos do CoAl2O4, entre os fatores estudados estaticamente verificou-se que com o aumento da temperatura de calcina??o 700<800<900?C, as bandas do Uv-vis diminuem com o aumento da intensidade da absorb?ncia e que com o aumento do tempo de puff ou pir?lise (h) h? um aumento das bandas do Uv-vis proporcionalmente, o modelo gerado ajustou-se para as condi??es propostas neste estudo, pois o coeficiente de determina??o consegue explicar cerca de 99,9%, da vari?ncia (R?), as superf?cies de respostas geradas foram satisfat?rias, sendo assim sua poss?vel aplicabilidade na ind?stria cer?mica de pigmentos

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior - CAPES / Monitoring of process control systems is extremely important for industries to ensure the quality of the product and the safety of the process. Predictive controllers, also known by MPC (Model Predictive Control), usually has a well performance initially. However, after a period, many factors contribute to the deterioration of its performance. This highlights the importance of monitoring the MPC control systems. In this work, tools based on multivariate statistical methods are discussed and applied to the problem of monitoring and Performance Assessment of predictive controllers. The methods presented here are: PCA (Principal Component Analysis) and ICA (Independent Component Analysis). Both are techniques that use data collected directly from the process. The first is widely used in Performance Assessment of predictive controllers. The second is a more recent technique that has arisen, mainly in order to be used in fault detection systems. The analyzes are made when applied in simulated processes characteristic of the petrochemical industry operating under MPC control. / O monitoramento de sistemas de controle de processos é extremamente importante no que diz respeito às indústrias, para garantir a qualidade do que é produzido e a segurança do processo. Os controladores preditivos, também conhecidos pela sigla em inglês MPC (Model Predictive Control), costumam ter um bom desempenho inicialmente. Entretanto, após um certo período, muitos fatores contribuem para a deterioração de seu desempenho. Isto evidencia a importância do monitoramento dos sistemas de controle MPC. Neste trabalho aborda-se ferramentas, baseada em métodos estatísticos multivariados, aplicados ao problema de monitoramento e avaliação de desempenho de controladores preditivos. Os métodos aqui apresentados são: o PCA (Análise por componentes principais) e o ICA (Análise por componentes independentes). Ambas são técnicas que utilizam dados coletados diretamente do processo. O primeiro é largamente utilizado na avaliação de desempenho de controladores preditivos. Já o segundo, é uma técnica mais recente que surgiu, principalmente, com o intuito de ser utilizado em sistemas de detecção de falhas. As análises são feitas quando aplicadas em processos simulados característicos da indústria petroquímica operando sob controle MPC.

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior - CAPES / Monitoring of process control systems is extremely important for industries to ensure the quality of the product and the safety of the process. Predictive controllers, also known by MPC (Model Predictive Control), usually has a well performance initially. However, after a period, many factors contribute to the deterioration of its performance. This highlights the importance of monitoring the MPC control systems. In this work, tools based on multivariate statistical methods are discussed and applied to the problem of monitoring and Performance Assessment of predictive controllers. The methods presented here are: PCA (Principal Component Analysis) and ICA (Independent Component Analysis). Both are techniques that use data collected directly from the process. The first is widely used in Performance Assessment of predictive controllers. The second is a more recent technique that has arisen, mainly in order to be used in fault detection systems. The analyzes are made when applied in simulated processes characteristic of the petrochemical industry operating under MPC control. / O monitoramento de sistemas de controle de processos é extremamente importante no que diz respeito às indústrias, para garantir a qualidade do que é produzido e a segurança do processo. Os controladores preditivos, também conhecidos pela sigla em inglês MPC (Model Predictive Control), costumam ter um bom desempenho inicialmente. Entretanto, após um certo período, muitos fatores contribuem para a deterioração de seu desempenho. Isto evidencia a importância do monitoramento dos sistemas de controle MPC. Neste trabalho aborda-se ferramentas, baseada em métodos estatísticos multivariados, aplicados ao problema de monitoramento e avaliação de desempenho de controladores preditivos. Os métodos aqui apresentados são: o PCA (Análise por componentes principais) e o ICA (Análise por componentes independentes). Ambas são técnicas que utilizam dados coletados diretamente do processo. O primeiro é largamente utilizado na avaliação de desempenho de controladores preditivos. Já o segundo, é uma técnica mais recente que surgiu, principalmente, com o intuito de ser utilizado em sistemas de detecção de falhas. As análises são feitas quando aplicadas em processos simulados característicos da indústria petroquímica operando sob controle MPC.

