This thesis is on fatigue crack growth experiments and assessments of fatigue crack growth rates. Both constant and variable amplitude loads in two different materials are considered; a nickel based super-alloy Inconel 718 and a stainless steel 316L. The considered load levels extend from small scale yielding (SSY) to large scale yielding (LSY) for both materials. The effect of different load schemes on the fatigue crack growth rates is investigated on Inconel 718 and compact tension specimens in Paper A. It is concluded that load decreasing schemes give a to high Paris law exponent compared to constant or increasing load amplitude schemes. Inconel 718 is further analyzed in Paper B where growth rates at variable amplitude loading in notched tensile specimens are assessed. The predictions are based on the fatigue crack growth parameters obtained in Paper A. The crack closure levels are taken into consideration and it is concluded that linear elastic fracture mechanics is incapable of predicting the growth rates in notches that experience large plastic cyclic strains. Even if crack closure free fatigue parameters are used and residual stresses due to plasticity are included. It is also concluded that crack closure free and nominal fatigue crack growth data predict the growth rates equally well. However, if the crack closure free parameters are used, then it is possible to make a statement in advance on the prediction in relation to the experimental outcome. This is not possible with nominal fatigue crack growth parameters. The last three papers consider fatigue crack growth in stainless steel 316L. Here the load is defined as the crack tip opening displacement parameter. Paper C constitutes an investigation on the effect of plastic deformation on the potential drop and consequently the measured crack length. It is concluded that the nominal calibration equation obtained in the undeformed geometry can be used at large plastic deformations. However, two conditions must be met: the reference potential must be taken in the deformed geometry and the reference potential needs to be adjusted at every major change of plastic deformation. The potential drop technique is further used in Paper D and Paper E for crack length measurements at monotonic LSY. Constant amplitude loads are considered in Paper D and two different variable amplitude block loads are investigated in Paper E. The crack tip opening displacement is concluded in Paper D to be an objective parameter able to characterize the load state in two different geometries and at the present load levels. Furthermore, if the crack tip opening displacement is controlled in an experiment and the local load ratio set to zero, then only monotonic LSY will appear due to extensive isotropic hardening, i.e. elastic shake-down. This is also the reason why the linear elastic stress-intensity factor successfully could merge all growth rates, extending from SSY to monotonic LSY along a single line in a Paris law type of diagram, even though the generally accepted criteria for SSY is never fulfilled. For the variable amplitude loads investigated in Paper E, the effect of plastic deformation on measured potential drop is more pronounced. However, also here both the crack tip opening displacement parameter and the linear elastic stress-intensity factor successfully characterized the load state. / <p>QC 20130108</p>

One of the most prominent factors affecting the performance and longevity of risers is vortex induced vibration (VIV), which can cause severe fatigue damage, especially in risers used in deep waters. The available approaches for analyzing VIV induced fatigue in risers mainly focus on the VIV aspect of the problem; indeed less attention has been paid on the effect of VIV on a riser’s fatigue life and in prediction of fatigue life using various models. This dissertation first demonstrates how one can characterize fatigue of pipes and risers using an equivalent plate specimen as opposed to using a pipe specimen, thereby simplifying the task, yet obtaining good accuracy. Actual variable amplitude loadings (VAL) are used to study the fatigue crack growth in risers’ material with a focus on the various influencing parameters. Extensive experimental investigations are performed, followed by analytical and computational nonlinear finite element analyses. It is shown that the higher harmonics do cause significant fatigue damage, thus their influence should not be ignored. The influence of load interaction effects is also investigated, focusing on the fatigue crack growth retardation effects due to tension overloads, as well as the acceleration effects due to compression underloads. The crack closure concept is then used to explore into both the fatigue retardation and acceleration effects within a VAL scenario. An effective method for calculation of the stress intensity factor is proposed, which considers only the tensile portion of the stress range, while proposing another effective approach for accounting for the influence of compressive stress cycles. Moreover, a two-parameter approach is used in this dissertation, relating the fatigue crack growth rate (FCGR) to the crack tip opening displacement (CTOD). It is shown that the CTOD provides adequate information for calculating the FCGR under VAL, and it can be effectively used to account for the influence of the compressive stress cycles. The experimental investigation also considers the retardation effect resulting from the applied peak tensile overload cycles (TOLC) and the influence of various so-called “clipping” levels, demonstrating the significant influence of the TOLC on crack growth retardation in VAL.

