Rammed earth is a monolithic construction formed by compacting processed soil in progressive layers. Rammed earth is used for the construction of load bearing walls, floors, sub base material in roadways, airport runways, taxiways, aprons, foundations and earthen bunds. Soil, sand, cement and water are the ingredients used for the preparation of cement stabilized rammed earth (CSRE) specimens. The cracking in a rammed earth structure is due to the development of tensile stresses. The tensile stresses are generated due to various causes like unequal settlement of foundation, eccentric loading and / or lateral loading such as wind pressure and earthquake on an earth structure. The cracking in a rammed earth structure causes the failure of its intended function. For example formation of crack may lead to the instability of an embankment slope. And earthen dam can be destroyed gradually by erosion of soil at the crack surface (Harison et al. 1994). Hence, it becomes important to understand the fracture behaviour of cement-stabilized rammed earth structures. Well focused studies in understanding the fracture behaviour of CSRE structures are scanty. The present work attempts to address some issues on the fracture behaviour of CSRE including size effect. Through an experimental programme material properties viz. compressive strength, tensile strength and stress-strain relationships are generated for two chosen densities, 17 and 18.5 kN/m3 of CSRE both in dry and saturated condition. Soil composition, density, cement content and moisture content of the specimen during testing influence the characteristics of CSRE. In the present investigation keeping the cement at 10%, the density is varied choosing a soil-sand mixture having optimum grading limits. The basic raw materials used are soil, sand, cement and water in the ratio of 1 : 1.5 : 0.25 : 0.34 by weight. The strength properties studied alone are inadequate to predict the mechanics of fracture due to the presence of microscopic flaws, cracks, voids and other discontinuities. Therefore, some linear elastic fracture parameters such as mode I fracture toughness (KIc), critical energy release rate (GIc), net section strength (f net) and notch sensitivity are calculated, presuming that CSRE is still a brittle material because it is yet to be confirmed that CSRE is a quasibrittle material. In fact, in the present work, it is shown that CSRE has significant amount of softening. A comprehensive experimental work has been undertaken to test CSRE beam specimens for two densities, three sizes of beam and three notch to depth ratios under three point bending (TPB) in a closed loop servo-controlled machine with crack mouth opening displacement control. Results indicate that the CSRE in dry condition exhibits a greater resistance to fracture than the saturated specimen. The variation of net section strength with the notch depth is not significant. Therefore the CSRE material is notch insensitive, implying that it is less brittle. An experimental program was undertaken to determine the nonlinear fracture parameters of beam specimens both in dry and saturated condition. The influence of moisture content, density, size of the specimen as well as notch to depth ratio of the specimen on RILEM fracture energy (G F ) are presented. The GF values increase with increase in density and size of the specimen, while they decrease with increase in notch to depth ratio. Results clearly show that the total energy absorbed by the beams (W OF ) and RILEM fracture energy (G F ) for all specimens tested in dry state are higher compared to the specimens tested in saturated state, indicating that the dry specimen offers higher resistance to the crack propagation. The RILEM fracture energy GF , determined from TPB tests, is said to be size dependent. The assumption made in the work of fracture is that the total strain energy is utilized for the fracture of the specimen. The fracture energy is proportional to the size of the fracture process zone (FPZ), which also implies that size of FPZ increases with increase in the un-cracked ligament (d - a) of beam. This also means that FPZ is proportional to the depth d for a given notch to depth ratio, because for a given notch/depth, (d - a) which is also is proportional to d because is a constant. This corroborates the fact that fracture energy increases with size. Interestingly, the same conclusion has been drawn by Karihaloo et al. (2006). They have plotted a curve relating fracture process zone length and overall depth the beam. In the present study a new method namely Fracture energy release rate method proposed by Muralidhara et al. (2013) is used. In the new method the plot of GF /(d - a) versus (d - a) is obtained from a set of experimental results. The plot is found to follow power law and showed almost constant value of GF /(d - a) at larger ligament lengths. This means the fracture energy reaches a constant value at large ligament lengths reaffirming that the fracture energy from very large specimen is size-independent. This Fracture energy release rate method is used to determine size-independent fracture energy GRf , based on the relationship between RILEM fracture energy and the un-cracked ligament