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior - CAPES / The data reconciliation in process control is extremely important regarding the industries because from this it is possible to obtain a greater efficiency in the performance in industrial process control meshes aiming at a lower cost and a higher quality of the product. In this work we approach data estimation techniques for the implementation of an online dynamic data reconciliation system in order to reduce the noise and the measurement uncertainties that are submitted in the process variables. The techniques used here are: the Kalman Filter, the Preditor-Corrector DDR Algorithm, the Moving Horizon Estimator (MHE) and the Constrained Extended Kalman Filter (CEKF). The analysis is performed by applying the dynamic data reconciliation system in a simulated process, characteristic of the chemical industry, operating under MPC (Model Predictive Control). The performance of the MPC controller is also enhanced by the use of the reconciled data in the feedback control loop. / A reconciliação de dados em controle de processos é extremamente importante no que diz respeito às indústrias, pois a partir dessa é possível obter uma maior eficiência no desempenho em malhas de controle de processos industriais visando à minimização dos custos e maximizando a qualidade do produto. Neste trabalho abordam-se técnicas de estimação de dados para a implementação de um sistema de reconciliação dinâmica de dados on-line a fim de reduzir os ruídos e as incertezas de medições a que estão submetidas às variáveis do processo. As técnicas aqui empregadas são: o Filtro de Kalman, o Algoritmo DDR Preditor-Corretor, o Estimador de Horizonte Móvel (MHE) e o Filtro de Kalman Estendido com Restrições (CEKF). As análises são efetuadas aplicando o sistema de reconciliação dinâmica de dados em um processo simulado, característico da indústria química, operando sob controle preditivo (MPC). Também é efetuado o aprimoramento no desempenho do controlador MPC utilizando os dados reconciliados na malha de realimentação do controlador.

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior - CAPES / Model predictive control (MPC) strategies have become the standard for advanced control applications in the process industry. Significant benefits are generated from the MPC's capacity to ensure that the plant operates within its constraints more profitably. However, like any controller, after some time under operation, MPCs rarely function as when they were initially designed. A large percentage of performance degradation of MPC is associated with the deterioration of model that controller uses to predict process outputs and calculate inputs. The objective of the present work is implementation of mathematical methods that can be used to detect model-plant mismatch in linear and nonlinear MPC systems. In this work, techniques based on cross correlation, partial correlation and mutual information are implemented and tested by numerical simulation in case studies characteristic of the petrochemical industry, represented by linear and nonlinear models, operating under MPC control. The results obtained through the applying the techniques are analyzed and compared as to their efficiency is not intended to offer their potential for real industrial applications. / Estratégias de controle preditivo (MPC) têm-se tornado o padrão para aplicações de controle avançado na indústria de processos. Os benefícios significativos são gerados a partir da habilidade do controlador MPC de assegurar que a planta opere dentro das restrições de forma mais lucrativa. Porém, como todo controlador, depois de algum tempo em operação, os MPCs raramente funcionam como quando foram inicialmente projetados. Uma grande porcentagem da degradação do desempenho dos controladores MPC está associada à deterioração do modelo que o controlador usa para fazer a predição das saídas do processo e calcular as entradas. O objetivo do presente trabalho é a implementação de métodos matemáticos que possam ser utilizados para a detecção de erros planta-modelo em sistemas de controle MPC lineares e não lineares. Neste trabalho, técnicas baseadas em correlação cruzada, correlação parcial e informação mútua são implementadas e testadas por simulação numérica em estudos de caso característicos da indústria petroquímica, representados por modelos lineares e não lineares, operando sob controle MPC. Os resultados obtidos através da aplicação das técnicas são analisados e comparados quanto à sua eficiência no objetivo proposto avaliando seu potencial para aplicações industriais reais.