L’interaction statique et dynamique entre une sonde locale et un film de liquide provoque la déformation de ce dernier. Ce phénomène a été décrit par des équations analytiques, qui ont été analysées et résolues numériquement. Les potentiels d’interaction sonde/liquide et liquide/substrat ont été déduits à partir de l’intégration des forces de dispersion. La différence de pression à travers l’interface air/liquide a été calculée avec une équation de Young-Laplace modifiée, qui prend en compte les effets de la gravité, de tension superficielle, ainsi que les potentiels d’interaction liquide/substrat et sonde/liquide. Pour le cas statique, l’équation modifiée de Young-Laplace en équilibre a été examinée. La théorie de la lubrification a été utilisé pour décrire l’évolution du film liquide, afin d’analyser le phénomène dynamique. Des simulations numériques de la forme de la surface d’équilibre et de l’évolution dynamique du film ont été réalisées. Des comportements stables et instables ont été discernés, et les résultats ont confirmé l’existence d’une distance de seuil, pour le cas statique, et d’une combinaison de paramètres d’oscillation, pour la situation dynamique, pour lesquelles le saut du liquide vers la sonde se produit. Une analyse théorique a confirmé l’existence de conditions critiques qui séparent les régimes de comportement. Ces conditions critiques indiquent le rôle des paramètres physiques et géométriques dans la stabilité du système. Pour le cas dynamique, les résultats préliminaires sont rapportés et une interprétation qualitative du phénomène est formulée. En outre, des expériences de spectroscopie AFM de force et amplitude ont été effectuées et comparées avec les résultats numériques. / The static and dynamic interaction between a local probe and a liquid film provokes the deformation of the latter. This phenomenon has been described by means of analytical equations, which had been analyzed and numerically solved. Probe/liquid and liquid/substrate interaction potentials have been deduced from the integration of the dispersion forces. The pressure difference across the air/liquid interface has been calculated with a modified Young-Laplace equation, which takes into account the effects of gravity, surface tension, the liquid film/substrate and the probe/liquid interaction potentials. For the static case, the equilibrium modified Young-Laplace equation has been considered. The lubrication theory has been used to describe the liquid film evolution, in order to analyze the dynamic phenomenon. Numerical simulations of the equilibrium surface shape and the dynamic evolution of the film have been performed. Stable and unstable behaviors had been discerned, and results confirmed the existence of a threshold distance, for the static case, and a combination of oscillation parameters, for the dynamic situation, for which the jump of the liquid to contact the probe occurs. A theoretical analysis confirmed the existence of critical conditions separating the behavior regimes. This critical conditions indicate the role of the physical and geometric parameters in the system stability. For the dynamic case, preliminary results are reported and a qualitative interpretation of the phenomenon is formulated. In addition, AFM force and amplitude spectroscopy experiments had been performed and compared with the numerical results.

Este trabalho discutiu o estudo da inferência de carregamento e a reconstrução fratográfica da taxa de propagação da trinca por fadiga em histórias de vôos simulados do tipo Twist, mini-Twist, Falstaff e mini-Falstaff. O material estudado foi uma liga de alumínio de grau aeronáutico SAE-AMS 7475 T7351 na qual foram obtidas as propriedades mecânicas a partir dos ensaios de tração e dureza, análise química, metalográfica. Foram realizados ensaios de amplitude constante de carregamento em corpos de prova com geometria tipo C(T) extraídos de um bloco e ensaios de amplitude variável em corpos de prova com geometria tipo M(T) extraídos de uma placa. Corpos de prova do tipo C(T) foram extraídos da orientação L-T e T-L, à temperatura ambiente com diferentes espessuras para a realização de ensaios de propagação de trinca por fadiga (da/dN vs. &#916K) com distintos valores de razão de carregamento,R (0,1;0,3; 0,5; 0,7 e 0,8) de acordo com a norma ASTM-E647 (1993). Foram realizados dois tipos de ensaios de fadiga com amplitude constante de carregamento. Primeiro, o ensaio com &#916P constante para obtenção dos dados dos estágios II e III das curvas da/dN vs. &#916K para distintos valores de R e, posteriormente, o ensaio com &#916K constante e R crescente para ser utilizado no estudo da inferência de carregamento de amplitude constante a partir da relação entre a morfologia da estria, H/s e a razão de carregamento R. Adicionalmente foram realizados ensaios de tenacidade à fratura, nas direções L-T e T-L, conforme a norma ASTME1820 (1999). As taxas de propagação macroscópica e microscópica foram comparadas e boas correlações foram obtidas para um intervalo entre 0,1 a 1,0 &#956m/ciclo, mesmo com distintos R. Através da técnica proposta por Berkovitz (1995), o espectro de carregamento foi estimado para distintos valores