length. The experimental results from the present work agree well with the proposed new method. Similarly, the method is extended to determine nominal shear strength τv for large size beam. Results show that for both densities GRf decrease in saturated condition, while in dry condition as the density is increased from 17 to 18.5 kN/m3 the GRf decrease by 7.58%, indicating that the brittleness increases with higher density. The τv for large size beam increases with density both in dry and saturated condition. The size effect method for evaluating material fracture properties proposed by Bazant (1984) is applied to cement stabilised rammed earth. By measuring the peak loads of 2D geometrically similar notched beam specimens of different sizes, nonlinear fracture parameters such as fracture energy (Gf ), fracture toughness (KIc), effective length of the fracture process zone (Cf ), brittleness number (β), characteristic length (l 0) and the critical crack tip opening displacement (CT ODc) are determined for both dry and saturated conditions. The crack growth resistance curves (R-curve) are also developed for dry and saturated specimens. In the size effect method, for both densities 18.5 and 17 kN/m3 the values of nonlinear fracture properties, namely G f , Cf , KIc, CT ODc and l 0 are lower for the saturated specimen compared to those of the dry specimen. In dry condition as the density is increased from 17 to 18.5 kN/m3 the Gf decreases to 13.54%, indicating that the brittleness increase with higher density. The areas under the load-displacement and load-CMOD curves are a measure of the fracture energy and these areas are low for saturated specimens. The crack growth resistance curves (R-curve) plotted using the size-effect law from peak loads are the measure of resistance against crack growth R. The value of R is high for dry specimen compared to that of the saturated specimens. During aggregate pullout or the opening of crack, the interlock or friction between the crack surfaces may cause the energy dissipation through friction and bridging across the crack. Therefore the wet friction in case of saturated specimen must be smaller resulting in more brittleness compared to the larger dry friction for dry specimen. In the present investigation the Digital Image Correlation (DIC) technique is used to study the FPZ properties in cement stabilised rammed earth. The MATLAB package written by Eberl et al. (2006) is suitably modified and used for image correlation to suit our requirements. CMOD measured using DIC technique is validated by comparison with the CMOD measured using clip gauge. The FPZ properties such as the development of FPZ and crack opening displacements at different loading points as well as the influence of notch/depth ratio on FPZ length (lFPZ ) are evaluated for both dry and saturated conditions. At peak load the lFPZ are about 0.315 and 0.137 times the un-cracked ligament length respectively for specimens tested under dry and saturated conditions. In dry and saturated states the FPZ length decreases as the ratio increases. Lower values of lFPZ in saturated specimen indicates that it is relatively more brittle compared to dry specimen.

Concrete, which was hitherto considered as a brittle material, has shown much better softening behavior after the post peak load than anticipated. This behavior of concrete did put the researchers in a quandary, whether to categorize concrete under brittle materials or not. Consequently concrete has been called a quasi-brittle material. Fracture mechanics concepts like Linear elastic fracture mechanics (LEFM) and Plastic limit analysis applicable to both brittle and ductile materials have been applied to concrete to characterize the fracture behavior. Because of quasi-brittle nature of concrete, which lies between ductile and brittle response and due to the presence of process zone ahead of crack/notch tip instead of a plastic zone, it is found that non-linear fracture mechanics (NLFM) principles are more suitable than linear elastic fracture mechanics (LEFM) principles to characterize fracture behavior. Fracture energy, fracture process zone (FPZ) size and the behavior of concrete during fracture process are the fracture characteristics, which are at the forefront of research on concrete fracture. Another important output from the research on concrete fracture has been the size effect. Numerous investigations, through mathematical modeling and experiments, have been carried out and reported in literature on the effect of size on the strength of concrete and fracture energy. Identification of the sources of size effect is of prime importance to arrive at a clear analytical model, which gives a comprehensive insight into the size effect. With the support of an unambiguous theory, it is possible to incorporate the size effects into codes of practices of concrete design. However, the theories put forth to describe the size effect do not seem to follow acceptable regression. After introduction in Chapter-1 and literature survey in Chapter-2, Chapter-3 details the study on size effect through three point bend (TPB) tests on 3D geometrically similar specimens. Fracture behavior of beams with smaller process zone size in relation to