The interest in autonomous vehicles has never been higher and there are several components that need to function for a vehicle to be fully autonomous; one of which is the ability to perform a parking at the end of a mission. The objective of this thesis work is to develop and implement an automatic parking system (APS) for a heavy-duty vehicle (HDV). A delimitation in this thesis work is that the parking lot has a known structure and the HDV is a truck without any trailer and access to more computational power and sensors than today's commercial trucks. An automatic system for searching the parking lot has been developed which updates an occupancy grid map (OGM) based on measurements from GPS and LIDAR sensors mounted on the truck. Based on the OGM and the known structure of the parking lot, the state of the parking spots is determined and a path can be computed between the current and desired position. Based on a kinematic model of the HDV, a gain-scheduled linear quadratic (LQ) controller with feedforward action is developed. The controller's objective is to stabilize the lateral error dynamics of the system around a precomputed path. The LQ controller explicitly takes into account that there exist an input delay in the system. Due to minor complications with the precomputed path the LQ controller causes the steering wheel turn too rapidly which makes the backup driver nervous. To limit these rapid changes of the steering wheel a controller based on model predictive control (MPC) is developed with the goal of making the steering wheel behave more human-like. A constraint for maximum allowed changes of the controller output is added to the MPC formulation as well as physical restrictions and the resulting MPC controller is smoother and more human-like, but due to computational limitations the controller turns out less effective than desired. Development and testing of the two controllers are evaluated in three different environments of varying complexity; the simplest simulation environment contains a basic vehicle model and serves as a proof of concept environment, the second simulation environment uses a more realistic vehicle model and finally the controllers are evaluated on a full-scale HDV. Finally, system tests of the APS are performed and the HDV successfully parks with the LQ controller as well as the MPC controller. The concept of a self-parking HDV has been demonstrated even though more tuning and development needs to be done before the proposed APS can be used in a commercial HDV.

L'objectif principal de ce travail a été d'apporter une nouvelle contribution quant à l'approche de contrôle optimal pendant la phase d'identification. Il s'agissait de trouver la commande à appliquer pendant l'expérience qui permet d'optimiser un critère qui est fonction des sensibilités des sorties par rapport aux paramètres du modèle à identifier. Cette approche couplant contrôleur prédictif sous contraintes et estimateur a résolu en ligne le problème d'identification à chaque instant en utilisant l'observateur. En ce sens, c'est une approche permettant d'automatiser et d'optimiser le design d'expérience, tout en réalisant conjointement l'identification d'un paramètre du modèle spécifié. L'aspect temps réel a été pris en compte dans la formulation de la solution apportée. Dans ce contexte, nous avons introduit deux stratégies de commande pour l'identification optimale. La première était basée sur un modèle de prédiction non linéaire et la seconde sur un modèle linéaire temps variant. Si le temps devient un paramètre critique pour l'implémentation de l'approche, cette dernière vise à réduire le temps alloué à l'optimisation. L'approche d'identification optimale en ligne a été appliquée à deux problèmes concrets du Génie des Procédés (réaction de saponification et cuisson de peintures). Ces exemples ont permis de vérifier en simulation, l'efficacité et la faisabilité de cette approche. / The main aim of this work is to give a new approach of optimal control during the phase of identification. The question is how to tune the control action to be applied during the experiment optimize a criterion which is function of the sensitivities of the mesure with respect to the parameters of the model to be identified. This approach coupling constrained predictive controller and estimator solves on line the problem of identification by using the observer. In that sense, it is an approach allowing an optimal and automatic design of experiment, while performing at the same time the identification of one parameter of the specified model. The real time aspect was taken into account in the formulation of the solution. In this context, we introduced two strategies for optimal identification : the first one is based on a nonlinear model of prediction and the second one is based on a linear time varying model that may be used if the real time aspect becomes a critical parameter for the implementation of the approach. This approach of on line optimal identification was applied on two concrete problems in Chemical Engineering. These examples show the performance and the feasibility of this approach.