de R, através da técnica de parametrização do fator K e os resultados foram comparados ao espectro de carregamento real imposto pela máquina de ensaio. Após os ensaios de amplitude constante de carregamento foram realizados ensaios de amplitude variável com a aplicação em corpos de prova M(T) de espectros de vôos simulados padronizados pela NLR do tipo Twist e Falstaff e seus vôos reduzidos, mini-Twist e mini- Falstaff, em uma máquina servohidráulica de ensaios dinâmicos. A partir destes ensaios notou-se que suprimir os vôos com os carregamentos menos severos influencia muito a vida da propagação da trinca de fadiga, quando vôos simulados do tipo Twist e mini-Twist, fato este não observado para o Falstaff e mini-Falstaff. Foi possível observar também o efeito da aceleração e desaceleração da trinca por fadiga observando os gráficos de d2a/dvôo vs. a obtidos dos ensaios de amplitude variável. Foi realizado um estudo da superfície de fratura do CP05 por meio da técnica fractográfica do reconhecimento de blocos marcadores sendo possível mostrar uma satisfatória reconstituição da taxa de propagação da trinca por fadiga de vôo simulado do tipo Falstaff por meio de medidas das marcações na superfície de fratura dos vôos mais severos, realizadas em imagens obtidas por MEV. / The loading inference and the fractographic reconstruction of fatigue crack propagation rate in simulated flight stories, as Twist, mini-Twist, Falstaff and mini-Falstaff were investigated in this work. The studied material was an aluminum alloy SAE-AMS 7475 T7351. Tensile and hardness tests were carried out in order to determine mechanical properties, as well as chemical and microstructure analysis of the material. C(T) specimens were extracted from a block of material for constant amplitude load testing and M(T) specimens were extracted from a plate and were tested in variable amplitude loading. The curves (da/dN vs. &#916K) for constant-amplitude loading were obtained from fatigue crack propagation tests performed in L-T and T-L directions in C(T) specimens for R (0.1; 0.3; 0.5; 0.7 and 0.8), at room temperature, according to ASTM-E647 (1993). Two different constant loading fatigue tests were performed. At constant &#916P and distinct values of R for obtaining data of stages II and III of da/dN - &#916K curves; and at constant &#916K and increasing the R ratio to be used in the inference of constant amplitude loading in the relation of H/s striation morphology (obtained from fractographic images) and the loading ratio, R. Additionally, fracture toughness tests were executed in T-L and L-T directions, according to ASTM-E1820 (1999). The macroscopic and microscopic fatigue crack propagations were compared and good correlation was obtained for the range 0.1-1.0 &#956m/cycle, for all R values. By using the K factor parametrization method, Berkovitz (1995), the loading spectrum was estimated for the distinct R-values and the results were compared to the actual spectrum imposed by the test machine. Variable amplitude tests were performed in M(T) specimens by applying simulating flight spectra normalized by NLR, as Twist, mini-Twist, Falstaff and mini-Falstaff, in a servohydraulic test machine MTS, in which a Flextest GT controller was coupled. The suppression of less severe loading flights showed a great influence in fatigue crack propagation life, in simulated flight tests Twist and mini-Twist, but not in Falstaff and mini-Falstaff. The acceleration and slowing down of fatigue crack were observed in the d2a/dflight - a curve obtained from variable loading tests. The fractured surfaces of some samples were examined by the fractographic technique of blocking marks recognition. A good reconstitution of fatigue crack propagation rate of a simulated flight like Falstaff was obtained by the measurements of marks in the fracture surfaces of the more severe flights, in MEV images.

Neste trabalho foram sintetizados a poli-2-etinilpiridina (P2EP), poli-4etinilpiridina (P4EP), o iodeto de poli(2-N-t-butilpiridiniumilacetileno) (P2EPtBu) e a poli-&#946;-etinilnaftaleno (P&#946:EN), os quais são poliacetilenos substituídos. Estes polímeros, juntamente com o cloreto de poli(2-piridínio-2-piridilacetileno) (P2EPH), foram caracterizados por espectroscopia vibracional no infravermelho e Raman. Estes polímeros apresentaram variação na posição das bandas Raman com a energia da radiação excitante - chamada dispersão Raman ou fotosseletividade - da ordem de 10 cm-1, bem inferior ao apresentado pelo poliacetileno (cerca de 60 cm-1). Este deslocamento foi interpretado utilizando-se dois dos modelos existentes para descrever este fenômeno: o Modelo de Modo de Amplitude (AMM) e o Modelo de Coordenada de Conjugação Efetiva (ECCM), os quais fornecem informações sobre a estrutura polimérica e sobre seus níveis eletrônicos. Utilizando-se o AMM foi possível obter informações sobre os níveis eletrônicos excitados de mesma simetria que o estado eletrônico fundamental. Por outro lado, o ECCM, com a ajuda de cálculos DFT, mostrou diferenças na extensão da conjugação e no grau de dimerização entre o P2EP na forma cis e trans e indicou que este polímero apresentava, predominantemente, a estrutura