ligament dimension approaches LEFM. The fracture energy obtained from such beams is said to be size independent. In the current work Size effect law (Bazant et al. 1987) is used on beams geometrically similar in three dimensions with the depth of the largest beam being equal to 750mm, and size independent fracture energy G Bf is obtained. In literature very few results are available on the results obtained from testing geometrically similar beams in three dimensions and with such large depth. In the current thesis the results from size effect tests yielded average fracture energy of 232 N/m. Generally the fracture energies obtained from 2D-geometrically similar specimens are in the range of 60-70 N/m as could be seen in literature. From 3D-geometrically similar specimens, the fracture energies are higher. The reason is increased peak load, could be due to increased width. The RILEM fracture energy Gf , determined from TPB tests, is said to be size dependent. The assumption made in the work of fracture is that the total strain energy is utilized for the fracture of the specimen. The fracture energy is proportional to the size of the FPZ, it also implies that FPZ size increases with increase in (W−a) of beam. This also means that FPZ is proportional to the depth W for a given notch to depth ratio, because for a given notch/depth, (W−a) which is also W(1 − a ) is proportional to W`because (1 − a ) is a constant. WWThis corroborates the fact that fracture energy increases with size. Interestingly, the same conclusion has been drawn by Abdalla & Karihaloo (2006). They have plotted a curve relating fracture process zone length and overall depth the beam. In the present study a new method namely Fracture energy release rate method is suggested. In the new method the plot of Gf / (W−a) versus (W−a) is obtained from a set of experimental results. The plot is found to follow power law and showed almost constant value of Gf / (W−a) at larger ligament lengths. This means that fracture energy reaches a constant value at large ligament lengths reaffirming that the fracture energy from very large specimen is size independent. The new method is verified for the data from literature and is found to give consistent results. In a quasi-brittle material such as concrete, a fracture process zone forms ahead of a pre-existing crack (notch) tip before the crack propagates from the tip. The process zone contains a scatter of micro-cracks, which coalesce into one or more macro-cracks, which eventually lead to fracture. These micro-cracks and macro-cracks release stresses in the form of acoustic waves having different amplitudes. Each micro or macro crack formation is called an acoustic emission (AE) event. Through AE technique it is possible to locate the positions of AE events. The zone containing these AE events is termed the fracture process zone (FPZ). In Chapter-4, a study on the evolution of fracture process zone is made using AE technique. In the AE study, the fracture process zone is seen as a region with a lot of acoustic emission event locations. Instead of the amplitudes of the events, the absolute AE energy is used to quantify the size of the process zone at various loading stages. It has been shown that the continuous activities during the evolution of fracture process zone correspond to the formation of FPZ, the size of which is quantified based on the density of AE events and AE energy. The total AE energy released in the zone is found to be about 78% of the total AE energy released and this is viewed as possible FPZ. The result reasonably supports the conclusion, from Otsuka and Date (2000) who tested compact tension specimens, that zone over which AE energy is released is about 95% can be regarded as the fracture process zone. As pointed out earlier, among the fracture characteristics, the determination of fracture energy, which is size independent, is the main concern of research fraternity. Kai Duan et al. (2003) have assumed a bi-linear variation of local fracture energy in the boundary effect model (BEM) to showcase the size effect due to proximity of FPZ to the specimen back boundary. In fact the local fracture energy is shown to be constant away from boundary and reducing while approaching the specimen back boundary. The constant local fracture energy is quantified as size independent fracture energy. A relationship between Gf , size independent fracture energy GF , un-cracked ligament length and transition ligament length was developed in the form of equations. In the proposed method the transition ligament length al is taken from the plot of histograms of energy of AE events plotted over the un-cracked ligament. The value of GF is calculated by solving these over-determined equations using the RILEM fracture energies obtained from TPB tests. In chapter-5 a new method involving BEM and AE techniques is presented. The histogram of energy of AE events along the un-cracked ligament, which incidentally matches in pattern with the local fracture energy distribution, assumed by Kai Duan et al. (2003), along the un-cracked ligament, is used to obtain the value of GF , of course using the same equations from BEM developed by Kai Duan et al. (2003). A critical observation of