This dissertation presents a pumping system operation efficiency improvement solution that includes optimal selection and control of the water pump. This solution is formulated based on the performance, operation, equipment and technology (POET) framework. The focus is on the minimization of the operational energy cost. This efficiency improvement solution is divided into three stages in accordance with the operation category of the POET framework. The first stage is to select the optimal pump capacity by considering both energy efficiency and load shifting requirements. The second stage is to develop a flexible pump controlling strategy that combines and balances the contributions from energy efficiency and load shifting. The last stage is to improve the robustness of the control system using the closed-loop model predictive control approach. An optimal pump capacity selection model is formulated. In this model, additional capacity requirements for load shifting are considered along with the traditional energy efficiency requirements. By balancing the contributions from load shifting and energy efficiency, the operational energy cost can be reduced by up to 37%. An optimal pump control is formulated. The objective of this control model is to balance the energy efficiency and load shifting contributions during the operation and minimize the operational energy cost. This control model is tested under different operational conditions and it is compared to other existing control strategies. The simulation and comparison results show that the proposed control strategy achieves the lowest operational energy cost in comparison to other strategies. This optimal pump control model is further modified into the closed-loop model predictive control format to increase the robustness of the control system under operation uncertainties. A mixed integer particle swarm optimization algorithms is employed to solve the optimization problems in this research. AFRIKAANS : Hierdie verhandeling bied ’n verbeterde oplossing vir die operasionele doeltreffendheid van pompstelsels wat die optimale keuse en beheer van die waterpomp insluit. Hierdie oplossing is geformuleer op ’n raamwerk wat werkverrigting, bedryf, toerusting en tegnologie in ag neem. Die oplossing fokus op die vermindering van bedryfsenergie koste. Hierdie oplossing is onderverdeel in drie fases soos bepaal deur die bedryfskategorie gegrond op die bogenoemde raamwerk: Die eerste fase is die keuse van die optimale pompkapasiteit deur beide energiedoeltreffendheid en lasverskuiwing in ag te neem. Die tweede fase is om ’n buigbare pompbeheer strategie te ontwikkel wat ’n goeie balans handhaaf tussen die onderskeie bydraes van energiedoeltreffendheid en lasverskuiwing. Die derde fase is om die stabiliteit van die beheerstelsel te verbeter deur gebruik te maak van ’n geslote-lus beheermodel met voorspellende beheer (Predictive Control). ’n Model vir die keuse van optimale pompkapasiteit is geformuleer. In hierdie model word vereistes vir addisionele pompkapasiteit vir lasverskuiwing sowel as vereistes in terme tradisionele energiedoeltreffendheid in ag geneem. Deur die regte verhouding tussen die onderskeie bydraes van energiedoeltreffendheid en lasverskuiwing te vind kan ’n besparing van tot 37% op die energiekoste verkry word. Optimale pompbeheer is geformuleer. Die doel van die beheermodel is om die bydraes van energiedoeltreffendheid en lasverskuiwing te balanseer en om die bedryfsenergie koste te minimiseer. Hierdie beheermodel is getoets onder verskillende bedryfstoestande en dit is vergelyk met ander bestaande beheerstrategiee. Die simulasie en vergelyking van resultate toon dat die voorgestelde beheerstrategie die laagste bedryfsenergie koste behaal in vergelyking met ander strategiee. Hierdie optimale pomp beheermodel is verder aangepas in ’n geslote beheermodel met voorspellende beheerformaat om die stabiliteit van die beheerstelsel te verbeter onder onsekere bedryfstoestande. ’n Gemende heelgetal partikel swerm optimisasie (Mixed interger particle swarm optimization) algoritme is gebruik om die optimiseringsprobleme op te los tydens hierdie navorsingsoefening. / Dissertation (MEng)--University of Pretoria, 2011. / Electrical, Electronic and Computer Engineering / Unrestricted

This thesis deals with model predictive control principally Based Predictive Control (MPC). The first part describes the principle of predictive control, cost function, the choice of a constraints in regulation and the choice of weights. In the next section is an analysis system: a system with non-minimal phase (control water turbine), oscillating systems (trolley frame control) and system with a time-delay . In all of these systems is performed classical feedback control using PID control and concurrently regulation with the MPC. MPC is selected as the solution fy Mathworks Model Predictive Control Toolbox and Simulink. The results are then analyzed using the criteria of quality control.

In underwater tracking and surveillance, the active towed array sonar presents a way of discovering and tracking adversarial submerged targets that try to stay hidden. The configuration consist of listening and emitting hydrophones towed behind a ship. Moreover, it has inherent limitations, and the characteristics of sound in the ocean are complex. By varying the pulse form emitted and the trajectory of the ship the measurement accuracy may be improved. This type of optimization constitutes a sensor management problem. In this thesis, a model of the tracking scenario has been constructed derived from Cramér-Rao bound analyses. A model predictive control approach together with information measures have been used to optimize a filter's estimated state of the target. For the simulations, the MATLAB environment has been used. Different combinations of decision horizons, information measures and variations of the Kalman filter have been studied. It has been found that the accuracy of the Extended Kalman filter is too low to give consistent results given the studied information measures. However, the Unscented Kalman filter is sufficient for this purpose.