cis, fato este confirmado pelos espectros no infravermelho. A dopagem com I2 provocou efeitos diferentes na estrutura dos polímeros. Os espectros no infravermelho dos polímeros dopados indicaram que o P2EP e o P2EPH apresentaram aumento na quantidade de segmentos cis enquanto o P2EPtBu apresentou diminuição na quantidade desses segmentos. Os espectros Raman dos polímeros dopados confirmaram os dados dos espectros no infravermelho. Esta diferença foi interpretada como sendo devida à diferença no volume do substituinte, pois grupos volumosos favorecem o isômero trans-cisóide onde a distância entre os substituintes é maior. A dopagem também levou a um aumento na condutividade dos polímeros, porém os valores de condutividade obtidos foram bem inferiores que os apresentados pelo poliacetileno dopado (10-5 a 10-7 contra 102 S cm-1, tipicamente). / In this work poly-2-ethynylpyridine (P2EP), poly-4-ethynylpyridine (P2EP), poly(2-N-t-butylpyridiniumylacetylene) iodide (P2EPtBu) and poly-&#946;-pethynylnaphthalene (P&#946;EN) were synthesized. These polymers, which are polyacetylenes derivatives, and poly(2-pyridinium-2-pyridylacetylene) chloride (P2EPH) were analyzed by vibrational techniques. It was observed that some Raman band positions shifted when excitation energy was changed, however this shift (ca. 10 cm-1) was substantially smaller than the presented by polyacetylene (ca. 60 cm-1). This phenomenon called Raman dispersion or photoselectivity - was examinated using Amplitude Mode Model (AMM) and Effective Conjugation Coordinate Model (ECCM) and gave us important information about polymer structure and its electronic energies levels. Using AMM it was possible to infere information about electronic excited states with the same symmetry of the electronic ground state. ECCM gave us evidences about differences in conjugation extension and dimerization degree between cis and trans structures. Besides this, ECCM was successful in indicating cis structure to P2EP. Infrared spectrum confirmed that this polymer is mainly cis. I2 doping of P2EP, P2EPH and P2EPtBu provoked differents perturbations in these systems. P2EP and P2EPH increased their cis segments amount, as showed by infrared spectra. On the other hand, this doping induced the decrease of cis segments in P2EPtBu. Raman spectroscopy supported these conclusions too. This difference was interpretated as due to the side group volume, which could favour one or another isomerization. Electronic conductivity increased by doping for all these three polymers, however the conductivity is considerably lower than the presented by polyacetylene (from 10-5 to 10-7 S cm-1 for these substituted polyacetylenes against typically 10-2 S cm-1 for polyacetylene).

Les structures en béton armé ou en bois se dégradent sous des actions mécaniques et climatiques. Les propriétés physiques et mécaniques de ces matériaux sont liées aux conditions d'exposition et à leurs variations. L’évaluation non destructive de ces propriétés en amont des dégradations est une nécessité pour les maîtres d'ouvrages afin de prédire la durée de vie des structures dans un contexte de gestion durable du patrimoine bâti. La présence d’eau dans les pores du béton est un facteur qui facilite la pénétration des agents agressifs (dioxyde de carbone, chlorures, etc. responsables de l’initiation de pathologies comme la corrosion des aciers). Pour le cas du matériau bois, les causes les plus fréquentes des détériorations sont souvent d’origine biologiques (champignons et insectes). L’humidité est également reconnue comme une des conditions les plus importantes pour le développement de ces attaques. Il est donc nécessaire d’évaluer et de quantifier la variation spatiale de l’humidité dans ces matériaux de construction pour limiter les actions de réparation. Le système radar (Ground Penetrating Radar, « GPR ») est un outil d’auscultation des matériaux totalement non destructif, rapide, compact et sans contact. Cette technique est basée sur la propagation des ondes électromagnétiques. Cette propagation est fortement liée à la permittivité et la conductivité du matériau qui sont très sensibles aux variations de l’humidité. L’objectif de cette thèse est double : d’une part, modéliser l’effet des variations de l’humidité dans un matériau homogène, multi-couches ou avec gradient, et d’autre part, de quantifier expérimentalement l’effet d’un gradient d’humidité sur le béton et celui de l’anisotropie sur le bois. Pour cela, un modèle analytique a été développé en se basant sur la notion des lois de mélange (ajustées sur des mesures expérimentales de la permittivité en prenant en compte l’effet de la dispersion fréquentielle) et sur la propagation d’une onde plane. Une simulation numérique a permis d’apprécier l’effet d’un gradient et d’un milieu anisotropique sur la vitesse de propagation des ondes radar. La phase expérimentale a été effectuée sur un matériau modèle homogène et isotrope comme le sable pour comparer les différentes méthodes de mesure de la vitesse de l’onde directe. Une analyse fréquentielle de l’atténuation a été également étudiée pour évaluer la dispersion de l’atténuation dans un milieu considéré comme homogène. La deuxième