the histogram of energy of AE events, described in the previous chapter, showed a declining trend of AE event pattern towards the notch tip also in addition to the one towards the specimen back boundary. The pattern of AE energy distribution suggests a tri-linear rather than bi-linear local fracture energy distribution over un-cracked ligament as given in BEM. Accordingly in Chapter-6, GF is obtained from a tri-linear model, which is an improved bi-linear hybrid model, after developing expressions relating Gf , GF , (W−a) with two transition ligament lengths al and blon both sides. The values of Gf , and GF from both bi-linear hybrid method and tri-linear method are tabulated and compared. In addition to GF , the length of FPZ is estimated from the tri-linear model and compared with the values obtained from softening beam model (SBM) by Ananthan et al. (1990). There seems to be a good agreement between the results. A comparative study of size independent fracture energies obtained from the methods described in the previous chapters is made. The fracture process in concrete is another interesting topic for research. Due to heterogeneity, the fracture process is a blend of complex activities. AE technique serves as an effective tool to qualitatively describe the fracture process through a damage parameter called b-value. In the Gutenberg-Richter empirical relationship log 10N=a−bM, the constant ‘b’ is called the b-value and is the log linear slope of frequency-magnitude distribution. Fault rupture inside earth’s crust and failure process in concrete are analogous. The b-value, is calculated conventionally till now, based on amplitude of AE data from concrete specimens, and is used to describe the damage process. Further, sampling size of event group is found to influence the calculated b-value from the conventional method, as pointed out by Colombo et al. (2003). Hence standardization of event group size, used in the statistical analysis while calculating b-value, should be based on some logical assumption, to bring consistency into analytical study on b-value. In Chapter-7, a methodology has been suggested to determine the b-value from AE energy and its utilization to quantify fracture process zone length. The event group is chosen based on clusters of energy or quanta as named in the thesis. Quanta conform to the damage stages and justify well their use in the determination of the b-value, apparently a damage parameter and also FPZ length. The results obtained on the basis of quanta agree well with the earlier results.

La miniaturisation des composants est aujourd’hui un challenge mondial. La fabrication de ces composants est rendue difficile par un certain nombre de phénomènes liés aux effets d’échelle. Il est ainsi nécessaire de répondre à ces contraintes de réduction d’échelle en termes de conception, de réalisation et de fonctionnement de ces systèmes. Cette étude aborde la problématique de la miniaturisation des procédés et plus particulièrement du procédé de micro-formage incrémental « mono-point » (micro-SPIF) à travers des études expérimentales et numériques. Le micro-formage incrémental de tôles est présenté comme une approche intéres sante de fabrication de structures minces. La géométrie désirée est assurée par la trajectoire d’un outil imposant une déformation locale sur la tôle serrée en son contour. Dans un premier temps, une approcheexpérimentale consistant à analyser le comportement mécanique des éprouvettes en alliage de cuivre avec différentes tailles de grains par des essais de traction a été proposée. L’interaction entre la géométrie et la microstructure est évaluée à l’aide du ratio de l'épaisseur par la taille moyenne de grains Φ=t/d. Un pilote de formage incrémental « mono-point » instrumenté a été également développé. Une campagne d'essais expérimentaux de micro-SPIF a été ainsi réalisée sur des flans par différentes tailles de grains afin d'étudier les effets de la microstructure sur la géométrie, l’état de surface, la distribution des épaisseurs et sur l’évolution des efforts. Dans un second temps, un modèle paramétrique de type éléments finis simulant le micro-SPIF a été développé en langage MATLAB®. Le code de calculs LS-DYNA® a été utilisé pour simuler le procédé en adaptant une loi de comportement élastoplastique. Ensuite, les résultats obtenus en termes de géométrie,d’évolution de l’épaisseur et d’efforts de formage sont confrontés aux relevés expérimentaux afin de valider la procédure numérique. Dans un troisième temps, une loi élastoplastique endommageable décrivant les principaux phénomènes physiques intervenant durant le formage des métaux en grandes déformations a été présentée. Une procédure d'identification de cette loi basée sur une analyse inverse de l’effort au cours du procédé de micro-SPIF a été proposée et des tests de validation du modèle ont été discutés. Enfin, une analyse de l'identifiabilité locale basée sur un indice de multicolinéarité des fonctions de sensibilité est effectuée pour valider la procédure d’identification paramétrique et quantifier l’intérêt du procédé pour la caractérisation quantitative des tôlesminces en très grandes déformations / The miniaturization of components is now a world challenge. The