partie de l’expérimentation a consisté à suivre par mesures radar le séchage d’une dalle en béton instrumentée par capteurs d’humidité. Enfin, une campagne expérimentale sur des échantillons en bois de deux essences (Pin et Epicéa) soumis à des humidités variables entre 0 et 50% a été menée. La phase de modélisation et de simulation a montré que la dispersion fréquentielle est significative seulement dans le cas d’un béton humide à forte salinité et que l’anisotropie et le gradient ont un effet significatif sur la propagation. La phase expérimentale a montré que dans le cas d’un matériau homogène, la vitesse est indépendante de la distance émetteur-récepteur, et qu’elle est variable dans le cas d’un béton soumis à un gradient d’humidité. Enfin, les essais sur le bois montrent que la partie réelle de sa permittivité est croissante en fonction de l’humidité. Le contraste de permittivité entre direction longitudinale et transversale (tangentielle ou radiale) est négligeable à l’état sec du matériau et commence à être significatif à partir de la saturation des fibres. Cela permet de privilégier la direction longitudinale à la direction transversale pour évaluer l’humidité des structures en bois. / The reinforced concrete or the timber structures are degraded under mechanical and climatic actions. Physical and mechanical properties of these materials are linked to outdoor exposure conditions and their variations. The early non-destructive evaluation of these properties before the initiation of degradations is a need for masters of structures in order to predict the service life of the structures in a context of sustainable management of the built heritage. The presence of water in the pores of the concrete is a factor which facilitates the penetration of aggressive agents (carbon dioxide, chlorides, etc. responsible of the initiation of pathologies such as steel corrosion). In the case of wood material, the most common causes of damage are often of biological origin (fungi and insects). Moisture is also recognized as one of the most important conditions for the development of these attacks. It is therefore necessary to evaluate and quantify the spatial variation of the humidity in the building materials to limit repair actions. The GPR system (Ground Penetrating Radar) is an auscultation tool of materials which is completely non-destructive, fast, compact, and contactless. This technique is based on the propagation of electromagnetic waves. This propagation is strongly linked to the permittivity and the conductivity of the material that are highly sensitive to changes in humidity. The objective of this thesis is twofold: first, modelling the effect of moisture variation in a homogeneous material, multi-layers or with gradient, and secondly, to experimentally quantify the effect of a moisture gradient on the concrete and the effect of the anisotropy (case of wood material). An analytical model has been developed based on the concept of mixing laws (Fitted on experimental measurements of the permittivity by taking into account the effect of the frequency dispersion) and the propagation of a plane wave. A numerical simulation was used to assess the effects of a gradient and the effect of an anisotropic medium on the propagation velocity of the radar waves. The experimental phase was performed on a homogeneous and isotropic model material such as sand to compare different measurement methods of the velocity of the direct wave. A frequency analysis of the attenuation was also examined to evaluate the dispersion of the attenuation in a considered homogeneous medium. The second part of the experiment was to monitor, by radar measurements, the drying of a concrete slab instrumented by humidity sensors. Finally, an experimental campaign on samples of two species of wood (Pine and Spruce) with different moisture content between 0 and 50% was conducted. The modelling and simulations phase has shown that the frequency dispersion is significant only in the case of wet concrete with a high salinity content. The anisotropy and the gradient have a significant effect on the spread. The experimental phase showed that in the case of a homogeneous material, the speed is independent of the offset (distance between transmitter and receiver), and it varies in the case of concrete with a moisture gradient. Finally, tests on the timber indicate that the real part of its permittivity increases as a function of moisture. The contrast between longitudinal and transverse direction (tangential or radial) is negligible in the dry state of the material and begins to be very significant from the fiber saturation point. It indicates that the longitudinal direction, instead of the transverse direction, is more convenient to measure the moisture of wood structures.

This thesis is focused on the evaluation of rotor dynamics of the induction machine, which can be used as a basis for online diagnosis of driven load in the future. It describes the problem of time varying loading torque at its impact to electromagnetic variables in induction machine. Followed by the possible ways of monitoring and diagnostic of loading torque using Fourier analysis on supply current.

Cette thèse a été effectuée dans le cadre du projet européen FP7 EMPHATIC (Enhanced Multicarrier Techniques for Professional Ad-Hoc and Cell-Based Communications). Plusieurs universités européennes et deux partenaires industriels: THALES Communications Security et CASSIDIAN ont participé à ce projet. L'objectif de ce projet est de développer, d'évaluer et de démontrer les apports des techniques multi-porteuses avancées, permettant une meilleure utilisation des bandes de fréquences radio existantes en fournissant des services de données à large bande, en coexistence avec les services traditionnels à bande étroite. Le projet porte sur l'application de radiocommunications mobiles professionnelles (Professional Mobile Radio : PMR). L'idée principale de ce projet est d'analyser la viabilité des systèmes à large bande utilisant des bancs de filtres (Filter Bank Multi Carrier : FBMC) conjointement avec une modulation d'amplitude en quadrature avec décalage (Offset Quadrature Amplitude Modulation : OQAM) dans le cadre de la 5ème génération (5G) des systèmes radio-mobiles. La modulation FBMC-OQAM se positionne comme candidate potentielle pour les futurs systèmes de communication. Cette modulation avancée offre de nombreux avantages tels que l’excellente localisation fréquentielle de sa densité spectrale de puissance (DSP), une robustesse au bruit de phase, aux décalages de fréquence ainsi qu’à l’asynchronisme entre les utilisateurs. Ces atouts, la rendent plus attrayant qu’OFDM pour l’application PMR, la radio cognitive (CR) et la 5G. Cependant, comme toute autre technique de modulation muti-porteuses, FBMC-OQAM souffre d’un facteur de crête ou d’un PAPR (pour Peak to Average Power Ratio) élevé. Lorsque l'amplificateur de puissance (AP), utilisé au niveau de l’émetteur, est opéré proche de sa zone non-linéaire (NL), ce qui est le cas dans la pratique, la bonne localisation fréquentielle de la DSP du système FBMC/OQAM est sérieusement compromise, en raison des remontées spectrales. Le premier objectif de cette thèse est de prédire l'étendue des remontées spectrales dans les systèmes FBMC-OQAM, introduites par la non-linéarité AP. Le deuxième objectif de ce travail est de proposer des techniques, pour les systèmes FBMC-OQAM, permettant la réduction du PAPR et la linéarisation de l’AP, afin d'atténuer les effets NL. L’utilisation des cumulants, a permis de prédire les remontées spectrales pour les signaux FBMC-OQAM après amplification NL. En outre, certains algorithmes de réduction du PAPR, basées sur des approches probabilistes et des techniques d'ajout de signaux, ont été proposés. La capacité de coexistence du système à large bande utilisant FBMC-OQAM avec des systèmes PMR à bande étroite en présence de PA a été analysée et il a été démontré que la coexistence est possible, à condition qu'il y est une bonne combinaison entre le recul du signal à l’entrée de l’AP (Input Back-Off : IBO), la réduction du PAPR et la linéarisation de l’AP. Enfin, une nouvelle technique de linéarisation de l’AP a été proposée pour le système FBMC-OQAM. / This thesis is part of the European FP7 EMPHATIC project (Enhanced Multicarrier Techniques for Professional Ad-Hoc and Cell-Based Communications) including various European universities and two main industrial partners: THALES Communications Security and CASSIDIAN. The EMPHATIC objective is to develop, evaluate and demonstrate the capability of enhanced multi-carrier techniques to make better use of the existing radio frequency bands in providing broadband data services in coexistence with narrowband legacy services. The project addresses the Professional Mobile Radio (PMR) application. The main idea is to analyze the viability of broadband systems based on filter-bank multi-carrier (FBMC) clubbed with o ffset quadrature amplitude modulation (OQAM) in the context of the future 5th Generation (5G) radio access technology (RAT). Increasingly, the FBMC-OQAM systems are gaining appeal in the probe for advanced multi-carrier modulation (MCM) waveforms for future communication systems. This advanced modulation scheme o ers numerous advantages such as excellent frequency localization in its power spectral density (PSD), a robustness to phase noise, frequency off sets and also to the multi-user asynchronism; making it more appealing than OFDM for PMR, cognitive radio (CR) and 5G RAT. However, like any other MCM technique, FBMC-OQAM suff ers from high PAPR. When the power amplifi er (PA) non-linearity, which is realistic radio-frequency impairment, is taken into account; the good frequency localization property is severely compromised, due to the spectral regrowth. The first objective of this PhD thesis is, to predict the extent of the spectral regrowth in FBMC-OQAM systems, due to the PA non-linearity. The second objective is to probe techniques for FBMC-OQAM systems, such as PAPR reduction and PA linearization, in order to mitigate the NL eff ects of PA. By cumulant analysis, spectral regrowth prediction has been done for FBMC-OQAM systems. Also, some algorithms for PAPR reduction, which are based on probabilistic approach and adding signal methods, have been proposed. The coexistence capability of the FBMC-OQAM based broadband system with the narrowband PMR systems in the presence of PA has been analyzed and it has been found that coexistence is possible, provided there is a symbiotic combination of PA Input Back-off (IBO), PAPR reduction and PA linearization. Finally, a novel PA linearization technique has been proposed for FBMC-OQAM.