manufacture of these componentsis difficult because of several phenomena related to the so-called size effect. It is thus necessary to fulfill theserequirements of scaling down in terms of design, implementation and operations. This study deals with theproblems of miniaturization processes, especially the “micro-Single Point" Incremental Forming process (micro-SPIF) through experimental and numerical studies. Micro-single point incremental forming process is presentedas an interesting approach for thin structures manufacturing. The desired geometry is provided by the tool pathrequiring a local deformation in a sheet clamped along its contour. Firstly, an experimental approach consistingin analyzing the mechanical behaviour of copper alloy specimens with various grain sizes by tensile tests hasbeen proposed. The interaction between the geometry and the microstructure is evaluated using the ratio of thethickness by the average grain size Φ=t/d. An instrumented micro-SPIF device was also developed. A set ofsingle point incremental sheet forming experimental tests were conducted on blanks with several grain sizesusing two forming strategies in order to study the effect of microstructure on the geometry, the surface topology,the thickness distribution and the forming forces evolutions. Secondly, a finite element parametric model capableof simulating the micro-SPIF process was developed in MATLAB® language. The commercial LS-DYNA® codewas used to simulate this process using an elastic-plastic constitutive law. Then, the results obtained in terms ofgeometry, thickness evolution and forming forces are compared with the experimental results in order to validatethe numerical procedure. Thirdly, an elastic-plastic damage model describing the main physical phenomenainvolved during metal forming by large deformation was presented. An identification procedure of thisbehaviour law based on the inverse analysis of the axial forming force during micro-SPIF process was proposedand several validation tests of the model were discussed. Finally, local identifiability analysis based on an indexof multicollinearity of the sensitivity functions was performed in order to validate the parameters identificationprocedure and quantify the advantage of the process for quantitative mechanical behaviour characterization ofthin metal sheets at large strains

Un nouveau procédé d’élaboration de CMC par voie liquide a été développé ; il met en œuvre l’utilisation de charges réactives afin d’obtenir un composite à bas coût. Afin de préserver le renfort en fibres Nicalon, ces charges doivent réagir sous azote à une température inférieure à 1100°C. Deux charges réactives répondant ces critères et présentant une prise de volume intéressante ont été identifiées : AlB2 et TiSi2.Le broyage planétaire de ces charges a été étudié afin d’évaluer l’influence de l’affinement de la microstructure sur les propriétés. Des poudres de surface spécifique élevée et de granulométrie proche l’échelle nanométrique ont été obtenues. La nitruration des charges a été analysée et un effet de taille a pu être mis en évidence sur la réactivité du TiSi2.Les poudres broyées ont été mises en suspension pour être imprégnées au sein de préformes. Les échantillons ont ensuite subi une étape de nitruration à 1100°C, cruciale pour la cohésion de la matrice. Un cycle PIP a ensuite été réalisé pour diminuer la porosité résiduelle.L’oxydation des matériaux obtenus a été étudiée dans des conditions correspondant à l’application aéronautique visée. Les propriétés mécaniques des composites élaborés ont été évaluées par des essais de flexion 3 points. La combinaison de l’utilisation de la charge réactive TiSi2 et d’un polysiloxane a permis d’obtenir un composite dont la contrainte à rupture est remarquable compte tenu du faible nombre d’étapes nécessaires à son élaboration par voie liquide. / A new CMC manufacturing process has been developped ; the active filler technique is used in order to obtain a low cost composite. Active fillers must react under nitrogen atmosphere at a temperature below 1100°C so that the Nicalon fiber reinforcement is not damaged. Two active fillers meeting these criteria and offering an interesting volume expansion have been identified : AlB2 et TiSi2.The planetary milling of these fillers has been explored in order to assess the influence of microstructure refinement on properties. Powders with high specific surface areas and of granulometry close to the nanometric scale were obtained. The nitridation of the active fillers was examined and a size effect on TiSi2 reactivity was displayed.Milled powders were used in colloidal suspensions in order to be impregnated in preforms. Samples were subsequently nitrided at 1100°C ; this step was crucial for matrix cohesion. A PIP cycle was eventually performed in order to reduce residual porosity.The oxydation behaviour of materials was studied in conditions corresponding to the considered aeronautics application. Mechanical properties of composites were estimated by 3 point bending tests. Combining the use of TiSi2 and of a polysiloxane enabled to obtain a composite whose maximum bending stress was remarkable considering the limited number of steps required for its processing.