Les centres de données deviennent de plus en plus importants, allant de petites fermes de serveurs distribuées à des grandes fermes dédiées à des tâches spécifiques. La diffusion de services "dans le nuage" conduit à une augmentation incessante de la demande de trafic dans les centres de données. Dans cette thèse, nous étudions l'évolution des réseaux dans les centres de données et proposons des solutions à court et à long terme pour leur intra-connexion physique. Aujourd'hui, la croissance de la demande de trafic met en lumière la nécessité urgente d’interfaces à grande vitesse capables de faire face à la bande passante exigeant de nouvelles applications. Ainsi, à court terme, nous proposons de nouveaux transpondeurs optiques à haut débit, mais à faible coût, permettant la transmission de 200 Gb /s utilisant des schémas de modulation en intensité et à détection directe. Plusieurs types de modulations d’impulsions en amplitude avancées sont explorés, tout en augmentant la vitesse à des débits symboles allant jusqu’à 100 GBd. La génération électrique à haute vitesse est réalisé grâce à un nouveau convertisseur analogique-numérique intégré, capable de doubler les vitesses des entrées et de générer des signaux à plusieurs niveaux d’amplitude. Cependant, le trafic continuera sa croissance. Les centres de données actuels reposent sur plusieurs niveaux de commutateurs électroniques pour construire un réseau d'interconnexion capable de supporter une telle grande quantité de trafic. Dans une telle architecture, la croissance du trafic est directement liée à une augmentation du nombre des composants du réseau, y-compris les commutateurs avec plus de ports, les interfaces et les câbles. Le coût et la consommation d'énergie qui peut être attendus à l'avenir est intenable, ce qui appelle à une réévaluation du réseau. Par conséquent, nous présentons ensuite un nouveau concept fondé sur la commutation de "slots" optiques (Burst Optical Slot Switching, i.e. BOSS) dans lequel les serveurs sont connectés via des nœuds BOSS à travers des anneaux de fibres multiplexé en longueur d'onde et en temps, et organisés dans une topologie en tore. Au cours de cette thèse, nous étudions la mise en œuvre des nœuds BOSS; en particulier, la matrice de commutation et les transpondeurs optiques. L'élément principal au sein de la matrice de commutation est le bloqueur de slots, qui est capable d'effacer n’importe quel paquet (slot) sur n’importe quelle longueur d'onde en quelques nanosecondes seulement. D'une part, nous explorons l'utilisation d'amplificateurs optiques à semi-conducteurs comme portes optiques à utiliser dans le bloqueur des slots, et étudier leur cascade. D'autre part, nous développons un bloqueur de slots intégré monolithiquement capable de gérer jusqu'à seize longueurs d'onde avec la diversité de polarisation. Ensuite, nous présentons plusieurs architectures de transpondeur et nous étudions leur performance. La signalisation des transpondeurs doit répondre à deux exigences principales: le fonctionnement en mode paquet et la résistance au filtrage serré. D'abord, nous utilisons des transpondeurs élastiques qui utilisent des modulations Nyquist N-QAM, et qui adaptent le format de modulation en fonction du nombre de nœuds à traverser. Ensuite, nous proposons l'utilisation du multiplexage par répartition orthogonale de la fréquence en cohérence optique (CO-OFDM). Avec une structure de paquet inhérente et leur grande adaptabilité fréquentielle, nous démontrons que les transpondeurs CO-OFDM offrent une capacité plus élevée et une meilleure portée que leurs homologues Nyquist. Finalement, nous comparons notre solution BOSS avec la topologie Clos replié utilisée aujourd'hui. Nous montrons que notre architecture BOSS nécessite 400 fois moins de transpondeurs et de câbles que les réseaux de commutation électronique d'aujourd'hui, ce qui ouvre la voie à des centres de données hautement évolutifs et durables / Data centers are becoming increasingly important and ubiquitous, ranging from large server farms dedicated to various tasks such as data processing, computing, data storage or the combination thereof, to small distributed server farms. The spread of cloud services is driving a relentless increase of traffic demand in datacenters, which is doubling every 12 to 15 months. Along this thesis we study the evolution of data center networks and present short- and long-term solutions for their physical intra-connection. Today, rapidly-growing traffic in data centers spotlights the urgent need for high-speed low-cost interfaces capable to cope with hungry-bandwidth demanding new applications. Thereby, in the short-term we propose novel high-datarate low-cost optical transceivers enabling up to 200 Gb/s transmission using intensity-modulation and direct-detection schemes. Several advanced pulse amplitude modulation schemes are explored while increasing speeds towards record symbol-rates, as high as 100 GBd. High-speed electrical signaling is enabled by an integrated selector-power digital-to- analog converter, capable of doubling input baud-rates while outputting advance multi-level pulse amplitude modulations. Notwithstanding, data centers’ global traffic will continue increasing incessantly. Current datacenters rely on high-radix all-electronic Ethernet switches to build an interconnecting network capable to pave with such vast amount of traffic. In such architecture, traffic growth directly relates to an increase of networking components, including switches with higher port-count, interfaces and cables. Unsustainable cost and energy consumption that can be expected in the future calls for