In der Dissertation werden Konzepte vorgestellt, mit denen die Abschätzung der Dauerfestigkeit von Bauteilen auf Grundlage von Werkstoffkennwerten möglich ist. Aus den sich dabei ergebenden Problemen sowie den speziellen Anforderungen der Werkstoffgruppe Sinterstahl wird ein neues Konzept aus bruchmechanischen Überlegungen abgeleitet. Damit ist eine Anwendung ohne prinzipielle Einschränkung bezüglich der Bauteilgeometrie und unter Berücksichtigung der individuellen Kerbempfi ndlichkeit des Werkstoffs möglich. Die Validierung und statistische Auswertung anhand einer breiten Datenbasis belegt eine gute Treffsicherheit im Vergleich zu anderen Verfahren. Empfehlungen zur praktischen Anwendung und den Grenzen der verschiedenen Konzepte werden gegeben.

The overall objective of this study was to develop an optimised Ultra-High-Performance Concrete (UHPC) matrix based on the modified Andreasen and Andersen optimum particle packing model by using available South African materials. The focus of this study was to determine the optimum combined fibre and superplasticiser content for UHPC by using a response surface design. The UHPC was appropriately designed, produced and tested. Various changes in mechanical properties resulting from different combinations of steel fibre and superplasticiser contents was investigated. The flowability, density and mechanical properties of the designed UHPC were measured and analysed. Both the fibre and superplasticiser content play a significant role in the flowability of the fresh concrete. The addition of fibres significantly improved the strength of the concrete. The results show that the superplasticiser content can be increased if a more workable mix is required without decreasing the strength significantly. The statistical analysis of the response surface methodology confirms that the designed models can be used to navigate the design space defined by the Central Composite Design. The optimum combined fibre and superplasticiser content depend on the required mechanical properties and cost. Using the modified Andreasen and Andersen particle packing model and surface response design methodology, it is possible to efficiently produce a dense Ultra-High-Performance Fibre Reinforced Concrete (UHPFRC) with a relatively low binder amount, low fibre content and good workability. The effect of heat curing on the mechanical properties was investigated. It was concluded that heat curing is not recommended when considering the long-term strength development. The estimated strength development of concrete obtained by using the fib Model Code 2010 (2013) does not incorporate the detrimental effect of high curing temperatures on long-term strength and therefore overestimate the long-term strengths. The strength estimates for both early and long-term ages can be improved by considering this effect in the strength development functions obtained from fib Model Code 2010 (2013). The effect of specimen size on the compressive and flexural tensile strength of UHPFRC members were established. It was found that the specimen size has a significant effect on the measured cube compressive strength. Smaller beam specimens showed higher ductility compared to those of the larger beam specimens. The crack width decreased as the beam’s depth decreased. A lower variability was experienced in the beams with limited depth (< 45 mm). Further testing is required to determine whether a span-to-depth ratio of 10 would yield optimum results. The utilisation of by-products, such as undensified silica fume and fly ash, as cement replacement materials makes UHPFRC sustainable, leading to a reduced life-cycle cost. The calculated Embodied Energy per unit strength (EE/unit strength) and Embodied Carbon per unit strength (EC/unit strength) values for the UHPFRC mixture yield lower values compared to that of the 30 MPa concrete mixture, indicating that UHPFRC can be used to reduce the environmental footprint of the concrete industry. The inverse analysis method used was successful in providing an improved simplified stress-strain response for the UHPFRC. The analysis provided valuable information into the stress-strain, load-deflection and moment-curvature responses of the UHPFRC. Standard material test results were used to theoretically calculate moment-curvature responses and were then compared to the experimental results obtained. The study demonstrated that it is possible to efficiently produce a dense and workable UHPFRC with relatively low binder amount and low fibre content. This can result in more cost-effective UHPFRC, thus improving the practical application thereof. / Dissertation (MEng)--University of Pretoria, 2020. / Civil Engineering / MEng (Structural engineering) / Unrestricted

The scope of the presented master thesis was the experimental study of multi-filament yarns made of AR-glass and used for textile-reinforced concrete. The behavior under the tensile loading was investigated by laboratory tests. A high number of yarn specimens (over 300) of six different lengths (from 1 cm to 74 cm) was tested to obtain statistically significant data which were subsequently corrected and statistically processed. The numerical model of the multi-filament bundle was studied and applied for prediction of the yarn performance and for later results interpretation. The model of n parallel filaments describes the behavior of a bundle with varying parameters representing different sources of disorder of the response and provides the qualitative information about the influence of their randomization on the overall bundle response. The aim of the carried experiment was to validate the model presumptions and to identify the model parameters to fit the real load-displacement curves. Unfortunately, due to unsuccessful correction of measured displacements devalued by additional non-linear contribution of the unstiff experiment device the load-displacement diagrams were not applicable to model parameters identification. The statistical evaluation was carried only for the maximal load values and the effect of the specimen size (length) on its strength was demonstrated. The size effect curve did not exclude the existence of spatial correlation of material mechanical properties modifying the classical statistical Weibull theory.

The work occupy by inverse analysis based on artificial neural network. This identification algorithm enable correct determine parameters of applied material model on creation of numerical model of construction so it's possible that the results of computerized simulation correspond with experiments. It look's like suitable approach especially in cases with complicated problems and complex models with many material parameters.

Die Nanoindentation ist ein inzwischen etabliertes Verfahren zur Bestimmung der Materialkennwerte Härte und Elastizitätsmodul in kleinen Größendimensionen. Eine zusätzliche Bestimmung der Fließspannung aus solchen Nanoindentationsexperimenten würde deren Einsatzmöglichkeiten deutlich erweitern und zum Beispiel für die Bauteilauslegung kleiner Strukturen, Schichtcharakterisierung und die Beschaffung von Simulationseingangsdaten einen großen Fortschritt bedeuten. Diese Gründe machen das Thema zu einem aktuellen Forschungsgegenstand. In der vorliegenden Arbeit steht deswegen die Bewertung von Fließspannungsbestimmungsverfahren für Massivmaterialien in der Nanoindentation mittels einer Kombination aus Finite-Elemente-Simulationen und umfangreichen Experimentaldaten im Zentrum. Im Speziellen wird dabei das Konzept des effektiv geformten Indenters mit dem erweiterten Hertzschen Ansatz und dessen Anwendung zur Fließspannungsbestimmung aus Eindringversuchen mit selbstähnlichen Berkovichpyramiden betrachtet. Zur Bearbeitung dieser Aufgabenstellung wurden unter anderem drei Referenzverfahren zur Fließspannungsbestimmung (die Expanding cavity-Modelle, das Loading partial unloading-Verfahren und Minidruckversuche) ausführlich charakterisiert. Damit konnten dann im Weiteren belastbare Referenzfließspannungen für die umfangreiche Experimentaldatenbasis zur Verfügung gestellt werden. Außerdem wurden die untersuchten Materialien auf den Einfluss der Größenabhängigkeit der Fließspannungen, den Indentation size effect, hin untersucht. Dabei wurden die vorliegenden physikalischen Vorgänge in den Proben beschrieben, dahingehende Unterschiede bei den betrachteten Referenzverfahren charakterisiert und den Fließspannungswerten die Fließzonendimensionen zugeordnet. Mit den damit zur Verfügung stehenden Informationen konnte das Konzept des effektiv geformten Indenters in seiner Anwendung zur Fließspannungsbestimmung grundlegend bewertet werden. Alle Untersuchungen wurden dabei stets parallel mit Hilfe von Simulations- und Experimentaldaten durchgeführt, um tiefere Einblicke in die zu Grunde liegende Mechanik der Fließprozesse zu gewinnen.