a network reassessment. Therefore, we subsequently present a novel concept for intra-datacenter networks called burst optical slot switching (BOSS); in which servers are connected via BOSS nodes through wavelength- and time-division multiplexed fiber rings organized in a Torus topology. Along this thesis we investigate on the implementation of BOSS nodes; in particular, the switching fabric and the optical transceivers. The main element within the switching fabric is the slot blocker, which is capable of erasing any packet of any wavelength in a nanosecond time-scale. On the one hand, we explore the use of semiconductor optical amplifiers as means of gating element to be used within the slot blocker and study their cascadability. On the other hand we develop a monolithically integrated slot blocker capable of handling up to sixteen wavelength channels with dual-polarization diversity. Then we present several transceiver architectures and study their performances. Transceivers’ signaling needs to fulfill two main requirements: packet-mode operation, i.e. being capable of recovering few microsecond –long bursts; and resiliency to tight filtering, which occurs when cascading many nodes (e.g. up to 100). First we build packet-mode Nyquist-pulse-shaped N-QAM transceivers, which adapt the modulation format as a function of the number of nodes to traverse. Later we propose the use of coherent-optical orthogonal frequency division multiplexing (CO-OFDM). With inherent packet structure and high spectral tailoring capabilities, we demonstrate that CO-OFDM-based transceivers offer higher capacity and enhanced reach than its Nyquist counterpart. Finally, we compare our BOSS solution to today’s Folded Clos topology, and show that our BOSS architecture requires x400 fewer transponders and cables than today’s electronic switching networks, which paves the way to highly scalable and sustainable datacenters

Konsistensen på en gel bestående av tvärbunden hyaluronsyra beror av tre faktorer: total koncentration hyaluronsyra, gelningsgrad och tvärbindningsdensitet. För att utföra detta projekt erhölls tre olika geler med olika tvärbindningsdensitet. Dessa geler späddes dels med lösning av fri, icke tvärbunden, HA från 100 % gelningsgrad till 90 % och 80 %. De olika gelningsgraderna späddes också med natriumkloridlösning från den totala koncentrationen HA, 35 mg HA/g gel, till 25 mg/g och 15 mg/g. Projekts huvudfråga är att kartlägga gelens reologiska egenkaper då både total koncentration HA och gelningsgrad varieras. För att kunna kartlägga detta har en reometer brukats där följande tre tester körts: tidssvep, frekvenssvep och amplitudsvep. Från erhållen data har sedan två parametrar som representerar gelkompositionernas viskösa egenskaper (G'') och elastiska egenskaper (G') observerats. Även mätning av extruderingskraft har genomförts för att dra vidare paralleller och slutsatser mellan extruderingskraften och de reoligiska egenskaperna. Ur resultaten ses att förlusttangenten tenderar att sjunka när gelningsgraden ökar, d.v.s. gelerna blir då mer viskösa och mindre elastiska. Förlusttangenten sjunker även vid ökande total koncentration HA vilket betyder att G’ ökar mer än G’’ i vardera punkt som gör att förlusttangenten minskar.Det gick även att avläsa att de viskösa egenskaperna i gelen ökar då total koncentration hyaluronsyra minskar samt att de viskösa egenskaperna i gelerna minskar vid en sjunkande gelningsgrad. Mellan gelningsgrad 90-100 % och total koncentration HA 25-35 mg HA/g har analyserna som gjorts i detta projekt gett följande slutsatser. Konsistensen på gel A och C är mer påverkade av gelningsgraden än total koncentration HA. För gel B kan ingen dominerande parameter utläsas. / The softness of a gel made of crosslinked HA (HA = hyaluronic acid) depends onthree factors. One is the amount of free hyaluronic acid in the gel. Another is thedensity of the crosslinked network, which is the molecular entanglements in the gel.The third is the total concentration of HA. In this project a rheometer is used to measure the rheological properties by runningthe following tests: time sweep, frequency sweep and amplitude sweep. From theobtained data, parameters related to viscous properties (G’’) and elastic properties(G’) of the gels were observed. 27 different compositions of gels with three differentconcentrations (35 mg HA/g, 25 mg HA/g, 15 mg HA/g), three different gel contents(100%, 90%, 80%) and three different densities of crosslinked network (A, B, C) wereanalyzed. To draw further conclusions an analysis of extrusion force was performedas well. The results from the frequency sweeps show that the loss tangent for a gel increasedas the total concentration of HA was reduced and that the loss tangent for a gelincreased as the gel content was decreased. This indicates that the gels become moreviscous when either the concentration of HA or the gel content was decreased. Anincrease in concentration of HA results in an increase of G' and an increase of gelcontent also results in an increase of G'. The results from the amplitude sweeps showthat xG' (xG' = storage modulus at the crossover point between G' and G'') increasesas either the concentration of HA or the gel content is increased. For xStrain (xStrain= deformation of the gel at the crossover point) and xStress (xStress = the stressapplied to the gel at the crossover point) no clear trend can be seen regarding the gelcontent. But an increase in concentration of HA results in an increase of both xStrainand xStress. The results from the analysis of extrusion force show that an increase intotal concentration HA increases the force.