Birch plywood has favorable mechanical properties that could be used in new types of connections for timber structures, and thus enable a substitution of the current system with steel plates. Such new connections could result in significant advantages in terms of environmental impact and economy as well as ease of prefabrication and mountability. However, there is a lack of data concerning some of the mechanical properties of birch plywood that would be necessary in order to perform a safe design. In particular, there is a lack of reliable data and understanding of the mechanical properties of birch plywood in directions other than along and perpendicular to the face grain. The aim of this thesis is to gain new knowledge about this anisotropy and to study the variation of the in-plane mechanical properties of birch plywood at different loading angles to the face grain, including effects of size and moisture changes. The goal is that this knowledge will serve as input for the design of birch plywood connections under various loading conditions in timber structures. Specifically, birch plywood specimens were laboratory tested in in-plane tension, compression, shear and bending. The results show that birch plywood possesses the highest tensile, compressive and bending strength and elastic modulus parallel to the face grain and the lowest ones at 45° to the face grain. The opposite findings were noticed for the shear strength and the shear modulus. Moreover, a size effect on the in-plane bending strength property was observed at 0° (parallel) and 90° (perpendicular) to the face grain but not at other angles, which is attributed to the different failure mechanisms. In addition, the increase of moisture leads to the decreased bending strength and elastic modulus in the hygroscopic range. Validated by the experimental work, both analytical and numerical models to predict the mechanical performance of birch plywood under different load conditions and various moisture contents are proposed. / Björkplywood har gynnsamma mekaniska egenskaper som skulle kunna användas i nya typer av knutpunkter (förband) för träkonstruktioner, och därmed möjliggöra en substituering av dagens system med stålplåtar. Sådana nya knutpunkter kan innebära avsevärda fördelar när det gäller miljöpåverkan och ekonomi samt en enkel prefabricering och monterbarhet. Det saknas dock data när det gäller vissa mekaniska egenskaper hos björkplywood som är nödvändiga för att kunna utföra en säker design. I synnerhet saknas tillförlitliga data och förståelse kring de mekaniska egenskaperna hos björkplywood i andra riktningar än längs och tvärs dess ytfanér. Syftet med denna avhandling är att ta fram ny kunskap om denna anisotropi och studera variationen av de mekaniska egenskaperna hos björkplywood i dess plan vid olika belastningsvinklar mot ytfanérets fiberriktning, inklusive effekter av storlek och fuktförändringar. Målet är att denna kunskap ska fungera som input för design av björkplywood-förband under olika belastningsförhållanden i träkonstruktioner. Specifikt testades prover av björkplywood i dess plan i drag, tryck, skjuvning och böjning. Resultaten visar att björkplywood har den högsta drag-, tryck- och böjhållfastheten och elasticitetsmodulen parallellt med ytfanérets fiberriktning och den lägsta vid 45° mot densamma. Det motsatta gäller för skjuvhållfasthet och -modul. Dessutom observerades en storlekseffekt avseende böjhållfastheten vid 0° (parallell) och 90° (vinkelrätt) mot ytfanérets fiberriktning men inte vid andra vinklar, vilket förklaras genom de olika brottmekanismerna. Dessutom leder ökningen av fukt till minskad böjhållfasthet och elasticitetsmodul i det hygroskopiska området. Validerat av det experimentella arbetet föreslås både analytiska och numeriska modeller för att förutsäga den mekaniska prestandan hos björkplywood under olika belastningsförhållanden och olika fuktkvoter. / <p>QC 20221117</p>